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VIETNAM ACADEMY OF AGRICULTURAL SCIENCES NGUYEN NHU HOA CONSTRUCTION OF DNA SEQUENCE DATABASE FOR RAPID IDENTIFICATION AND DIVERSITY EVALUATION OF DENDROBIUM SPECIES IN SOUTHERN VIETN

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VIETNAM ACADEMY OF AGRICULTURAL SCIENCES

NGUYEN NHU HOA

CONSTRUCTION OF DNA SEQUENCE DATABASE FOR RAPID IDENTIFICATION AND DIVERSITY EVALUATION

OF DENDROBIUM SPECIES IN SOUTHERN VIETNAM

Major: Biotechnology

Code: 9 42 02 01

SUMMARY OF DOCTORAL THESIS

Ho Chi Minh City, 2021

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The study was completed at:

VIETNAM ACADEMY OF AGRICULTURAL SCIENCES

Supervisor:

1 Duong Hoa Xo, Assoc Prof PhD

2 Tran Kim Dinh, PhD

The thesis can be referred at:

1 National Library of Vietnam

2 Library of Vietnam Academy of Agricultural Sciences

3 Library of Institute of Agricultural Sciences for Southern Vietnam

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INTRODUCTION

1 Rationale of the study

Orchid (family Orchidaceae), thanks to its highly diversified and beautiful flowers, has long attracted great interest from large groups

of spectators In Vietnam, it consists of a rich and special taxon with

significant value in many aspects Dendrobium is the largest genus

amongst the orchid family and also the most favored and sought in Vietnam Many works have been done on orchid conservation, including the Orchid Collection of the Biotechnology Center Of Ho Chi Minh City with 400 orchid samples including 190 from the

Dendrobium genus Morphological identification of the orchids

requires complete samples with all the anatomical components –

especially the flowers whose information is vital – which is not always possible, however Amongst molecular technologies, DNA

barcoding is acknowledged as a useful tool for plant identification,

including orchids

The study aimed to construct a DNA barcode reference database

for Dendrobium identification Morphology identification was

performed on 40 flowered samples collected in southern Vietnam

On the molecular part, the ITS, rbcL, matK, and trnH-psbA regions

of 71 samples from 25 species and 13 hybrid samples were sequenced, and taxonomic diversity and phylogenetic relationship were determined by bioinformatics tool The results were applied for the paternity test of several hybrid samples

2 Aim of the study

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This study aimed to construct a DNA sequence database and DNA barcodes for the identification and diversity evaluation of

Dendrobium samples collected in southern Vietnam

3 Scientific and practical significance

3.1 Scientific significance

The study successfully determined the genetic diversity of

Dendrobium orchids in southern Vietnam based on morphological

traits and DNA barcodes The data were submitted to GenBank and

enriched the Dendrobium database which laid the basis for further

researches Potential markers for rapid identification of Dendrobium were proposed to conserve the rare and valuable genetic resources in Vietnam

3.2 Practical significance

This study proposed the application of DNA barcoding for more

accurate and rapid identification of Dendrobium orchids for genetic

conservation

4 Object and scope of the study

4.1 Object of study

The orchid species in the Dendrobium genus

4.2 Scope of the study

The study was performed on orchid samples of the Orchid Collection, Biotechnology Center of Ho Chi Minh City The samples were also the results of the previous study “Collection, import, selection and rapid multiplication of the orchid cultivars for

domestic consumption and export” of Dr Hoa-Xo Duong et al

(2011)

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This study evaluated and constructed a phylogenetic tree based

on 72 morphological traits of 40 Dendrobium samples This study also evaluated the sequences of the rbcL, matK, trnH-psbA, and ITS

of 84 samples (including 71 samples of 25 Dendrobium species in

southern Vietnam and 13 hybrid samples)

5 Novel contributions of the study

This study provided the data of the markers ITS, matK, rbcL, and trnH-psbA of native Vietnamese Dendrobium species, submitted to GenBank database, amongst which many rbcL and

trnH-psbA sequences had not or limitedly published on that

database

This study preliminarily evaluated the genetic diversity of

Dendrobium DNA markers in southern Vietnam and proposed the

potential markers for Dendrobium identification

6 Structure of the thesis

The thesis consists of 127 pages excluding Appendixes It includes Introduction (5 pages), Chapter 1: Literature review and theoretical framework (38 pages), Chapter 2: Materials and methods (22 pages), Chapter 3: Results and discussion (48 pages), Conclusion and Recommendation (2 pages), and References (12 pages), uses 26 Vietnamese and 96 English reference works The thesis includes 11 tables, 43 figures, 8 appendixes, and 4 published works

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CHAPTER 1 LITERATURE REVIEW AND THEORETICAL

FRAMEWORK

The study referred to and summarized various Vietnamese and English literary works related to (1) Introduction of the Orchidaceae

family, (2) Introduction of the Dendrobium genus, (3) Current status

of Dendrobium conservation and identification in Vietnam and worldwide, (4) Studies related to Dendrobium genetic diversity, and

(5) DNA Barcoding and their applications in species identification

1.1 Introduction of the Orchidaceae family

The Orchidaceae, commonly known as the orchid family, is the largest monocot family and the second largest flowering plant family only after Asteraceae (Takhtajan, 1987)

1.2 Introduction to Dendrobium genus

1.2.1 Classification

Kingdom Plantae

Phylum Angiospermae (Magnoliophyta)

Class Monocotylendones (Liliopsida)

Dendrobium is found only in the Eastern Hemisphere, from

Oceania, throughout South Pacific, the Philippines, India, several

spotted in Japan, and mostly occurred in South East Asia

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1.2.3 Diversity and richness

Dendrobium genus consists of 1600 species with high diversity in

color, size, and morphology for adaptation to a great range of ecological habitats

1.2.4 Morphology

1.3 Dendrobium conservation and identification in Vietnam and

worldwide

Dendrobium conservation worldwide has been carried out in

various centers and projects In vitro tissue culture also attracts

significant attention Accurate sample identification is essential for all conservation and cultivation efforts Morphological traits have long been employed for such works, however, in many cases, it is difficult to rely on morphology only Advances in molecular genetics, nucleotide sequence technology, bioinformatics, and DNA barcoding enable rapid and accurate identification of known taxa and allow data retrieval from them

1.4 Genetic diversity researches on Dendrobium

1.4.1 Markers for genetic diversity evaluation of Dendrobium

Various markers have been used for genetic diversity evaluation

of populations and species such as morphological, cytological, biochemical, and DNA markers Molecular markers currently are considered the most effective evaluation tools as they are not affected by changes in environment and phenotype There are many types of molecular markers and various technique employed in this field, some of them have been used for orchid diversity assessment such as AFLP (Amplified Fragment Length Polymorphism), RAPD (Randomly Amplified Polymorphism DNA), RFLPs (Restriction

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Fragment Length Polymorphisms), SSRs (Microsatellite or Simple Sequence Repeats), ISSR (Inter-Simple Sequence Repeat), and the method utilizing DNA sequence database

1.4.2 Genetic diversity researches on Dendrobium

Researches on Dendrobium genetic diversity, thanks to highly

developed biotechnology, have been strongly promoted in Singapore, Taiwan, or Thailand, using various markers such as SSR, AFLP, RAPD, ISSR, and RFLP

1.5 DNA barcoding in taxa identification

DNA barcode is one or several nucleotide sequences gene sequences taken from a standardized portion of the genome used to identify species The technique was first applied to animals

1.5.1 Sequences for construction of DNA barcodes

Plant DNA in the nucleus, chloroplast, and mitochondria are all used for molecular identification The mitochondrial genome has the slowest evolution rate, followed by the chloroplastic and the nuclear genomes, respectively

Kress et al (2005) proposed two potential regions for DNA barcoding in flowering plants which are the ITS and the trnH-psbA

The Kew, Royal Botanic Gardens (UK) proposed five candidate

regions including matK, rpoC1, rpoB, accD, and và YCF5, together with the combination of multiple region (rpoC1 + rpoB + matK, or

rpoC1 + matK + trnH-psbA) for better efficiency The CBOL

proposed a combination of matK and rbcL for plant barcoding

(2009) The China Plant BOL Group proposed combining ITS with

matK + rbcL for plant barcoding (2011) The 4th International

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Barcode of Life Conference proposed using matK + rbcL +

psbA-trnH

Based on the mentioned works, this study chose the region of

ITS, rbcL, matK, and psbA – trnH for the evaluation of Dendrobium

genetic diversity

1.5.2 DNA barcoding studies on orchids and Dendrobium

As soon as the concept of DNA barcoding was proposed, various researches, in Vietnam and worldwide, have been performed on building a DNA database for native species including orchids Many

studies have been done on the regions of ITS, ITS1, ITS2,

psbA-trnH, matK, rbcL, rpoB, or rpoC, most of which indicated a lower

discrimination power in chloroplastic barcodes than in nuclear ones – amongst which the ITS region has the highest power A barcode using multiple sequences is essential for plant species in general and

Dendrobium species in specific

The ITS and psbA-trnH sequences were seen as potential markers for Dendrobium species, and the more conserved matK and rbcL

could be used as data for phylogenetic analysis and in combination with other sequences for DNA barcoding

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CHAPTER 2 MATERIAL AND METHODS

2.1 Materials, time, and location

The study was carried out on Dendrobium spp samples

The morphological description was performed on 40

Dendrobium samples from the Orchid Collection of the

Biotechnology Center of Ho Chi Minh City

Sequencing was performed on leaf DNA extracted from 84

Dendrobium samples, including 71 samples from 25 native species

for the DNA barcoding database, and 13 hybrid samples for parental identification

This study was carried out from August 2014 to August 2018, at the Biotechnology Center of Ho Chi Minh City

Objective 4: Using DNA data for paternity test of Dendrobium

hybrids cultivated by the Biotechnology Center of Ho Chi Minh City and from other sources

2.3 Methods

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2.3.1 Phylogenetic tree construction based on morphological traits

Morphological traits were described for 40 flowered samples from the Biotechnology Center of Ho Chi Minh City

2.3.1.1 Dendrobium morphological description

Forty flowered samples were described uniformly for 72

morphological traits, using the DUS criteria for Cymbidium and

Phalaenopsis Flower anatomy was analyzed horizontally and

vertically Photographic illustrations of each sample were recorded

2.3.1.2 Dendrobium phylogenetic relationship based on morphology

The phylogenetic tree was built using NTSYS PC software

2.3.2 DNA barcode reference database for the samples

2.3.2.1 Sample collection and storage

Fresh leaf samples were collected from morphologically healthy plants and stored in numbered tubes at -20oC to -80oC

2.3.2.2 Genomic DNA extraction

Leaf DNA was extracted using the CTAB method or specialized kit (GeneJET Plant Genomic DNA Purification Mini Kit)

2.3.2.3 PCR and gel electrophoresis

The ITS, matK, rbcL, and trnH-psbA sequences were amplified

by PCR using designated primers PCR products were examined by gel electrophoresis on 0.8% agarose gel, at 120V, 65mA for 20 minutes

Table 1 Primers and thermal cycles for amplification of the ITS,

matK, rbcL, trnH-psbA regions

Regions Primers PCR cycles

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Regions Primers PCR cycles

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Raw sequences were adjusted by FinchTV to remove the ambiguities and check the peak reliability A BLAST search was performed on the NCBI database for the sequence similarity and origin, and sequence alignment was performed by SeaView 4.0 The ITS2 sequence was obtained from the ITS region (JN388570.1)

2.3.3 Evaluation of Dendrobium genetic diversity by DNA markers

Genetic diversity evaluation based on phylogenetic branching was performed on discrete and combined markers The phylogenetic tree was constructed by MEGA 7.0 software using the Maximum Likelihood algorithm based on the Kimura-2 parameter model with

1000 bootstrap replicates Paphiopedilum sequence was used as an

outgroup

2.3.4 Evaluation of the marker discrimination power

The most optimal markers were chosen based on species discrimination power using the phylogenetic tree together with DNA indels (insertion and deletion mutations) data, and the “Best Match / Best Close Match” techniques in which the genetic distances of the target sequences were compared

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CHAPTER 3 RESULTS AND DISCUSSION

3.1 Phylogenetic tree based on Dendrobium morphology

3.1.1 Morphological description of the Dendrobium samples

This study successfully described the morphology of 40

Dendrobium samples including 37 natives and 3 hybrids; each was

recorded for 72 standardized traits based on DUS criteria, with five photographic images of high resolution Morphological evaluation

managed to detect errors in the identification of the Dendrobium

chrysotoxum Lindl – which was previously mistaken for Dendrobium thyrsiflorum Lindl

3.1.2 Genetic relationship between 40 Dendrobium samples

The data of 72 recorded morphological traits partly revealed the

genetic relationship between the 40 sampled Dendrobium, however,

several close taxa with similar appearance could not be discriminated

In detail, the morphological assessment categorized the 40

samples into two groups Group I included D amabile và D

palpebrae Group II included 2 sub-groups The sub-group IIA (17

samples) had only one member with pendulous stem, while the

sub-group IIB (21 samples) had 10 members with the same trait D

anosmum (7,8,9,10), D aphyllum (11,12), and D parishii (28) with

close phylogenetic relationship and morphological similarity, and the

hybrid of D anosmum and D aphyllum, all were grouped together However the hybrid (D anosmum x D parishii) was put in a different cluster, together with D hercoglossum, D heterocarpum, and D venustum D primulinum and D crepidatum due to the

morphological similarity were together grouped in a separated cluster

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