Cr Thursday, September 21, 2017 Cr(357.9nm) File Comment: Comment: Furnace Add 0.1% La(Lanthanum) solution Instrument Information Device Name: Type AA ASC GFA AA Model Name AA-6300 ASC-6000 GFA-EX7 ROM Version 1.08 1.62 1.00 S/N A30524100188 A30324101696YS A30534100055LP Optics Parameters Element: Socket #: Lamp Current Low(Peak)(mA): Wavelength(nm): Slit Width(nm): Lamp Mode: Cr 10 357.9 0.7 BGC-D2 Measurement Parameters Order: Zero Intercept: Conc Unit: Signal Processing: 1st Non-Pass ppb Peak Height Blank Standard Sample Reslope Num Reps 2 2 Furnace Program Temp Time(sec) 150 20 250 10 800 10 800 10 800 2300 2500 Max Reps 3 3 HeatMode RAMP RAMP RAMP STEP STEP STEP STEP GFA Tube Last Coating Cycle Number of Boost Cycles ASC Parameters Rinse with Sample Mixing Injection Volume(uL) Injection Speed(uL/sec) Intake Speed(uL/sec) RSD Limit 7.00 7.00 7.00 7.00 Sens REGULAR REGULAR REGULAR REGULAR HIGH HIGH REGULAR SD Limit 0.0000 0.0000 0.0000 0.0000 GasType Flow Rate(L/min) #1 0.10 #1 0.10 #1 1.00 #1 1.00 #1 0.00 #1 0.00 #1 1.00 Unknown 1 No No 20 25 130 D:\VIET - K25\14042017-23 - diem chuan 9966.aa Page Sample OFF OFF OFF OFF OFF ON OFF Discharge Speed(uL/sec) Diluent Reagent Reagent Reagent Sample Intake Order 150 R1 R2 R3 R4 Diluent -> Reagent -> Reagent -> Reagent -> Sample QA/QC Parameters IDL CRDL 0.0000 0.0000 TV Method Order Zero Intercept: Conc Unit: Calibration Curve 1st Non-Pass ppb Blank Condition Reslope Condition Action BLK STD STD STD STD STD STD STD Sample ID Auto OFF OFF Frequency 20 20 True Value 0.0000 0.2000 1.0000 2.0000 3.0000 4.0000 5.0000 7.0000 Auto Dilution & Remeasurement QC Type Criteria Pos 1 Vol 10 10 Sample Group Weight Factor Vol.Factor Dil.Factor Corr.Factor Actual Conc Unit QC Type SPK PDS DUP Sample ID Dil 0 0 0 0 Dil 0 R1 0 0 0 0 R1 0 R2 0 0 0 0 R2 0 R3 0 0 0 0 R3 0 Retry Out of Ctrl Action Dil 0 R1 0 R2 0 R3 0 Dil 0 R1 0 R2 0 R3 0 1.000000 1.00 1.00 1.000000 NONE SA Conc UNK Prep Param Spike Prep Param Vol 20 20 20 20 20 20 20 20 Vol 10 10 No Judge Calc ICV/CCV Prep Param ICB/CCB Prep Param Action Pos Pos 1 0.0000 Vol 10 10 Pos Judge Calc %R %R %R Criteria 85.0% to115.0% 85.0% to115.0% 20.0% Retry OFF OFF OFF Out of Ctrl Action Mark and Continue Mark and Continue Mark and Continue LCS Prep Param PB Prep Param True Value 0.0000 Pos 1 Vol 10 10 Dil 0 R1 0 R2 0 R3 0 : BLK -0.200 0.000 -0.100 0.000 0.100 0.200 0.300 0.400 0.500 0.600 0.700 0.800 0.600 0.700 0.800 0.600 0.700 0.800 4.000 Abs BG Data Process Range 0.0037 -0.0041 0.00-4.00 Date Time User Name Device Name 4/14/2017 11:16:53 AM(+0700) System Administrator AA -0.200 0.000 -0.100 0.000 0.100 0.200 0.300 0.400 0.500 4.000 X Abs BG Data Process Range X 0.0050 -0.0023 0.00-4.00 Date Time User Name Device Name 4/14/2017 11:19:01 AM(+0700) System Administrator AA -0.200 0.000 -0.100 0.000 0.100 0.200 0.300 0.400 0.500 4.000 Abs BGData Process Range 0.0032 0.0012 0.00-4.00 Date Time User Name Device Name 4/14/2017 11:21:16 AM(+0700) System Administrator AA : BLK Average Abs BG 0.0034 -0.0014 R4 Pos VOL R1 R2 20 R3 %RSD TotalVolume 20 10.25 SD 0.0004 Calibration Curve (C# : 01) Conc Abs Abs (ppb) 0.020 0.010 0.000 0.000 2.500 5.000 Conc(ppb) 7.500 2.0000 0.0100 3.0000 0.0137 4.0000 0.0174 5.0000 0.0218 7.0000 0.0267 0.2000 0.0035 1.0000 0.0059 Abs=0.0035449Conc+0.0029006 r=0.9966 : STD -0.200 0.000 -0.100 0.000 0.100 0.200 0.300 0.400 0.500 4.000 X M True Value Conc Abs BG Data Process Range X M 0.2000 -0.4797 0.0012 -0.0009 0.00-4.00 Date Time User Name Device Name 4/14/2017 11:23:31 AM(+0700) System Administrator AA 0.600 0.700 0.800 -0.200 0.000 -0.100 0.000 0.100 0.200 0.300 0.400 0.500 0.600 0.700 0.800 0.600 0.700 0.800 0.600 0.700 0.800 0.600 0.700 0.800 0.600 0.700 0.800 4.000 X M True Value Conc Abs BG Data Process Range X M 0.2000 -0.3105 0.0018 -0.0023 0.00-4.00 Date Time User Name Device Name 4/14/2017 11:25:48 AM(+0700) System Administrator AA -0.200 0.000 -0.100 0.000 0.100 0.200 0.300 0.400 0.500 4.000 X M True Value Conc Abs BG Data Process Range X M 0.2000 0.0845 0.0032 -0.0006 0.00-4.00 Date Time User Name Device Name 4/14/2017 11:28:03 AM(+0700) System Administrator AA : STD Average X True Value X 0.2000 TotalVolume 20 C# 01 Pos VOL R1 R2 20 R3 R4 0 : STD -0.200 0.000 -0.100 0.000 0.100 0.200 0.300 0.400 0.500 4.000 X True Value Conc Abs BG Data Process Range X 1.0000 2.6234 0.0122 -0.0015 0.00-4.00 Date Time User Name Device Name 4/14/2017 11:30:18 AM(+0700) System Administrator AA -0.200 0.000 -0.100 0.000 0.100 0.200 0.300 0.400 0.500 4.000 X True Value Conc Abs BG Data Process Range X 1.0000 2.2566 0.0109 -0.0011 0.00-4.00 Date Time User Name Device Name 4/14/2017 11:32:34 AM(+0700) System Administrator AA -0.200 0.000 -0.100 0.000 0.100 0.200 0.300 0.400 0.500 4.000 X True Value Conc Abs BGData Process Range X 1.0000 1.5232 0.0083 0.0031 0.00-4.00 Date Time User Name Device Name 4/14/2017 11:34:49 AM(+0700) System Administrator AA : STD Average X True Value X 1.0000 TotalVolume 20 C# 01 Pos VOL R1 R2 20 R3 R4 0 : STD -0.200 0.000 -0.100 0.000 0.100 0.200 0.300 0.400 0.500 0.600 0.700 0.800 0.600 0.700 0.800 0.600 0.700 0.800 4.000 True Value Conc Abs BGData Process Range 2.0000 1.8053 0.0093 0.0015 0.00-4.00 Date Time User Name Device Name 4/14/2017 11:37:04 AM(+0700) System Administrator AA -0.200 0.000 -0.100 0.000 0.100 0.200 0.300 0.400 0.500 4.000 True Value Conc Abs BGData Process Range 2.0000 2.1720 0.0106 0.0014 0.00-4.00 Date Time User Name Device Name 4/14/2017 11:39:20 AM(+0700) System Administrator AA -0.200 0.000 -0.100 0.000 0.100 0.200 0.300 0.400 0.500 4.000 X True Value Conc Abs BG Data Process Range X 2.0000 2.7080 0.0125 -0.0029 0.00-4.00 Date Time User Name Device Name 4/14/2017 11:41:35 AM(+0700) System Administrator AA : STD Average True Value Conc Abs 2.0027 0.0100 R3 R4 TotalVolume SD BG 0.0014 Pos VOL R1 R2 2.0000 320 0 %RSD 20 0.0009 9.24 %R C# 100.0 01 : STD -0.200 0.000 -0.100 0.000 0.100 0.200 0.300 0.400 0.500 0.600 0.700 0.800 0.600 0.700 0.800 4.000 True Value Conc Abs BGData Process Range 3.0000 2.9619 0.0134 0.0011 0.00-4.00 Date Time User Name Device Name 4/14/2017 11:43:50 AM(+0700) System Administrator AA -0.200 0.000 -0.100 0.000 0.100 0.200 0.300 0.400 0.500 4.000 True Value Conc Abs BGData Process Range 3.0000 3.1311 0.0140 0.0027 0.00-4.00 Date Time User Name Device Name 4/14/2017 11:46:06 AM(+0700) System Administrator AA : STD Average True Value Conc Abs 3.0465 0.0137 R3 R4 TotalVolume SD 20 0.0004 BG 0.0019 Pos VOL R1 R2 3.0000 420 0 %RSD 3.10 %R C# 101.7 01 : STD -0.200 0.000 -0.100 0.000 0.100 0.200 0.300 0.400 0.500 0.600 0.700 0.800 0.600 0.700 0.800 0.600 0.700 0.800 4.000 X True Value Conc Abs BGData Process Range X 4.0000 3.6107 0.0157 0.0040 0.00-4.00 Date Time User Name Device Name 4/14/2017 11:48:21 AM(+0700) System Administrator AA -0.200 0.000 -0.100 0.000 0.100 0.200 0.300 0.400 0.500 4.000 True Value Conc Abs BGData Process Range 4.0000 4.2031 0.0178 0.0000 0.00-4.00 Date Time User Name Device Name 4/14/2017 11:50:36 AM(+0700) System Administrator AA -0.200 0.000 -0.100 0.000 0.100 0.200 0.300 0.400 0.500 4.000 True Value Conc Abs BGData Process Range 4.0000 3.9774 0.0170 0.0055 0.00-4.00 Date Time User Name Device Name 4/14/2017 11:52:51 AM(+0700) System Administrator AA : STD Average True Value Conc Abs 4.0903 0.0174 R3 R4 TotalVolume SD BG 0.0028 Pos VOL R1 R2 4.0000 520 0 %RSD 20 0.0006 3.25 %R C# 102.2 01 : STD -0.200 0.000 -0.100 0.000 0.100 0.200 0.300 0.400 0.500 0.600 0.700 0.800 0.600 0.700 0.800 4.000 True Value Conc Abs BGData Process Range 5.0000 5.1905 0.0213 0.0044 0.00-4.00 Date Time User Name Device Name 4/14/2017 11:55:07 AM(+0700) System Administrator AA -0.200 0.000 -0.100 0.000 0.100 0.200 0.300 0.400 0.500 4.000 True Value Conc Abs BGData Process Range 5.0000 5.5008 0.0224 0.0038 0.00-4.00 Date Time User Name Device Name 4/14/2017 11:57:22 AM(+0700) System Administrator AA : STD Average True Value Conc Abs 5.3315 0.0218 R3 R4 TotalVolume SD 20 0.0008 BG 0.0041 Pos VOL R1 R2 5.0000 620 0 %RSD 3.56 %R C# 106.6 01 : STD -0.200 0.000 -0.100 0.000 0.100 0.200 0.300 0.400 0.500 0.600 0.700 0.800 0.600 0.700 0.800 4.000 True Value Conc Abs BGData Process Range 7.0000 6.9959 0.0277 0.0015 0.00-4.00 Date Time User Name Device Name 4/14/2017 11:59:37 AM(+0700) System Administrator AA -0.200 0.000 -0.100 0.000 0.100 0.200 0.300 0.400 0.500 4.000 True Value Conc Abs BGData Process Range 7.0000 6.4317 0.0257 0.0052 0.00-4.00 Date Time User Name Device Name 4/14/2017 12:01:53 PM(+0700) System Administrator AA : STD Average True Value Conc Abs 6.7138 0.0267 R3 R4 TotalVolume SD BG 0.0034 Pos VOL R1 R2 7.0000 720 0 %RSD 20 0.0014 5.30 %R C# 95.9 01 : STD -0.200 0.000 -0.100 0.000 0.100 0.200 0.300 0.400 0.500 0.600 0.700 0.800 0.600 0.700 0.800 0.600 0.700 0.800 4.000 X True Value Conc Abs BGData Process Range X 1.0000 1.8335 0.0094 0.0046 0.00-4.00 Date Time User Name Device Name 4/14/2017 12:08:49 PM(+0700) System Administrator AA -0.200 0.000 -0.100 0.000 0.100 0.200 0.300 0.400 0.500 4.000 X True Value Conc Abs BGData Process Range X 1.0000 2.4541 0.0116 0.0002 0.00-4.00 Date Time User Name Device Name 4/14/2017 12:10:58 PM(+0700) System Administrator AA -0.200 0.000 -0.100 0.000 0.100 0.200 0.300 0.400 0.500 4.000 X True Value Conc Abs BGData Process Range X 1.0000 2.2284 0.0108 0.0027 0.00-4.00 Date Time User Name Device Name 4/14/2017 12:13:13 PM(+0700) System Administrator AA : STD Average X True Value X 1.0000 TotalVolume 20 C# 01 Pos VOL R1 R2 20 R3 R4 0 : STD -0.200 0.000 -0.100 0.000 0.100 0.200 0.300 0.400 0.500 0.600 0.700 0.800 0.600 0.700 0.800 0.600 0.700 0.800 4.000 X True Value Conc Abs BG Data Process Range X 0.2000 -0.3669 0.0016 -0.0024 0.00-4.00 Date Time User Name Device Name 4/14/2017 12:17:21 PM(+0700) System Administrator AA -0.200 0.000 -0.100 0.000 0.100 0.200 0.300 0.400 0.500 4.000 True Value Conc Abs BG Data Process Range 0.2000 0.3383 0.0041 -0.0031 0.00-4.00 Date Time User Name Device Name 4/14/2017 12:19:29 PM(+0700) System Administrator AA -0.200 0.000 -0.100 0.000 0.100 0.200 0.300 0.400 0.500 4.000 True Value Conc Abs BG Data Process Range 0.2000 -0.0002 0.0029 -0.0029 0.00-4.00 Date Time User Name Device Name 4/14/2017 12:21:44 PM(+0700) System Administrator AA : STD Average True Value Conc Abs BG 0.2000 0.1691 0.0035 -0.0030 R3 R4 TotalVolume SD Pos VOL R1 R2 120 0 %RSD 20 0.0008 24.24 %R C# 85.0 01 : STD -0.200 0.000 -0.100 0.000 0.100 0.200 0.300 0.400 0.500 0.600 0.700 0.800 0.600 0.700 0.800 0.600 0.700 0.800 4.000 X True Value Conc Abs BGData Process Range X 1.0000 2.3130 0.0111 0.0012 0.00-4.00 Date Time User Name Device Name 4/14/2017 12:23:59 PM(+0700) System Administrator AA -0.200 0.000 -0.100 0.000 0.100 0.200 0.300 0.400 0.500 4.000 True Value Conc Abs BG Data Process Range 1.0000 1.0154 0.0065 -0.0046 0.00-4.00 Date Time User Name Device Name 4/14/2017 3:36:01 PM(+0700) System Administrator AA -0.200 0.000 -0.100 0.000 0.100 0.200 0.300 0.400 0.500 4.000 True Value Conc Abs BG Data Process Range 1.0000 0.6769 0.0053 -0.0017 0.00-4.00 Date Time User Name Device Name 4/14/2017 3:38:15 PM(+0700) System Administrator AA : STD Average True Value Conc Abs BG 1.0000 0.8461 0.0059 -0.0032 R3 R4 TotalVolume SD 20 0.0008 Pos VOL R1 R2 220 0 %RSD 14.38 %R C# 85.0 01 D:\VIET - K25\14042017-23 - diem chuan 9966.aa Page 10 ... (ppb) 0. 020 0.010 0.000 0.000 2. 500 5.000 Conc(ppb) 7. 500 2. 0000 0.0100 3.0000 0.01 37 4.0000 0.0 174 5.0000 0. 021 8 7. 0000 0. 026 7 0 .20 00 0.0035 1.0000 0.0059 Abs=0.0035449Conc+0.0 029 006 r=0 .9966 :... 4/14 /20 17 11: 52: 51 AM(+ 070 0) System Administrator AA : STD Average True Value Conc Abs 4.0903 0.0 174 R3 R4 TotalVolume SD BG 0.0 028 Pos VOL R1 R2 4.0000 520 0 %RSD 20 0.0006 3 .25 %R C# 1 02. 2 01... Device Name 4/14 /20 17 12: 01:53 PM(+ 070 0) System Administrator AA : STD Average True Value Conc Abs 6 .71 38 0. 026 7 R3 R4 TotalVolume SD BG 0.0034 Pos VOL R1 R2 7. 0000 72 0 0 %RSD 20 0.0014 5.30 %R