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S T D = A P I / P E T R O PUBL 310-ENGL 1997 `,,-`-`,,`,,`,`,,` - Health and Environmental Affairs Department Publication Number 310 November 1997 Copyright American Petroleum Institute Provided by IHS under license with API No reproduction or networking permitted without license from IHS Not for Resale m 0332290 ObO4bb3 ?SO m ~ S T D - A P I / P E T R O P U B L 310-ENGL 1997 H 0732270 ObOqbbll b77 ?- American Petroleum Institute American Petroleum Institute Environmental, Health, and Safety Mission and Guiding Principles MISSION PRINCIPLES The members of the American Petroleum Institute are dedicated to continuous efforts to improve the compatibility of our operations with the environment while economically developing energy resources and supplying high quality products ana' services to consumers We recognize our responsibility to work with the public, the government, and others to develop and to use natural resources in an environmentally sound manner while protecting the health and safety of our employees ana' the public To meet these responsibilities, API members pledge to manage our businesses according to the following principles using sound science to prioritize risks and to implement cost-effective management practices: o To recognize and to respond to community concerns about our raw materials, products and operations o To operate our plants and facilities, and to handle our raw materials and products in a manner that protects the environment, and the safety and health of our employees and the public To advise promptly, appropriate officials, employees, customers and the public of information on significant industry-related safety, health and environmental hazards, and to recommend protective measures To counsel customers, transporters and others in the safe use, transportation and disposal of our raw materials, products and waste materials To economically develop and produce natural resources and to conserve those resources by using energy efficiently To extend knowledge by conducting or supporting research on the safety, health and environmental effects of our raw materials, products, processes and waste materials To commit to reduce overall emission and waste generation To work with others to resolve problems created by handling and disposal of hazardous substances from our operations To participate with government and others in creating responsible laws, regulations and standards to safeguard the community, workplace and environment o Copyright American Petroleum Institute Provided by IHS under license with API No reproduction or networking permitted without license from IHS To promote these principles and practices by sharing experiences and offering assistance to others who produce, handle, use, transport or dispose of similar raw materials, petroleum products and wastes Not for Resale `,,-`-`,,`,,`,`,,` - To make safety, health and environmental considerations a priority in our planning, and our development of new products and processes ~ ~ S T D * A P I / P E T R O PUBL 310-ENGL 1997 0732290 0604665 523 `,,-`-`,,`,,`,`,,` - Analysis of Refinery Screening Data Health and Environmental Affairs Department API PUBLICATION NUMBER 31O PREPARED UNDER CONTRACT BY: HALTABACK COMPANY 378 PASEOSONRISA WALNUT,CALIFORNIA 91789 NOVEMBER 1997 American Petroleum Institute Copyright American Petroleum Institute Provided by IHS under license with API No reproduction or networking permitted without license from IHS Not for Resale m ~ STD.API/PETRO ~~ PUBL - E N G L 1997 0732290 O b O Y b b b Y b T D FOREWORD API PUBLICATIONS NECESSARILY ADDRESS PROBLEMS OF A GENERAL NATURE WITH RESPECT TO PARTICULAR CIRCUMSTANCES, LOCAL, STATE, AND FEDERAL LAWS AND REGULATIONS SHOULD BE REVIEWED API IS NOT UNDERTAKING TO MEET THE DUTIES OF EMPLOYERS, MANUFACTURERS, OR SUPPLIERS TO WARN AND PROPERLY TRAIN AND EQUIP THEIR EMPLOYEES, AND OTHERS EXPOSED, CONCERNING HEALTH AND SAFETY RISKS AND PRECAUTIONS, NOR UNDERTAKING THEIR OBLIGATIONS UNDER LOCAL, STATE, OR FEDERAL LAWS `,,-`-`,,`,,`,`,,` - NOTHING CONTAINED IN ANY API PUBLICATION IS TO BE CONSTRUED AS GRANTING ANY RIGHT, BY IMPLICATION OR OTHERWISE, FOR THE MANUFACTURE, SALE, OR USE OF ANY METHOD, APPARATUS, OR PRODUCT COVERED BY LETTERS PATENT NEITHER SHOULD ANYTHING CONTAINED IN THE PUBLICATION BE CONSTRUED AS INSURING ANYONE AGAINST LIABILITY FOR INFRINGEMENT OF LETïERS PAENT All rights reserved No part of this work m y be reproduced, stored in a retrieval system, or transmitted by any means, electronic, mechanical, photocopying, recording, or otherwise, without prior written permission from the publisher Contact the publisher, API Publishing Services, 1220 L Street, N.W., Washington, D.C 20005 Copyright O 1997 American Petroleum Institute iii Copyright American Petroleum Institute Provided by IHS under license with API No reproduction or networking permitted without license from IHS Not for Resale ~ STD.API/PETRO PUBL 310-ENGL -~ 1997 m 0732290 Ob04bb7 3Tb ACKNOWLEDGMENTS THE FOLLOWING PEOPLE ARE RECOGNIZED FOR THEIR CONTRIBUTIONS OF TIME AND EXPERTISE DURING THIS STUDY AND IN THE PREPARATION OF THIS REPORT: API STAFF CONTACT Karin Ritter, Health and Environmental Affairs Department STATIONARY SOURCE EMISSIONS RESEARCH íSSER) WORKGROUP FUGITIVE EMISSIONS OVERSIGHT (FEO) COMMIïTEE Lee Gilmer, SSER Chairperson, Exxon Jeff Siegell, FEO Chairperson, Texaco Miriam Lev-On, ARCO Dan VanDerZanden, Chevron HAL TABACK COMPANY Kelvin Lu, Computer Analyst H.J Taback, PE, DEE, QEP, REA, Principal Investigator and Project Manager `,,-`-`,,`,,`,`,,` - Copyright American Petroleum Institute Provided by IHS under license with API No reproduction or networking permitted without license from IHS Not for Resale m ABSTRACT This report presents the findings and recommendations of a study of fugitive emissions from piping components (valves, flanges, etc.) at seven Los Angeles California refineries over a period of five and one-half years These screening measurements, taken to determine the estimated fugitive emissions of volatile organic compounds (VOC) from those refineries, were collected and analyzed These screening measurements comprise the detection portion of a leak detection and repair (LDAR) program designed to reduce fugitive emissions from components in process unit piping The study was conducted to determine whether a more cost effective LDAR protocol could be developed The study was expected to clarify the cause(s) of leaks by identifying the repeat leakers and high-rate leakers and by investigating the design and operational characteristics of those leaking components High leakers (components screening 210,000 ppmv) were found to occur randomly and repeat leakers (components screening > 1,000 ppmv more than once within a year) were negligible This finding indicates that there is not an easily identifiable cohort of leakers within the population of refinery components subject to LDAR Overall, only O 13 percent of the components were high leakers, but they accounted for 92 percent of the reducible VOC emissions Based on the current findings, a leak detection protocol that would concentrate on locating high rate leakers may be more cost effective than the current practice of `,,-`-`,,`,,`,`,,` - monitoring all components Copyright American Petroleum Institute Provided by IHS under license with API No reproduction or networking permitted without license from IHS Not for Resale ~~ S T D m A P I l P E T R O PUBL 310-ENGL 1797 m 0732290 0604667 179 m TABLE OF CONTENTS Pap;e Section EXECUTIVE SUMMARY S-1 INTRODUCTION 1.1 BACKGROUND I- OBJECTIVE 1-2 APPROACH 1-2 REPORT ORGANIZATION 1-3 2- 2- ACQUISITION PROCESSING 2-3 DATA ANALYSIS 3-1 HIGH AND REPEAT LEAKERS 3- DISTRIBUTION OF EMISSIONS BY SCREENING RANGES 3- 11 DISTRIBUTION OF EMISSIONS BY COMPONENT CATEGORY 3-1 3- 13 PROCESS UNIT VARIATIONS REFINERY-TO-REFINERY VARIATIONS 3.22 GREATER LEAK TENDENCY OF COMPONENTS IN LPG STREAMS 3-28 RECOMMENDATION FOR COST EFFECTIVE LDAR 4-1 REFERENCES 5-1 DATA FROM THE LOS ANGELES REFQERES APPENDIX A A- `,,-`-`,,`,,`,`,,` - MATRIX TABLE OF RESULTS Copyright American Petroleum Institute Provided by IHS under license with API No reproduction or networking permitted without license from IHS Not for Resale `,,-`-`,,`,,`,`,,` - LIST OF FIGURES Pane Figure 3- Average Per Component Emissions for High Leakers, Repeat Leakers and Total Components for Aggregate of All Components and Services 3-4 3-2 Average Per Component Emissions for High Leakers, Repeat Leakers and Total Components for Valves in Light Liquid Service 3-4 3-3 Average Per Component Emissions for High Leakers, Repeat Leakers and Total Components for Valves in Gas Service 3-5 3-4 Average Per Component Emissions for High Leakers, Repeat Leakers and Total Components for Pumps in Light Liquid Service 3-5 3-5 Average Per Component Emissions for High Leakers, Repeat Leakers and Total Components for Connectors in Light Liquid Service 3-6 3-6 Average Per Component Emissions for High Leakers, Repeat Leakers and Total Components for Connectors in Gas Service 3-6 3-7 Percentage of Total Emissions for High Leakers, Repeat Leakers, and Other Leakers .3-8 for Aggregate of All Components and Services 3-8 Percentage of Total Emissions for High Leakers, Repeat Leakers, and Other Leakers .3-9 for Valves in Light Liquid Service 3-9 Percentage of Total Emissions for High Leakers, Repeat Leakers, and Other Leakers .3-9 for Valves in Gas Service 3-10 Percentage of Total Emissions for High Leakers, Repeat Leakers, and Other Leakers 3-10 for Pumps in Light Liquid Service 3-1 Percentage of Total Emissions for High Leakers, Repeat Leakers, and Other Leakers 3-10 for Connectors in Light Liquid Service 3-12 Percentage of Total Emissions for High Leakers, Repeat Leakers, and Other Leakers 3-1 for Connectors in Gas Service 3- 13 Distribution of Component Count and Estimated Emissions by Screening Range 3- 12 Average of All Component Types, Service Types for 5.5 Years 3-14 Percentage of Total Emissions for High Leakers and Repeat Leakers in Refinery Processes for Aggregate of All Components and Services 3-15 3-15 Percentage of Total Emissions for High Leakers and Repeat Leakers in Refinery Processes for Valves in Light Liquid Service 3-16 Copyright American Petroleum Institute Provided by IHS under license with API No reproduction or networking permitted without license from IHS Not for Resale LIST OF FIGURES (Continued) Page Fimire 3-16 Percentage of Total Emissions for High Leakers and Repeat Leakers in Refinery Processes for Valves in Gas Service 3-16 3-17 Percentage of Total Emissions for High Leakers and Repeat Leakers in Refinery Processes for Pumps in Light Liquid Service 3-17 3- 18 Percentage of Total Emissions for High Leakers and Repeat Leakers in Refinery Processes for Connectors in Light Liquid Service 3- 17 3-19 Percentage of Total Emissions for High Leakers and Repeat Leakers in Refinery Processes for Connectors in Gas Service 3- 18 3-20 Percentage of Total Components for High Leakers and Repeat Leakers in Refinery Processes for Aggregate of All Components and Services 3-19 3-21 Percentage of Total Components for High Leakers and Repeat Leakers in Refinery Processes for Valves in Light Liquid Service 3-19 3-22 Percentage of Total Components for High Leakers and Repeat Leakers in Refinery Processes for Valves in Gas Service 3-20 3-23 Percentage of Total Components for High Leakers and Repeat Leakers in Refinery Processes for Pumps in Light Liquid Service 3-20 3-24 Percentage of Total Components for High Leakers and Repeat Leakers in Refinery Processes for Connectors in Light Liquid Service 3-21 3-25 Percentage of Total Components for High Leakers and Repeat Leakers in Refinery Processes for Connectors in Gas Service 3-21 3-26 Emission Factors by Processes for Aggregate of All Components and Services 3-22 3-27 Aggregated Quarterly Emissions from High Leakers, Repeat Leakers and Total Components for Refinery A 3-23 3-28 Aggregated Quarterly Emissions from High Leakers, Repeat Leakers and Total Components for Refinery B 3-24 3-29 Aggregated Quarterly Emissions from High Leakers, Repeat Leakers and Total Components for Refinery C 3-24 3-30 Aggregated Quarterly Emissions from High Leakers, Repeat Leakers and Total Components for Refinery D 3-25 3-3 Aggregated Quarterly Emissions from High Leakers, Repeat Leakers and Total Components for Refinery E 3-25 `,,-`-`,,`,,`,`,,` - Copyright American Petroleum Institute Provided by IHS under license with API No reproduction or networking permitted without license from IHS Not for Resale LIST OF FIGURES (Continued) Figure Page 3.32 Aggregated Quarterly Emissions from High Leakers Repeat Leakers and Total Components for Refinery F 3-26 3.33 Aggregated Quarterly Emissions from High Leakers, Repeat Leakers and Total Components for Refinery G 3-26 3.34 Refinery by Refinery Comparison of Average Emissions of High Leakers Repeat 3-27 Leakers and Total Components for Aggregate of All Components and Services 3.35 Refinery by Refinery Comparison of Percentage of Components That Are High Leakers 3-27 Repeat Leakers and Other Components for Aggregate of All Components and Services LIST OF TABLES Pap;e Table 2.1 Summary of the Screening Data Collection Effort 2-2 3.1 Screening Results for Seven Refineries (5.5 years) 3-2 3.2 Valve and Connector Emissions Distribution 3-7 3.3 Distribution of Emissions by Component Category 3-13 3.4 Process Unit Description 3-13 3.5 Contribution to Total Emissions by Process Unit High and Repeat Leakers 3-15 3.6 Comparison of Various Refinery Performance; Average Emissions, lbhr-component 3-23 3.7 Proportion of High Leakers in Low Pressure Gas Line Components for Refinery A 3-28 Combined Matrix for Leakers with Value >= 500 A-2 A.2 Combined Matrix for Leakers with Value >= 1,O00 A-4 A.3 Combined Matrix for Leakers with Value >= 10,O00 A-6 A.4 Combined Matrix for Leakers with Value >= 50,O00 A-8 Combined Matrix for Leakers with Value >= 100,O00 A-10 A.1 `,,-`-`,,`,,`,`,,` - A.5 Copyright American Petroleum Institute Provided by IHS under license with API No reproduction or networking permitted without license from IHS Not for Resale GREATER LEAK TENDENCY OF COMPONENTS IN LPG STREAMS In investigating the individual refinery data, it was found that one refinery had reported its stream identifications For that refinery, as shown in Table 3-7, it was found that 57 percent of the high leakers, 68 percent of the two-time high leakers (screening 10,000ppmv) and 81 percent of the three and four times high leakers were located on specific process streams, those categorized as liquefied petroleum gas (LPG) or fuel gas streams For the leakers over 50,000 ppmv, the LPG lines account for 62 percent While this tendency of the LPG sections of a refinery to have disproportionately large number of high leakers was observed, it was not possible to check for these tendencies in other refineries -4 Table 3-7 Proportion of High Leakers in Low Pressure Gas Line Components for Refinery A rn Components Screening at Level Shown + L -> 10,Ooo > 10,000 ppmv- 3X >10,000 > 100,000 ppmv- 2X ppmv 4X PPmv No % No % No 9% No % No % No % 1319 1O0 264 1O0 64 1O0 16 100 245 100 20 1O0 Butane 280 21.2 78 29.6 29 45.3 50.0 57 23.3 45 22.4 Propane 104 7.9 29 11.0 10.9 18.8 24 9.8 22 10.9 LPG 96 7.3 24 9.1 6.3 O 0.0 23 9.4 19 9.5 Fuel Gas/ Nat’l Gas 161 12.2 27 10.2 9.4 6.3 31 12.7 25 12.4 Product in Stream Total - All Products `,,-`-`,,`,,`,`,,` - Hydrogen -106 8.0 22 8.3 9.4 6.3 19 7.8 14 7.0 56.6 180 68.2 52 81.3 13 81.3 154 62.9 125 62.2 p_ Total LPG 747 3-28 Copyright American Petroleum Institute Provided by IHS under license with API No reproduction or networking permitted without license from IHS Not for Resale STD.API/PETRO PUBL 310-ENGL 1997 0732290 Ob04711 233 Section RECOMMENDATZONFOR COST EFFECTIVE LDAR Currently, LDAR programs involve screening all components and repairing and re-screening of leaking components These programs involve extensive screening inspections of non-leaking components From the preceding data presentation, high leakers (screening >10,000 ppmv) account for 92 percent of the controllable emissions from the Los Angeles refineries included in the study Furthermore, of that 92 percent, 83 percent of the emissions are from the pegged sources (i.e., components screening > 100,000 ppmv) Clearly, a more cost effective LDAR program would be one that does not require the monitoring of all components, but one that finds and repairs the high leakers The perception is that the current program wastes at least 98 percent of its effort monitoring non-leakers 4-1 `,,-`-`,,`,,`,`,,` - Copyright American Petroleum Institute Provided by IHS under license with API No reproduction or networking permitted without license from IHS Not for Resale Section REFERENCES CMA, 1989 Improving Air Quality: Guidance for Estimating Fugitive Emissionsfrom Equipment, Chemical Manufacturers Association, Washington, D.C Radian Corp., 1980, Assessment of Atmospheric Emissions from Petroleum Refining, Vol I, Technical Report, Environmental Protection Agency Report EPA-600/2-80-075a, Research Triangle Park, NC 5- `,,-`-`,,`,,`,`,,` - Copyright American Petroleum Institute Provided by IHS under license with API No reproduction or networking permitted without license from IHS Not for Resale S T D - A P I / P E T R O PUBL 310-ENGL 1997 0732290 Ob04713 OOb m Appendix A MATRIX TABLE OF RESULTS The following tables are intended for those interested in the exact numbers used during the study There are five sets of tables Each table is a summary of the information for a specific leak definition The first table is at 500 ppmv, the second at 1,000 ppmv, and so on, as indicated by the title Each table is divided into two pages due to the large amount of information The first page of the table is for the first quarter of 1991 through the fourth quarter of 1993 The second page of the table is for the first quarter of 1994 through the second quarter of 1996 The quarters are listed at the top of each table (the last two numbers of the year, a dash, and the quarter) For example, 91-1 means the first quarter of 1991 Each table is divided into five sections, one section for each component type Each row is labeled as to the information it holds and each column is the number for that quarter of the year The first column, however, is the aggregated total for all the quarters This number is repeated on the second page of the table as well so that it can be referenced without having to look back to the first page Here is an explanation of each of the row headings - Total Components The count of the total number of components screened Total Leakers - The number of components having a screening value at or above the level set in the title Leaked or More - The number of components that were found to be leaking at least twice within the past four quarters This represents the number of repeat leakers % of Leakers - The percentage of repeat leakers from total leakers 9% of Total Comp - The percentage of repeat leakers out of the total components The last three rows repeat but with components that leaked at least three times and with four times Then the entire section of rows is repeated for the next component type A- `,,-`-`,,`,,`,`,,` - Copyright American Petroleum Institute Provided by IHS under license with API No reproduction or networking permitted without license from IHS Not for Resale ~~ ~~ STD.API/PETRO m 0732290 0604734 P U B L 310-ENGL 1997 T42 m Table A-1 Combined Matrix for Leakers with Values >= 500 9L2 %I 9w 924 931 93-3 932 m 130269 177i89 179582 185107 189235 231 361 392 378 266 13 15 24 29 5.628% 24B% m o 6.349% 1O.%Q% 0.010% 0.005% W o 0.013% O.Ol5% 1 1 m 0.277% ~ % am% 0.752% 0.001% 0.001% 0.001% 0.001% 0.001% O O O O m m o 0.433% O.ClKF% 0.O.oo(y% O.CO% a m o.wo0.001% m o m o o m o o m o 128462 128506 128815 181 280 236 16 1.105% 285% 6.78(ylb 0.OUXo 0.006% 0.012% O O o.mo0 m 0.424% m o m o 0.001% O O O 0.mo o.mo Led= 500 (continued) Total Total M e r s Leaked20rMore % of M e r s %ofTotalComp Leaked orMore %ofMers %ofTotalComp Leaked4Times % of ieakers %ofTotalComp Fitting Liauid Total Components Total M e r s Leaked or More % of M e r s %ofTotalComp Leaked3orMore %ofMers %ofTotalComp Leaked4Tinies % of M e r s of Total C o q P u m p Liquid Total Components Total M e r s Leaked or More % of M e r s % of Total Comp Leaked or More % of M e r s % of Total Comp Leaked Times % of Leakers - I 94-1 I I 94-2 4657771 I 207828 212462 12330 364 424 1281 24 26 10.389% 6.593% 6.132% I 0.028% 0.012% 0.012% I 210 I O I 1.703% I 0.824% 0.000% 0.005% 0.001% 0.000% 40 I I O 0.324% 0.275% 0.000% 0.001% 0.000% 0.000% I I I 94-3 94-4 %-I 95-2 95-3 `,,-`-`,,`,,`,`,,` - 95-4 96.1 362524 1101 159 14.441% 0.044% 30 2.725% 0.008% 0.817% 0.002% 367645 977 178 18.219% 0.048% 30 3.071% 0.008% 0.307% 0.001% 379201 1121 187 16.682% 0.049% 37 3.301% 0.010% 0.268% 0.001% 351719 390172 488 686 65 95 13.320% 13.848% 0.018% 0.024% 13 I 12 2.664% I 1.749% 0.004% 0.003% 10 1.585% 0.820% 0.292% 0.003% 0.001% 0.001% 406744 749 I37 18.291% 0.034% 30 4.005% 0.007% 300659 302539 275600 800 771 769 39 81 106 4.875% 10.506% 13.784% 0.013% 0.027% 0.038% 18 0.750% 1.167% 2.341% 0.002% 0.003% 0.007% O O.OOO% 0.389% 0.260% 0.000% 0.001% 0.001% 14.067% 0.064% 36 2.752% 0.013% 0.612% 0.003% 278592 284082 404 411 56 58 13.861% 14.112% 0.020% 0.020% 12 0.743% I 2.920% 0.001% 0.004% O 0.000% 0.000% 0.000% 0.000% 288115 582 95 16.323% 0.033% 27 4.639% 0.009% 1.203% 0.002% 354230 631 95 15.055% 0.027% 25 3.962% 0.007% 2188 2160 2177 77 77 100 29 27 30 37.662% 35.065% 30.W% 1.325% 1.250% 1.378% 10 6.494% 12.987% 7.000% 0.229% 0.463% 0.322% 3.896% 2.000% 0.139% 0.092% 3791 105 23 21.905% 0.607% 11 10.476% 0.290% 3.810% 0.106% 2.353% 0.054% 101227 860 204 23.721% 0.202% 34 3.953% 0.034% 0.233% 0.002% 106169 1018 263 25.835% 0.248% 54 5.305% 0.051% 0.589% 0.006% 103955 1175 253 21.532% 0.243% 53 4.511% 0.051% 0.681% 0.008% 101357 996 241 24.197% 0.238% 55 5.522% 0.054% 105120 102263 934 732 236 187 25.268% 25.546% 0.225% 0.183% 37 41 3.961% 5.601% 0.035% 0.040% 0.321% 0.273% 0.000% 0.003% 0.002% 780638 799109 765332 104926 910 255 28.022% 0.243% 62 6.813% 0.059% 287896 1308 184 347880 1232 158 12.825% 0.045% 31 2.516% 0.009% 10 0.812% 0.003% %-2 I I I I I - 4310233 7547 890 I 793% 0.021% 168 2.226% 0.004% 34 0.451% 0.001% 170644 209 12 5.742% 0.007% I I 1.435% I 0.002% I O 0.000% O.OOO% 178590 184 13 7.065% 0.007% O 0.000% 267999 417 26 6.235% 0.010% 0.480% 0.001% O 0.000% 0.000% 34431 1102 303 27.495% 0.880% 83 7.532% 0.241% 16 1271 41 10 24.390% 0.787% I 2.439% 0.079% O 1289 56 17 30.357% 1.319% 5.357% 0.233% O 2061 94 21 22.340% 1.019% 6.383% 0.291% O O.OOO% 0.000% O 0.000% I I - I I 3686 85 31 36.471% 0.841% 4.706% 0.109% 0.668% 0.001% 3653 82 28 34.146% 0.766% 10 12.195% 0.274% 3994 83 32 38.554% 0.801% 11 13.253% 0.2759 o 0.000% 4.819% 0.000% 0.100% Valve Gas Totl M e r s Leaked or More % of M e r s % of Total Comp Leaked orMore %ofMers %ofTotalComp Leaked4Times % of M e r s % of Total Comp Valve Liquid Totl Comp&ents Total M e r s Leaked or More % of M e r s % of Total Comp Leaked or More % of M e r s % of Total Comp Leaked4Tms % of Leakers % of Total Comp Total Components I I I I - I I 0.168% 511 3.536% 0.034% 81 0.560% 0.005% I 0.127% 18 I 3.321% I I I 0.131% 22 3.379% 0.026% 0.032% 0.369% 1.075% 0.003% 0.010% 60176 60910 1364399 13817 451 482 66 2567 90 i 8.579% 14.634% 18.672% 0.188% 0.110% 0.148% 10 12 596 4.314% 2.217% 2.490% 0.044% 0.017% 0.020% 94 I O O 0.680% O.OOO% 0.000% 0.007% 0.000% 0.000% 11861137 508187 522007 I 0.135% 23 2.277% 0.021% 0.198% 0.002% 0.198% 37 3.544% 0.033% 0.575% 0.005% 101800 917 130 14.177% 0.128% 23 2.508% 0.023% O 0.000% I A-3 Copyright American Petroleum Institute Provided by IHS under license with API No reproduction or networking permitted without license from IHS Not for Resale 97831 905 222 24.530% 0.227% 69 7.624% 0.071% 10 15 1.099% 1.657% 0.010% 0.015% 789283 907687 102736 113913 768 822 232 276 30.208% 33.5774 0.226% 0.242% 52 92 6.771% 11.1924 0.051% 0.081% 10 15 18 1.004% 1.953% 2.190% 0.010% 0.015% 0.016% 101419 93627 716 585 186 165 25.978% 28.205% 0.199% 0.163% 52 46 7.263% 7.863% 0.056% 0.045% 15 I 14 2.095% 2.393% 0.016% 0.014% 912913 965625 I 102999 653 200 30.628% 0.194% 68 10.413% 0.066% 12 1.838% 0.012% 1006851 - S T D m A P I I P E T R O P U B L 310-ENGL 1997 Gas Tdanpc*iars TdIJ2k3 Lz3kd2cak %ofLedairs 'IbbJ 91-1 91-2 91-3 4657771 m 1014 9.457% 86316 164 95679 88992 315 294 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 114068 139 113ZíJ3 374 112949 410 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 374 12 417 IO 461 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA N'A NA NA NA NA 27036 389 34û!4 32225 31231 633 NA NA NA NA NA NA NA NA NA 632 305 NA NA NA NA NA NA NA NA N'A 58 19.016% 0.984% 0.01W 57576 57% 297 3w 461 32 54 25 52 51 W o 9.581% 14.173% 17.172% 6345% ll.Bl% 0.013% O.M% 0.143% 0.1% 0.043% W o O O m 0.MJB'o 1.05046 3.Wo 1.015% 1.3U2% 0.0ûXo O.tKû% 0.011% O.Cû4% O.W% 0.010% O O O O o.o.mo a m 0.000% m 0.217% O.ooo% 0.003% m W o O.ooo% O.aazol, 33199 31624 Bi45 %ofTddcarp LPakd3cake %ofIJ2k3 %OfTdcarp W T m o.ozz% %ofLeduas 0.270% %ofTdalCaip Fittiqg-Iiqlid T~talanpc*iars TdLeduas LedPrlZorke %of%ofTdcarp W m k %ofLeduas %ofTdCarp W T m %of- 144 1.343% 0.003% 29 0.001% 4310233 6174 653 10.577% 0.015% 114 1.846% 0.003% 23 0.373% ~ o f ~ d l c c n p 0.001% R n p w 34431 Tdcarpaiats 861 TdIJ2k3 an LPakd2CrMm %ofLeduas 24.042% %OfTdcarp 0.601% Lz3kd3orke 45 %ofLeduas 5.226% %OfTdalcarp W T m %ofldœrS %ofTdCOnp Vahp-Ges Tdalanpc*iars TdIJ2k3 LPakd2ork %of%ofTdChp W m k 0.131% 12 1.394% %ofLeduas %OfTdcarp Lz3kd4Tnres %of%ofTdcaip Valve-Iipid Td& TaalLeduas Leiked2ork O.U35% 14943û3 irni 192 15.411% 0.131% 362 2843% 0.024% 48 om% 0.003% 11472 34781 415 177 NA 1364399 15.4% NA % o f T d G n p I 0.130% NA I e d a d ~ M ~I ~ 349 I N A %didm I 3.042% I N A S o f T d C i n p I 0.026% I N A 45 I N A LPakd4Tnres I NA %Ofkalaxs 0.392% %ofTaaiChp 0.003% NA 11861137 262575 Tdcanponats %of- I NA NA NA NA NA NA NA NA NA I `,,-`-`,,`,,`,`,,` - Copyright American Petroleum Institute Provided by IHS under license with API No reproduction or networking permitted without license from IHS 32115 963 NA NA NA NA NA NA NA NA NA n m 23 1119 NA NA NA NA NA NA NA NA NA x7826 914 0732290 Ob0471b 815 921 9L2 x 924 9%1 9%2 m3 ?H 128462 1285oá 128815 13(1269 161 259 333 219 n) 14 i2 11.696% 0.621% 2703% 6.897% m 0.021% 0.001% m 0.01011% m O O O O 1.754% O.ooo% 0.0% W o W o 0.0(13% m m o W O.ooo% O O O O O m O.ooo% W m O.ooo% 0.ûJMo W o W o 0.CûYo O.ooo% 179582 185707 1851235 352 379 3ỵ3 240 2557% 3.95% 7.4Wo 10.833% 0.0~6% o a m 0.013% 0.014% 1 0.284% 0.264% 0.310% 0.833% 0.001% 0.001% 0.001% 0.01% o O O O.CW% 0.096 0.31Wo O.ooo% m O.ooo96 0.001% O.aïF% 112%8 122 16 13.115% 0.014% 2459% 130828 122 O 94185 171 81147 85416 82158 844130 146 261 155 137 12 34 21 31 8.219% 12734% 13548% 22628% 0.015% 0.040% W O.W% 0.685% 1.124% 2581% 1.460% 0.003% 0.001% 0.004% 0.005% W O O O O O 0.000% o.mo0 m m o.mo 0.000% m m m o m 410 5O.aKl% 0.244% O O.ooo% 0.mo O O.oO(w0 m 0.186% 11 3.607% 0.035% 604 # 3 4 33.333% 17.391% 17.391% 28.ooo% W o W o 0.652% 1.153% O W 4.348% 8.696% 4.O00% O.ooo% 0.16% 0.331% 0.165% O O O O O.OK% O.oM)% W W W o W o O.OW5 W o 604 37455 341 606 37515 334 371% A-4 Not for Resale 134987 141000 14á482 142 112 115 15 14 û W o 3.521% 13.393% 12174% W o 0.004% 0.011% 0,OIWo O O O.ooo96 0.7040/0 O.ooo96 3.478% W o 0.0011 O.ooo% 0.0034 O O O O a m 0.096 m o.^ amo 0.096 o.- o.mo 1010 1010 1057 101 19 14 3 3.846% 10.345% 15.7m 21.4% 0.09% 0.297% 0.284% 0.30370 O O O O.ooD% m o 5.263% W O.aC% W o 0.095% 0.096 O O O O m O.ooo% 0.096 O.ooo% O.OC@% W O.OW% O.oo1wO 37# 381 23616 27956 23811 2% 363 342 27.4 58 32 51 64 83 n).423% 10.811% 14.@&?1 18.713% 30.292% 0.18396 0.135% 0.215% 0.264 0.348% 14 15 m l 23ú% 1.102% 2339% 5.474% 0.044% W o 0.017% 0.033% O.W% O 1 O.ooo% 1.014% 0.551% 0.292% O.%% O.W% 0.013% 0.008% 0.004% 0.004% 270018 271313 27>m n m nam 284 177789 61249 57949 4û2 516 58 64 11.240% 15.920% 0.095% 0.110% 10 1.163% 2488% 0.0iWo 0.017% o.=% 1.741% 0.003% 0.012% M807 54166 50760 347 342 331 339 16 57 54 64 4.611% 16.67% 16.314% m 50)28 O.U32% 0.112% 0.100% O W % 17 1.7'29% 0.877% 2115% 5.015% 0.012% W o 0.013% O.û33% 1 O O O.%% 0.232% W O.OK% O.m%0.002% m O.ooo96 417931 423932 443179 445427 Table A-2 Combined Matrix for Leakers with Values >= 1,000 (continued) - `,,-`-`,,`,,`,`,,` - Fitting Gas TotalComponents Total M e r s W e d or More % of M e r s % of Total C o q Leaked or More % of M e r s %ofTotalComp Leakeed4Tms % of M e r s %ofTotalComp Fitting Liquid Total Compokmts Total M e r s Leaked or More % of M e r s % of Total Co Leaked or More % of M e r s %ofTotalComp Leaked4Times % of M e r s %ofTotalComp P u m p Liquid Total Components Total M e r s Leaked or More % of M e r s % of Total COW Leaked3orMore %ofMers %ofTotalComp Leaked4Tms % of Leakers %ofTotalComp Valve Gas Total Components Total Leakers Leaked or More % of Lealcers % of Total C o q Leaked or More % of M e r s 70of Total Comp Leaked4Times % of Leakers % of Total Comp Valve Liquid Total Components Total M e r s Leaked or More % of M e r s % of Total C o q Leaked or More % of M e r s % of Total Comp Leaked Times % of M e r s % ofTotal Comp I I - I I - I I I I I - I I Total 94-1 94-2 94-3 4657771 10722 1014 9.457% 0.022% 144 1.343% 0.003% 29 0.270% 0.001% 207828 338 19 5.621% 0.009% 0.296% O.ooO% O O.ooO% 0.000% 212462 397 22 5.542% 0.010% O 0.000% 0.000% 0.756% 0.001% 300659 707 29 4.102% 0.010% 0.849% 0.002% 0.283% 0.001% I I I 95-1 I 95-2 95-3 287896 1143 152 13.298% 0.053% 24 2.100% 0.008% 0.612% 0.002% 347880 1032 117 11.337% 0.034% 26 2.519% 0.007% 0.194% 0.001% 96-1 95-4 362524 367645 884 859 117 149 13.235% 17.346% 0.032% 0.041% 19 20 2.149% 2.328% 0.005% 0.005% 1 O 0.113% O.OOO% O.OOO% 0.000% I %-2 379201 943 131 13.892% I 0.035% 23 2.439% 0.006% O 0.0004 0.000% , 43 10233 6174 653 10.577% 0.015% 390172 406744 i 346% 1.257% 3.061% O 0.756% 0.000% 0.001% O.OOO% 0.000% 23 0.373% 0.001% I 3443 86 207 24.042% 0.601% 45 5.226% 0.131% 12 1.394% 0.035% 1271 1289 2061 32 46 83 12 15 21.875% 26.087% 18.072% 0.551% 0.931% 0.728% I 1 3.125% 2.174% 4.819% 0.079% 0.078% 0.194% I O O 0.000% 0.000% 2.410% 0.000% 0.000% 0.097% I I I 2188 2160 55 60 18 19 32.727% 31.667% 0.823% 0.880% 5.455% I10.000% 0.137% 0.278% 3.636% 5.000% 0.091% 0.139% 1494303 12731 1962 15.411% 0.131% 362 2.843% 0.024% 48 0.377% 0.003% 68268 481 72 14.969% 0.105% 15 3.119% 0.022% I 0.416% 0.003% 68756 585 65 11.111% 0.095% 19 3.248% 0.028% 0.855% 0.007% 108119 887 123 13.867% 0.114% 16 1.804% 0.015% 0.225% 0.002% 110670 908 172 18.943% 0.155% 29 3.194% 0.026% I 0.022% 0.220% 0.531% 0.002% 0.004% 0.039% 0.228% 0.002% 0.038% 0.509% 0.005% 0.038% 12 1.441% 0.012% 60176 382 52 13.613% 0.086% 2.094% 0.013% O 0.000% 0.000% 60910 438 73 16.667% 0.120% 1.826% 0.013% 0.457% 0.003% 101800 800 114 14.250% 0.112% 17 2.125% 0.017% 0.125% 0.001% 105120 806 181 22.457% 0.172% 26 3.226% 0.025% 0.744% 0.006% 104926 760 197 25.921% 0.188% 34 4.474% 0.032% 0.789% 0.006% 97831 723 155 21.438% 0.158% 47 6.501% 0.048% 1.107% 0.008% 93627 565 133 23.540% 0.142% 33 5.841% 0.035% 0.885% 0.005% O 0.000% O.OOO% I - - 94-4 302539 275600 660 679 63 87 9.545% 12.813% 0.021% 0.032% II 0.909% 1.620% 0.002% 0.004% 0.758% 1.178% 0.002% 0.003% 1364399 1472 1777 15.490% 0.130% 349 3.042% 0.026% 45 0.392% 0.003% I O O 0.000% O.ooO% 0.0006 0.000% 7 1.966% 1.977% 0.800% 0.003% 0.002% 0.001% I I 102263 604 136 22.517% 0.133% 27 4.470% 0.026% 1.325% 0.008% A-5 Copyright American Petroleum Institute Provided by IHS under license with API No reproduction or networking permitted without license from IHS Not for Resale 0.408% 0.001% 2177 3791 85 80 22 20 27.500% 23.529% 1.011% 0.528% 5.000% 8.235% 0.184% 0.185% O 2.500% 0.000% 0.092% 0.000% 3686 3653 71 63 22 18 30.986% 28.571% 0.597% 0.493% 5.634% I 7.937% 0.109% 0.137% O 4.225% 0.000% 0.081% 0.000% I I O 0.000% 3994 68 24 35.294% 0.601% 7.353% 0.125% O 0.000% O.OOO% I 0.031% I 0.053% O 0.000% 0.000% 0.000% 0.000% O 101419 102999 472 507 i4 143 24.153% 28.205% 0.112% 0.139% 25 43 5.297% 8.481% 0.025% 0.042% O O 0.000% 0.000% 0.000% 0.000% ~~ - = 0732290 Ob04718 ~~ ~~ STD-API/PETRO PUBL 310-ENGL 1997 698 Table A-3 Combined Matrix for Leakers with Values >= 10,ûûû 9%2 9tl 9.24 9L-J `,,-`-`,,`,,`,`,,` - 128462 128506 128815 1Xü@ l r n 17958L m if9235 TbalI2dKl.S 4210 a 6 O O 5.m 0.m 0.m O.CDRo 0.001% 0.0% m O O O O 0.m m a m m 0.mo 0.mo 3.333% 1.m% 3.008% 634% m 0.001% m O.W% O 0.000% m m m o m y".O O O O O m m m amo m m m m m m m m m o.O00% O."% I 431û23 2247 172 7.65% O.W% 40 1.780% 0.001% IO TdalCcsrp&s TdI2dKl.S LeAEXILorMXe %dTdOnp M3orhkxe %ofIakm %ofTuaiQip kabaì4Tnips 0.45% %ofprb~f~dcaip 0.000% NA NA NA NA 114068 113an NA NA NA NA NA NA NA NA NA 163 NA NA NA NA NA NA NA NA NA m NA NA 112949 193 NA NA NA NA NA NA NA NA NA 112568 81147 SI76 82158 a) 38 54 44 O 5.aXB 0.KWÓ 9.259% 6818% 0.001% m 0.005% O.W% O O O O O.C#% 0.OWh m W W o O.OK% W O.O00% O O O O 84480 3.750% m I 130828 53 36 O 19.444% O.oOo% 0.008% O.ooo96 O O 0.00W O.oo(r% O.ON& m O O 0.000%~ a m 0.000% a m 0.000%~ m o.wo m a m m 0.000% m o.y m 0.wo m 141000 146482 41 45 W o 24% 13.333% 0.001% 0.001% O.Oo1510 O O O.Mx)% O.oooLH, 222?% m W o 0.001% O O 0 m 0.000%~ m 0.m m m 1345%' 50 Rnp-Liqi*l 34431 310 TdCkqcmts Tdkakm w2orhkxe 39 12581% 0.113% %ofkakm %ofTdcmp Ledad3OrMXe BofI2dKl.S SofTdCarp kabaì4Ti %ofkakm aof~dcbnp Vahie-c;is Tdalh~pxuts TbalLedprs LeAEXI20rhbe %of- 2258% O.o1D% 0.968% o.mo I%I 3494303 %dTaalQip kakd4Tnips %ofLedairs %CfTdcaip Vahp-Iiqiid Td& %ofI2dKl.S %ofTdUnp NA NA NA NA NA NA NA NA NA DU36 A: 9.435% NA o w o NA 52 NA NA 1.261% 0.003% NA NA O.W% NA NA 0.- %OfTCdOnp Ledad3orhkxe %ofIakm TUdkk5 Le2kd2orMae 4bofI2dKl.S %ofTUdChp kakEd3aMXe 374 1364399 3872 316 8161% I I I I 0.0038 I I 0.023% I 4 1.1% 34781 84 NA NA NA NA NA NA NA 417 461 NA NA NA NA NA NA NA NA NA NA NA N'A NA NA NA NA NA NA 34íMS 167 NA NA NA NA NA NA NA NA NA 3ìE5 32115 424 NA NA NA NA NA NA NA 33199 563 238 NA NA NA NA NA NA NA NA N'A NA NA NA NA NA NA NA 606 604 607 I010 1010 1057 12 12 11 o o o 1 O O O W o O.oOo% 16.667% 8.333% O.ooo96 W 0.033% W o O.ooD% 0.Wo 0.16% 0.166% O.alû% 0.00% O.W% 0.Wo 410 O 604 O O O o O o o O.ooo% O.oM)% 0.O W % O.aû% m O.ûYl% O.al% m W o m 0.0Wi W m m O.ooo% O.ooo46 W O.O00% 0 o o O O O O O m O.oo[)% m O.ooo% O.ooo9b 0.0% O.oOo% 0.0% m o O.ooo% o.mo0 m a m m m 0.000% 0.00046 0.Wo 37455 37515 37% 78 87 88 3 1.282% 3.448% 3.40996 0.~~3% o.m%0 m O O m 1.1m m 0.000% am% m O O O O.ooo9b O.OK% m o O.oM9ro 0.0003ro o.COB 37W 57576 57% 61249 57919 81 141 158 233 142 ~ 10 13 4.938% 1.418% 6329% 6.m% 6338% 0.011% o.m% 0.017% ami% o.oia O O O 1 m a m m 0.4~~3%0.701% m m m a m m O O O O 0 m O.ooo96 O.ooo9b O.O00% 0.00% 0.046 m 0.00% m 0.- 31624 23645 23871 44 E5 0.000% 31231 53 5- aoim O 0.m 0.0005~ O O.ooo% 10 2727% 5.88246 O.U32% I O.al% I 11.364%1 1.176% 0.016%1 O.W% O I O A-6 Copyright American Petroleum Institute Provided by IHS under license with API No reproduction or networking permitted without license from IHS O 1001 Not for Resale 23676 23956 'i2 I ~ 50228 76 156 11.94(y36 4.167% 7.695% 1.282% 0.034% 0.013% 0.025561 O.W% O O O O.Kí% O.ooo46 O W % l m m O.ooo% W l O.û@% O O O 61 0.000% ~~ 54166 50760 129 111 120 15 10 IO 7.752% m m O.U20% 0.018% 0.033% O 0.03% 1.832% M807 O.C€C% O O.W% O.OC% O S T D - A P I / P E T R O PUBL - E N G L 1997 = 0732290 Ob04729 524 Table A-3 Combined Matrix for Leakers with Values >= 10,000 (continued) 94-1 Total Leakers Leaked or More % of M e r s % of Total Comp Leaked or More % of Leakers % of Total Comp Leaked Times % of M e r s % of Total Comp Fitting Liquid Total Components Total Leakers Leaked or More % of Leakers % of Total Comp Leaked or More % of Leakers % of Total Comp Leaked Times % of Leakers % of Total Comp P u m p Liquid Total Components Total Leakers Leaked or More % of Leakers % of Total Comp Leaked or More % of Leakers % of Total Comp Leaked Times % of M e r s % of Total Comp Valve Gas Total Components Total Leakers Leaked or More % of M e r s %ofTotalComp Leaked 3or More %ofLeakers %ofTotalComp Leaked4Times %ofMers %ofTotalComp Valve Liquid Total Components Total M e r s Leaked or More % of M e r s % of Total Co 4210 283 6.722% 0.006% 32 0.760% 0.001% 0.071% 0.000% - 4310233 2247 172 7.655% 0.004% 40 I 780% 0.001% - `,,-`-`,,`,,`,`,,` - - O O ).000% O.OOO1 ).O008 0.000% 94-4 95-1 95-2 95-3 95-4 302539 258 14 5.426% 0.005% O 0.000% 275600 296 24 8.108% 0.009% O 0.000% 0.000% O 0.000% 0.000% 287896 486 47 9.671% 0.016% 1.235% 0.002% O 347880 405 37 9.136% 0.011% 2.222% 0.003% 0.494% 0.001% 362524 381 37 9.711% 0.010% 1.837% 0.002% 0.262% 0.000% 354230 194 28 14.433% 0.008% 14 7.216% 0.004% 1.031% 0.001% 351719 O.OOO% O O 0.000% 0.000% O.OOO% O.OOO% O.OOO% 0.000% 0.445% 0.000% 178590 267999 61 154 1.639% 1.299% 0.001% 0.001% O O 0.000% O.OOO% ).000% 0.000% 0.000% O O O 1.000% 0.0008 0.000% 1.000% 0.000% 0.000% 278592 284082 288115 120 121 194 10 34 13 8.333% 10.744% 17.526% 0.004% 0.005% 0.012% O I 12 0.000% 0.826% 6.186% 0.000% 0.000% O.W% O O 0.000% 0.000% 0.515% 0.0002 0.000% 0.000% 34431 310 39 12.581% 0.113% 2.258% 0.020% 0.968% 0.009% 1271 1289 2061 17 23 34 5 5.882% 21.739% 14.706% 3.079% 0.388% 0.243% O O 0.000% 2.941% 3.000% 0.000% O.OOO% 0.049% O O O 0.000% 0.0004 0.0002 0.000% 0.000% 0.0008 2188 24 20.833% 0.229% O 0.000% 0.000% O 0.000% 0.000% 2160 2177 3791 23 25 29 21.739% 12.000% 13.793% 0.231% 0.138% 0.106% 4.348% 12.000% 3.448% 0.046% 0.138% 0.026% O 1 0.000% 4.000% 3.448% 0.000% 0.046% 0.026% 68268 171 16 9.357% 0.023% 1.170% 0.003% O 0.000% 110670 307 41 13.355% 0.037% 2.606% 0.007% O 0.000% 0.000% 101227 261 39 14.943% 0.039% 1.149% 0.003% 105120 255 39 15.294% 0.037% 1.176% 0.003% 1.176% 0.003% 799109 102263 184 28 15.217% 0.027% 1.630% 0.003% O 1494303 4123 389 9.435% 0.026% I 52 I 1.261% 0.003% I I I I 0.024% 0.000% ).000% O.OOO% ).000% 0.000% 94-3 300659 343 2.332% 0.003% 0.583% 0.001% 170644 76 !.632% ).O0116 O 1.000% 10 - 94-2 !O7828 212462 129 153 1.550% 3.922% ).001% 0.003% O O O.Ooo% 68756 224 21 9.375% 0.031% 1.786% 0.0061 O 0.000% 0.000% 108119 320 31 9.688% 0.029% 1.250% O.W% O 0.000% O.OOO% 106169 321 42 13.084% 0.040% 1.869% 0.006% O 0.383% 0.000% 0.001% 0.000% 140 12 8.571% 0.003% 4.286% 0.002% 2.143% 0.001% 351 50 14.245% 0.014% 1.140% 0.001% O 0.000% 0.000% 395 37 9.367% 0.010% 1.013% 0.001% O 0.000% O.OOO% 390172 406744 221 203 15 30 7.389% 13.575% 0.004% 0.007% 0.985% 1.810% 0.0021% "-21% I 3686 23 8.696% 11.111% 23.810% 0.054% 0.055% 0.125% 4.348% 0.000% 0.000% 0.027% 4.348% 0.000% 0.000% 0.027% 0.000% O.Ooo% 103955 311 39 12.540% 0.038% 2.251% 0.007% 101357 102736 113913 214 269 216 42 35 35 13.0119 16.204% 19.626% 0.035% 0.034% 0.037% 4 1.487% 1.852% 3.271% 0.004% 0.004% 0.006% O O o O 0.000% 0.000% 0.000% 0.000% O.Ooo% 0.000% 0.000% 0.000% I 1364399 3872 316 8.161% % of M e r s 1.136% % of M e r s 0.232% 60910 101800 60176 159 160 284 12 21 26 7.547% 13.125% 9.155% 0.020% 0.034% 0.026% O I 0.000% 0.625% 1.056% O.OOO% 0.002% 0.003% O O 0.000% 1.250% 0.000% 0.000% 0.003% 0.000% 508187 522007 780638 0.000% 0.000% 765332 A-7 Copyright American Petroleum Institute Provided by IHS under license with API No reproduction or networking permitted without license from IHS Not for Resale 104926 269 40 14.870% 0.038% 2.602% 0.007% 97831 212 31 14.623% 0.032% 3.302% 0.007% 0.372% 0.943% 0.001% 0.002% 789283 907687 93627 130 15 11.538: 0.0169 1.538% 0.0029 O 0.0004 0.0009 91291: 101419 139 14 10.072% 0.014% 2.878% 102999 149 21 14.098,% 0.02:)% 2.013% 0.004% 0.003% O O 0.000% 0.000% 0732290 ObOi.1720 246 S T D m A P I l P E T R O P U B L 3LO-ENGL 1997 9l-2 91-3 9ld 95679 91185 NA NA 88992 23 NA NA NA NA NA NA NA NA NA 114068 NA 113an 62 NA NA 112949 65 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 374 O 417 461 410 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA O O 604 O a m o.- o.mo 0.00% 0.03% 0.Wo O O I 91-1 I I TaalhkYl20rm 858 49 %ofLedais 5.711% %ofTaalcOnp 0.001% LeakKl3orlvbIe I %ofkakm I 0.932% NA I %ofIpdaa NA I 0.117% TccalLPdras liAPd2orm 89 5.618% 0.015% %ofLedais %ofTaalcarp O Ledax30rrvbIe %ofo.mo %OfTUaicaip O.ooo% O Leakjd4Tm %ofLdm O.ooo% %ofTaalCarp O.ooo% vahl?-Ges I I 14943(n Tdalcaipcriats TcralhkE7S 1563 116 Ledpxl2orhhe 7.422% SJofIpdaa CofTdCaip O.W% Lpdaxl3cfrvbIe I 15 I %of0 m I %ofTdaicOnp 0.001% Lpdaxl4Tnes I I I NA NA NA NA 340% 3ZZ2.5 48 53 NA NA NA %ofLpdars 0.128% 0.W 1364399 1379 34781 24 90 NA I I I NA NA NA 27û36 11 %OfTdalcaip I NA 9L2 9&3 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 931 924 9S2 933 18 13 17 O O O O 41 38 35 O O O W o W W o W 0.0.000% m O.ooo% O W % l O.ooo% W o O.W% 0.0û.Vo W W O.ooo% O I O O O O O O O I o.mo o.- W 0.03% 0.000% 0.000% 934 O.ooo% O.ooo% O O 29 3.448% 0.001% O o.mo0 m a m o.am o.- m QMX)% O.ooo% O.CW% W O O O O O O.KD% W 0.000% O.ooo% 0.03% O.MD% W o O.ooo% W O.Cû% W W B 0.0Wo W O.ooo% W 0.Wo O O 112568 81147 85476 11 O O O O.al% 0.W 0.W W l W O.ooo% O I O O W W O.ooIy% W o 0.W.X O.ooo% O O 82158 84480 13oa28 12 134987 13 O O O O O O.ooo% O O.ooo% W O.C0X% W 0.03% O.ooo% W O.ooo96 W o W O.ooo% O.ooo% O O O 10 O O O IO 10.WNi 0.001% O O.CU% 0.Wo O W O.ooo% O.ooD% O.ooo% O.ooo% 606 604 607 O 1010 1010 1057 1001 O O O O O O O O O O a m o.mo o.mo0.000% o.- O.ooo% W W O.ooo% O.ooo% O 0.0.Wo~ O.ooo96 O.ûCû% O o.^ o.^ o.mo 0.00096 o m o o.^ W 0.m' W W o O.OU% B 0.m O O O.aI370 0.- 141000 146482 W W O.ooo% O.ooo% O.ooo% W W o l W O.oo[p/, O.ooo% O O O O O.ooo% B O.ooo% O.ooo% 0.03% 0.033% 0.03% O.ooo% W O.@D% O O.ooo% O.oM)% O o.- 0.Wo 0.Wo O O O O O o.mo 0.000% O.ooo% W O O.ooD% W O.Mx)% O.@B% O W % l O.ooo% W O.ooo% I NA NA NA NA NA NA NA NA NA I I NA 39 NA NA NA NA NA NA 92-1 128462 128506 128815 13(1269 lm89 179582 18sKn 1891215 `,,-`-`,,`,,`,`,,` - w GRS 4657771 86316 TUaicìmpmts 11 1913 TdJJAES LeakKl2cfrvbIe NA 93 % ' o o f I d ~ ~ ~ 4.861% NA %ofTdaiCarp O.ûCQ% NA Ledpxl3orm I NA %ofLedais I 0.314% NA NA %ofTaal0.mo Ledpxl4Tm I O NA %ofL&e3 I m NA NA O O.M10% O.KC% I 37515 37646 37637 57576 51546 61249 57949 14 41 57 67 41 O O O O O 2 m O.ooo% W W W O.ooo% 3.509% 2985% 4.878% 0.0XXl O.oM)% O.oo[)% W W o l W o m O.Oo3310 O.m% 31231 O 37455 O I O O O O O o.^ 0.000% ~ ~ O m l W O.ooo% W o W l O.ooo% W 0.0.002% O I O O O O O O O 0.0 W W o W 0.0.W 0.W 0.W 0.W 0.0 W o W o O.û3% W 0.O.ooo% O.ooo% W o.molo.am m m O o.molaam Vahe-Ii= 50,000 (continued) % of ieakers Total Components Total ieakers Leaked or More 9’0 of M e r s I I %ofLeakers %ofmers Total Components Total M e r s Leaked or More % of Leakers % of M e r s Total 94-1 94-2 94-3 1657771 1913 93 4.861% 0.002% 0.314% 0.000% 207828 43 212462 67 2.985% 0.0012 O 0.000% 0.000% O 0.000% 300659 188 1.596% 0.001% O.OOo% O.Ooo% O O 0.000% 0.000% 1310233 858 49 5.711% 0.001% 0.932% 0.000% 0.117% 0.000% O 0.000% 0.000% 0.000% O 0.000% 0.000% 0.000% 0.000% 3443 89 5.618% 0.015% O 0.000% 0.000% O IT1 0.000% I- % of M e r s I ==- Valve Liquid Total Components Total Leders Leaked or More % of Leakers % of M e r s % of M e r s 0.000% 0.000% 0.000% 0.000% 0.000% Total Components Total Leaken Leaked or More % of Leakers % of Total Com Leaked or More % of ieakers % of Total Co 2.326% 0.000% O 1494303 1563 i i6 7.422% 0.008% 15 0.960% 0.001% 0.128% 0.000% 1364399 1379 90 6.526% 0.007% 0.435% 0.000% O 0.000% 0.000% 11861137 O.Ooo% I$’ 0.532% 0.000% O 0.000% 0.000% O.Ooo% 0.000% 0.000% O 0.000% O.Ooo% 0.000% 0.000% 2yl 95-1 944 302539 275600 117 144 3.419% 4.861% 0.001% 0.003% O O 0.000% 0.000% 0.000% 0.000% O O 0.000% 0.000% O.Ooo% 0.000% I O 8!2 0.000% 12.500% O.OOo% 0.000% 0.049% 0.000% O O O O 0.000% 0.000% 0.000% 0.000% 0.000% 0.000% 0.000% 0.000% O O O O 0.000% 0.000% 0.000% 0.000% 0.0001 0.000% 0.000% 0.000% 0.000% 0.000% 0.000% O O 0.000% 0.000% 0.000% 0.000% 0.000% O 0.000% O O.oOo% 0.000% O.Ooo% 0.000% 1.111% 0.002% O 0.000% 0.000% 0.000% O 0.000% 0.000% :2 0.000% 0.000% O 0.000% 0.000% ::2 O.Ooo% 0.000% 0.000% 0.000% 0.000% 0.000% O 0.000% 0.000% 95-2 9.091% 0.000% 0.046% O O 0.000% 0.000% 0.000% 0.000% O O 0.000% 0.000% 0.000% 0.000% 2.222% 1.754% 0.003% 0.002% O 1.481% 0.000% 0.002% 0.000% 95-3 287896 347880 280 230 11 17 3.929% 7.391% 0.004% 0.005% 1 0.357% 0.435% 0.000% 0.000% O O 0.000% 0.000% 0.000% 0.000% 954 362524 174 11 6.322% 0.003% 10.000% 0.026% O 0.000% 0.000% O 0.000% 0.000% 379201 9.938% 0.004% 8.511% 0.005% 0.000% 0.000% 0.851% 0.001% 0.000% 0.000% 0.000% 0.000% 390172 406744 7.229% 0.002% 8.247% 0.002% 2.410% 1.031% 0.575% 0.000% O 0.000% 0.000% 1.111% 5.479% 0.000% 0.0014 O O 0.000% 0.000% 0.000% 0.000% 3i;l 367645 0.000% 0.000% O 0.000% 0.000% O 0.000% 0.000% 1.852% 1.439% 0.000% 0.003% 0.002% 0.000% O O O 0.000% 0.000% 0.000% 0.000% 0.000% 0.000% 0.001% 0.000% 0.002% 0.002% 0.0006 O O 0.000% 0.000% 0.000% 0.000% O 0.000% O 0.000% O 0.000% 1.205% 0.000% 0.000% 0.000% 3653 3994 11 1 9.091% 12.500% 0.027% 0.025% O O 0.000% O.Ooo% 0.000% O.Ooo% O O 0.000% 0.000% 0.000% 0.000% 102736 111 10 9.009% 0.010% 1.802% 0.002% O O.OOo% 0.000% 101419 102999 49 13 8.163% 12.329% 0.004% 0.009% O 0.000% 1.370% 0.000% 0.001% O O O.OOo% O.OOo% 0.000% 0.000% 965625 100685I 0.000% 0.000% 0.000% -P 508187 P A-9 Copyright American Petroleum Institute Provided by IHS under license with API No reproduction or networking permitted without license from IHS Not for Resale 113913 87 9.195% 0.007% O 0.000% 0.000% O 0.000% 0.000% `,,-`-`,,`,,`,`,,` - Total Components Total ìeakers Leaked or More % of Leakers STD.API/PETRO ~ ~ ~ PUBL 310-ENGL 1997 0732290 Ob04722 019 Table A-5 Combined Matrix for Lakers with Values >= 100,ûûû TdslI 46771 %ofTdcbnp hkKl3orlMcae %ofk&fs QofTdCaip i.&d4Tm I I 0.W 0.W d Taalk&fs %ofTuaiCcarp I€A7d3orm %ofLakm QofTdcaip W T m 0.001% I 0.~5% O %OfTaalCarp Le&d2ork %oflP&m I O.ûD% %ofkakm T 'g 4.052% I I I 4310233~ 639 25 3.912% 0.001% 0.46% I I 91-1 86316 GA NA NA NA NA NA NA NA NA 114068 NA NA NA 91.2 913 NA NA NA NA 113233 55 NA NA NA NA 112949 53 NA NA NA NA NA NA NA 81147 85476 O O O O.ûD% W 0.W0 O.Oû% o.ooo%o m O O O O.OK% W o o.ooo% O.ooo% m 0.W0 O O O O.ûX)% m m O.CK% m m o I 0.W I NA NA NA EUA NA NA NA NA NA 374 O NA NA NA NA 417 NA NA NA NA NA NA NA NA NA NA NA 461 NA NA NA NA NA NA NA NA NA NA 2Ỵ(136 34048 37 NA NA NA NA NA NA 3225 37 NA NA NA I %oflP&m 0.Wo %OfTaalcaip O.ooo% NA 9t3 9t2 %185 128462 128506 O O O O O.Oû% o.a m 0.WoI m W o O O I O O.W~ o.moo W W O.ooo% O O O NA NA NA I %I 914 88992 14 NA NA NA NA NA NA NA NA NA 95679 32 NA NA NA NA NA 9.24 128815 13029 31 O O O 0.m 0.m 0.m m û W l 0.W O O ~ m m a m 0.0005"o W W o O O O 0.03% 0.0% W o W O W % W m W o m O.OfDZ W 0.00% 112568 El58 84480 O O m m O m 0.W 0.0% m m m O O O m m m m 22 19 28 O O m 0 m o 5.263% O.ooo46 W 0.001% O O O o.wo o.mO m O W u O.ooo% W O O m 0.0.Wo 0.Wo 130828 W 9 O O m o.ooo% W 0.0% O O 0.m0 m 0 m 0.W0 O O o.ooo% m 0 m m 141W O m m O o.ooo% 0.mo O 0.Wc 0.ûYR 146482 10 lo.m 0.001% O m m O 0.W 0.m m m O Rnp-Iiqlld lofkakm %ofTaalcCnp Ledad3orMXe O %oflP&m O.ooo% %ofTaallconp I€A7d4Tm %ofJ2¿bs BofTaallconp 0.W O 0.000% 0.Wo NA NA 410 O 604 O O O 606 O O 604 O 607 1010 O O O O OOSvo W O.ooD4Bo m 0a W m W o O.ûX% O O O O W W W o O.ooo% 0.Wo W o W 0.03% O a m O.NO% 0.Wo W 0.W 0.W O O O.ûB% O.ooo% O.ooo% O.Oal% O O O O O O.W m 0.000% m 0.000% O.ooo4b 0.CXWo 0.CQX W m 1010 1057 O 1001 O O O O O.NO% 0.Wo 0.Wo 0.Wo 0.Wo O.ooo% O O O 0.Wo 0.W W W O.ooo% W o O O O O.W~ 0.00046 W o W o O.ûD% o.m0 Valve-* 14W3û3 1174 83 O 0.085% NA NA NA NA NA NA NA NA m NA NA 1364399 34781 NA NA NA 32115 7.070% 0.006% 12 l.oZZ% 0.001% I 1 1058 64 6.M% O.W% I %ofTaalcCnp hkKl3orlVtX NA I NA o.mO I NA NA 0.0009ro I N A m %OfTaalcaip Ledied4Tnres %ofJ2¿bs %ofTaalccaip Tdalcaiporats I0.m I I NA 11861137I 262575 NA NA 108 NA NA NA NA NA NA NA NA NA zl5462 NA NA NA NA NA NA 33199 i57 NA NA NA NA NA NA NA NA NA 2678% 37455 O o.ml 376% 23676 239515 O O O O m m W O.aX% O o o o S O m O.ûB% 0.000% O [ O O O ~ a~ m1 m O.W o.mol a m m m O O O I O W l O.Cû3% W O.ooo% O.ooD4Bol W W 0.Wo 2700is I 271313 27sT19 273729 31624 Not for Resale 37W V576 O o.m0 23645 A-10 Copyright American Petroleum Institute Provided by IHS under license with API No reproduction or networking permitted without license from IHS 37515 O 57546 3 O O O O O o.am a m m 0.000% o.^ O.wIy% W W o O.aJ2% W 0.CWh m O.ooo% O.Cü% O O O O O O O O.ooD4Bo m O.ûB% O.ooo% m 0.033% 0.000% m a m 0.m10.m o.mO O O I O O O O O.Kt% 0.Wo 0.03% 0.KJX O.OC% 0.0% W O.CH% W W O.ooo96 0.0 m o O.ooo96 31231 m 50807 23871 O O O.ooD% 0.- 0.mlO.W 61249 51449 2 2381% 7.692% O.CU2% 0.003% O O.CO% 3.846% 0.000% m O O 0.0.0 W 0.00% O 0.W 54166 mm 3 7.692% 5.714% 0.001)96 0032% 0.001% O O O O O.W m O O O O o m l o.0.00095 m o m l o.mO o.am a m O W % W o 0.KJX ~ ~ 0.0KK 0.033% ~ 0.W 2761(341 417931 423932 443179 445427 W o l 0.00% `,,-`-`,,`,,`,`,,` - 31431 58 3.448% 0.006% Taal&q&íTs TdlP&m bkdZWlVtX Table A-5 Combined Matrix for Leakers with Values >= lûû,Oûû (continued) Totnl Total Leakers Leaked or More % of M e r s % of Total Comp Leaked or More % of M e r s % of Total Comp Leaked Times % of M e r s % of Total Comp Fitting Liquid Total Components Total ieakers Leaked or More % of Leakers % ofTotalComp Leaked3orMore % ofLeakers %ofTotalComp Leaked4Times 4657771 1456 59 4.052% 0.001% 0.275% % of Leakers %ofTotalComp Valve Gas Total Components Total Leders Leaked or More % of M e r s % of Total Comp Leaked or More % of M e r s % of Total Comp Leaked Times % of Leakers %ofTotalComp Valve Liquid Total Components Total Leakers Leaked or More % of M e r s % of Total Comp Leaked or More % of Lakers % of Total Comp Leaked Times - ~ %ofTotalComp TotalComponents 94-3 94-4 3.125% 0.000% O 0.000% 0.000% 300659 137 2.190% 0.001% 302539 97 2.062% 0.001% O O 0.000% O.Ooo% 0.000% 0.000% 32 O 0.000% 0.000% 170644 4310233 20 639 O 25 3.912% 0.000% I 0.001% I 0.000% I I O 0.469% 0.000% I 0.000% I 0.000% I O I I I I 0.000% I 0.000% I 178590 23 O 0.0001 0.000% O 0.000% 0.000% O 95-2 95-3 95-4 96-1 %-2 287896 226 3.097% 0.002% O 0.000% 347880 362524 146 4.110% 0.002% 0.685% 0.000% 367645 134 11 8.209% 0.003% O 0.000% 0.000% O 0.0002 O.Ooo% 379201 192 13 6.771% 0.003% 170 O 0.000% 0.000% O 0.000% O.Ooo% O O O O O 0.000% 0.000% 0.000% 0.000% 0.000% 0.000% 0.000% 0.000% 0.000% 0.000% 0.000% 267999 71 O 284082 35 1 O.Ooo% 2.857% 2.857% 0.000% 0.000% I 0.000% O O 0.000% 0.000% 0.000% 0.000% 0.000% I O.Ooo% O O 278592 35 I 0.000% 1271 O 0.000% 0.0001 O 0.0002 0.000% 1289 O 0.000% 2061 O 0.000% 0.000% 0.000% 2188 O 0.000% O.Ooo% O 0.000% 0.000% O.Ooo% 1494303 1174 83 7.070% 0.006% 12 1.022% 0.001% 68268 43 6.977% 0.004% O 0.000% O 0.000% 0.000% 95-1 I 275600 0.730% 0.000% O O O.OOO% 0.0002 0.000% 0.000% 0.000% O O 0.000% 0.000% 0.000% O O.Ooo% 0.000% 0.000% O 0.000% I 106 1.887% 0.001% O 0.000% 0.000% 0.000% I 34431 58 3.448% 0.006% O 0.000% I O.OOO% I 0.000% 11 6.471% 0.003% 0.588% 0.000% 288115 354230 351719 59 61 56 6.780% 11.475% 10.714% 0.001% 0.002% 0.002% O 0.000% 1.639% 3.571% 0.000% 0.000% 0.001% O 0.000% O 0.000% 2177 3791 O 14.286% 0.000% 0.000% 0.046% 0.000% O O O 0.000% 0.000% 0.000% 2160 O 0.000% 0.000% O 0.000% 0.000% 0.000% O 0.000% 0.000% 0.000% O 0.000% 0.000% 0.521% O.Ooo% O O.Ooo% O.Ooo% 390172 60 3.333% 0.001% O 0.000% 406744 68 4.412% 0.001% O 0.0004 0.0001 O.Ooo% O O O 0.000% 0.000% 0.000% 0.000% 3653 10 O O.Ooo% 0.0001 0.000% 0.000% O O 0.000% 0.000% 0.000% 0.000% O O 0.000% 0.00046 0.000% 0.000% 3686 O 0.000% 3994 20.0004 0.02s'.; O 0.000% 0.000% O O.Ooo% 0.000% I 0.000% 0.085% 0.000% - % of Leakers 94-2 212462 55 3.636% 0.001% O 0.000% 0.000% 94-1 I 207828 0.000% - %ofTotalComp Pump-Liquid Total Components Total M e r s Leaked or More % of M e r s % of Total Comp Leaked or More % of M e r s % of Total Com I I I 0.000% 1364399 1058 64 6.049% 0.005% O 0.000% 0.000% O 60176 56 7.143% 0.007% O 0.000% 0.000% O O.OOo% 0.000% 0000% 11861137 0000% I 508187 108119 110670 101227 I43 i9 93 13 10 6.294% 10.924% 10.753% 0.008% 0.012% 0.010% O.OOO% 0.699% 2.521% 2.151% O.Ooo% 0.0018 0.003% 0.002% O O I O 0.000% 0.000% 0.840% 0.000% 0.000% 0.000% 0.001% 0.000% 68756 76 7.895% 0.009% O 60910 101800 105120 63 119 103 13 14 9.524% 10.924% 13.592% 0.010% 0.013% 0.013% O O O 0.000% 0.000% O.OOO% 0.000% 0.000% 0.000% O O O 0.000% O.Ooo% 0.000% 0000% 0000% 0000% 522007 780638 799109 I I O.Ooo% 101357 102736 113912 85 69 102 10 6 9.524% 8.824% 7.059% 8.696% 0.010% 0.009% 0.006% 0.005% O O 1.905% 0.000% 2.353% O.ooO% 0.002% 0.000% "0; 0.oy O O 0.000% O.Ooo% 0.000% O.Ooo% O.OOO% 0.000% 0.000% O.Ooo% 103955 i 05 102263 104926 97831 55 96 46 II 3.636% 11.458% 6.522% 0.002% 0.010% 0.003% O O O 0.000% O.Ooo% 0.000% 0.000% 0.000% O.Ooo% O O O 0.000% 0000% 765332 0.000% 0.000% 0000% 907687 A-1 `,,-`-`,,`,,`,`,,` - Copyright American Petroleum Institute Provided by IHS under license with API No reproduction or networking permitted without license from IHS 106169 132 5.303% 0.007% 0.758% 0.001% O 0.000% Not for Resale OOoo% 789283 101419 93627 37 2.703% 5.714% 0.0014 0.002% O 0.0004 0.000% 0.000% O o.o00?i O.Ooo% O0004 91291: 102999 9.615% 0.005% 0.000% O.Oo(i'6 I I I ~~ STD.API/PETRO American Petroleum Institute PUBL 310-ENGL 1993 ~ ~ 0732290 Ob04724 991 1220 L Street, Northwest Washington, D.C 20005 202-682-8000 http:llwww.api.org Order No J31O00 `,,-`-`,,`,,`,`,,` - Copyright American Petroleum Institute Provided by IHS under license with API No reproduction or networking permitted without license from IHS Not for Resale ~

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