Affinity guided isolation, structure elucidation and total synthesis of laetirobin a and its analogue synthesis for therapeutic development 5

Appendix FT-IR Data OH 3-11 C8H7IO3 278.0 HO O I 316 Appendix OTs 3-2 C22H19IO7S2 586.4 TsO O I FT-IR Data 317 OBn 3-3 C13H12O 184.2 318 Appendix TsO O OTs 3-24 C57H48O15S4 1101.2 OBn OTs O OTs FT-IR Data 319 3-5 C29H24O7 484.5 O OBn OH HO O O O 320 Appendix FT-IR Data 321 OH O O HO O O O OH O OH O 2-1 C44H32O12 752.7 O OH O 5-2 C18H14O3 278.3 O 322 Appendix I OH 5-8 C8H7IO2 262.0 O FT-IR Data 323 I OTs 5-9 C15H13IO4S 416.2 O 324 Appendix OTs 5-18 C20H17IO6S2 544.4 TsO I FT-IR Data 329 TsO OTs OBn 5-19 C53H44O13S4 1017.2 OTs OTs 330 Appendix MeO O O 3-40 C19H14O5 322.3 O OMe FT-IR Data 331 HO O O 5-23 C17H10O5 294.3 O OH 332 Appendix TsO OTs 3-56 C30H34O7S2Si 598.8 O TES FT-IR Data 333 HO OH 3-57 C16H22O3Si 290.4 O TES 334 Appendix HO O 3-35 C16H22O3Si 290.4 O TES FT-IR Data 335 HO O 3-34 C10H7IO3 302.1 O I 336 Appendix FT-IR Data 337 HO O 5-28 C14H16O3 232.3 O 338 Appendix HO O 5-33 C14H16O3 232.3 OH FT-IR Data 339 AcO O O 5-32 C16H18O4 274.3 340 Appendix AcO O OAc 5-35 C18H20O5 316.3 FT-IR Data 341 AcO O 5-38 C18H20O6 332.3 OAc O 342 Appendix HO O 5-40 C14H16O4 248.3 O OH FT-IR Data 343 344 Appendix [...]... 3 -56 C30H34O7S2Si 59 8.8 O TES FT-IR Data 333 HO OH 3 -57 C16H22O3Si 290.4 O TES 334 Appendix 5 HO O 3- 35 C16H22O3Si 290.4 O TES FT-IR Data 3 35 HO O 3-34 C10H7IO3 302.1 O I 336 Appendix 5 FT-IR Data 337 HO O 5- 28 C14H16O3 232.3 O 338 Appendix 5 HO O 5- 33 C14H16O3 232.3 OH FT-IR Data 339 AcO O O 5- 32 C16H18O4 274.3 340 Appendix 5 AcO O OAc 5- 35 C18H20O5 316.3 FT-IR Data 341 AcO O 5- 38 C18H20O6 332.3 OAc... OTs 5- 10 C43H36O9S2 760.9 OBn OTs O FT-IR Data 3 25 O OH OBn 5- 11 C29H24O5 452 .5 OH O 326 Appendix 5 O O O OBn 5- 12 C29H24O5 452 .5 O FT-IR Data 327 O O O 5- 13 C44H32O8 688.7 O O O O O 328 Appendix 5 OTs 5- 18 C20H17IO6S2 54 4.4 TsO I FT-IR Data 329 TsO OTs OBn 5- 19 C53H44O13S4 1017.2 OTs OTs 330 Appendix 5 MeO O O 3-40 C19H14O5 322.3 O OMe FT-IR Data 331 HO O O 5- 23 C17H10O5 294.3 O OH 332 Appendix 5 TsO... HO O 5- 33 C14H16O3 232.3 OH FT-IR Data 339 AcO O O 5- 32 C16H18O4 274.3 340 Appendix 5 AcO O OAc 5- 35 C18H20O5 316.3 FT-IR Data 341 AcO O 5- 38 C18H20O6 332.3 OAc O 342 Appendix 5 HO O 5- 40 C14H16O4 248.3 O OH FT-IR Data 343 344 Appendix 5 . OBn OTs O OTs O 5- 10 C 43 H 36 O 9 S 2 760.9 Appendix 5 326 OBn OH O OH O 5- 11 C 29 H 24 O 5 452 .5 FT-IR Data 327 OBn OO O O 5- 12 C 29 H 24 O 5 452 .5 Appendix 5 328 O O O O O O O O 5- 13 C 44 H 32 O 8 688.7 FT-IR. O O O O HO O OH O OH O OH O 2-1 C 44 H 32 O 12 752 .7 Appendix 5 322 OO OH 5- 2 C 18 H 14 O 3 278.3 FT-IR Data 323 OH O I 5- 8 C 8 H 7 IO 2 262.0 Appendix 5 324 OTs O I 5- 9 C 15 H 13 IO 4 S 416.2 FT-IR Data 3 25 OBn OTs O OTs O 5- 10 C 43 H 36 O 9 S 2 760.9 Appendix. Appendix 5 FT-IR Data Appendix 5 316 OH HO O I 3-11 C 8 H 7 IO 3 278.0 FT-IR Data 317 OTs TsO O I 3-2 C 22 H 19 IO 7 S 2 58 6.4 Appendix 5 318 OBn 3-3 C 13 H 12 O 184.2 FT-IR