Affinity guided isolation, structure elucidation and total synthesis of laetirobin a and its analogue synthesis for therapeutic development 5

... δ 15 9 .42 , 15 8 .10 , 15 5.06, 15 5.03, 15 4 .19 , 15 3.80, 15 3.25, 15 1.98, 12 9.50, 12 9.03, 12 8.39, 12 8 .12 , 12 4. 42, 12 3.22, 12 2.83, 12 1. 34, 12 1.29, 12 0.66, 11 1 .49 , 11 1.23, 11 1. 01, 11 0.55, 10 6 .10 , 10 4. 92, ... 16 1.5, 16 1 .4, 16 1.3, 15 9.8, 15 9.7, 15 9.7, 15 9.6, 15 8.7, 15 8.2, 15 7.3, 15 3.7, 14 4. 7, 12 3.9, 12 3.9,...

Ngày tải lên: 10/09/2015, 15:48

... O OTs 5- 10 C43H36O9S2 760.9 OBn OTs O FT-IR Data 3 25 O OH OBn 5- 11 C29H24O5 452 .5 OH O 326 Appendix O O O OBn 5- 12 C29H24O5 452 .5 O FT-IR Data 327 O O O 5- 13 C44H32O8 688.7 O O O O O 328 Appendix ... Data 337 HO O 5- 28 C14H16O3 232.3 O 338 Appendix HO O 5- 33 C14H16O3 232.3 OH FT-IR Data 339 AcO O O 5- 32 C16H18O4 274.3 340 Appendix AcO O OAc 5- 35 C18H20O5 316.3 FT-IR Dat...

Ngày tải lên: 10/09/2015, 15:49

... Low-Resolution-Mass Data HO O 5-33 C14H16O3 232.3 OH 373 AcO O O 5-32 C16H18O4 274.3 374 Appendix Low-Resolution-Mass Data AcO O OAc 5-35 C18H20O5 3 16. 3 375 AcO O 5-38 C18H20O6 332.3 OAc O 3 76 Appendix ... Low-Resolution-Mass Data 353 OH O 5-2 C18H14O3 278.3 O 354 Appendix Low-Resolution-Mass Data 355 O 5-4 C36H24O4 520 .6 O O O O O 5 -6 C36H24O4 520 .6 O O 3 56 Appendix Low-Resolutio...

Ngày tải lên: 10/09/2015, 15:50

... 232.1099 412 Appendix O AcO O 5-32 C16H18O4 274 .1205 High-Resolution-Mass Data 413 O AcO OAc 5-35 C18H20O5 316.1311 414 Appendix O O AcO OAc 5-38 C18H20O6 332.1260 High-Resolution-Mass Data 415 O ... High-Resolution-Mass Data 391 O O O O 5-4 C36H24O4 520.1 675 392 Appendix O O O O 5-6 C36H24O4 520.1 675 High-Resolution-Mass Data 393 O I OH 5-8 C8H7IO2 261.9491 394 Appendix O I OTs 5-9 C15H13...

Ngày tải lên: 10/09/2015, 15:50

... Programme (PhD student under the supervision of Dr Martin Lear) • Affinity- Guided Isolation, Structure Elucidation and Total Synthesis of Laetirobin A and Its Analogue Synthesis for Therapeutic Development ... theta = 27. 48 99 .8 % Absorption correction Sadabs, (Sheldrick 2001) Max and transmission 0. 988 8 and 0.9456 Refinement method Full-matrix l...

Ngày tải lên: 10/09/2015, 15:50

... T matsutake polysaccharide, named TMP -A, was obtained by the above processes and the yield rate of TMP -A was 0.22% (0.432 g) for the starting material The DPPH− radical scavenging activity of ... recorded on a Varian Unity INOVA 400/45 in D2 O with tetramethylsilane as internal standard All data were presented as means ± standard deviation (SD) of three replications Statisti...

Ngày tải lên: 28/06/2014, 11:20

... A < /b> and < /b> B syntheses < /b> by employing a < /b> cation-controlled regioselective ring opening of < /b> a < /b> tertiary epoxynitrile < /b> which follows predominantly a < /b> ‘non-favored’ palladium-< /b> catalyzed < /b> 5-< /b> endo < /b> pathway As catalyst, ... of < /b> DIPEA or absence of < /b> base afforded no cyclization products (Table 1, entries 13 and < /b>...

Ngày tải lên: 26/01/2016, 10:44

... Institute Working Paper Series No 11 July 2000 The Case of the Missing Market: The Bond Market and Why It Matters for Financial Development Richard J Herring and Nathporn Chatusripitak ADB I NSTITUTE ... maturities of less than year), notes (with maturities of to years) and bonds (usually with maturities greater than years) 18 market and holding i...

Ngày tải lên: 24/10/2012, 09:40

... performance characteristics and mechanical properties of bamboo Dissertation, Chinese Academy of Forestry, Beijing, China pp 147 Yusoff, M.N.M, A Abd.Kadir, and A.H Mohamed 1992 Utilization of bamboo ... the physical properties of pulp [Tamolong 1967; Zamuco et al 1969] Aging of a bamboo culm influences physical, chemical, and mechanical properties, and...

Ngày tải lên: 22/02/2014, 09:20

... ACCOUNTING ETHICS AND ITS IMPORTANT ROLE FOR REDUCTION OF ACCOUNTING FRAUD: AN EMPIRICAL STUDY IN HANOI By HOANG VAN THU October 2011 Supervisor: Dr Nguyen Hong Quan ABSTRACT As ... going to analyze the accounting ethic and its role for reduction of accounting fraud in this project -8- 1.2 Problem and statement Nowadays, the ethics has be...

Ngày tải lên: 13/03/2014, 14:20

... more and more developing; ethic is cared more and more In this study, I will analyze the importance of accounting ethics and prove its role in reducing accounting fraud 1.2 Accounting fraud in ... private and public companies in Hanoi, and auditors in the public companies and private companies The content of the questionnaire include impact of eth...

Ngày tải lên: 13/03/2014, 14:20

... standard could handle thousands of devices in an Asian metering product [2] N-DIMENSIONAL ADDRESSING SCHEME AND ITS ROUTING ALGORITHM (3, 255) 1023 (2, 5) 517 Figure 5: Tree-based addressing and ... TRAACS algorithm and traditional Cskip based tree-based routing algorithm for ZigBee network The Cskip algorithm assumes two network parameters, Cm and Rm A perfo...

Ngày tải lên: 21/06/2014, 23:20

... concentration on the surface of the film and finally ks is the desorption rate constant Substituting known values and by fitting the experimental data with the mathematical model of Eq 1, the h value ... bulk, C10 is the concentration inside the gel, S and V1 are, respectively, the surface and the volume of film, V2 is the volume of the bulk, h is the mas...

Ngày tải lên: 22/06/2014, 00:20

... onto Chitin 72 Free dithizone Chitin -dithizone Figure 3: IR spectra of (a) free dithizone and (b) dithizone- immobilized chitin The XRD spectra and their d-spacing data of free dithizone and dithizone- immobilized ... (ml), and m is the weight of the chitin or chitin -dithizone adsorbents The effect of adsorbent mass on the amount of adsorbed...

Ngày tải lên: 07/08/2014, 14:20

... noitanimesni laicifitrA JM sdleiF ,CA kcinraW ,RD nidraH 21 917-517 ,75 ,5002 cetooZ teV deM sarB qrA anivob aemêf ad latineg oãgró od asonev arutetiuqraoignA DJ seãramiuG ,RAT aluaP ,CAC sednanreF ... noitalupinam dna nrettaP FM zenitraM ,SP illesuraB ,AG oB 44-73 ,64 ,9891 minA dnI loB asocumbusovluvartni uo ralucsumartni aiv alep adartsinimda lonetsorpolc ed esod-inim a2 moc sadatart sahl...

Ngày tải lên: 07/08/2014, 18:21