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Tiêu đề Research and Production of Scented Candle Products from Certain Essential Oils
Tác giả Pham Thi Hong Hanh
Người hướng dẫn Ph.D. Pham Bang Phuong
Trường học Thai Nguyen University of Agriculture and Forestry
Chuyên ngành Food Technology
Thể loại Bachelor Thesis
Năm xuất bản 2023
Thành phố Thai Nguyen
Định dạng
Số trang 58
Dung lượng 834,95 KB

Cấu trúc

  • PART I. INTRODUCTION (0)
    • 1.1. Research rationale (8)
    • 1.2. Research’s Objectives (9)
      • 1.2.1. General objectives (9)
      • 1.2.2. Specific objectives (9)
    • 1.3. Scientific and practical significance (9)
      • 1.3.1. Scientific significance of the topic (9)
      • 1.3.2. Practical significance of the topic (10)
  • CHAPTER II. LITERATURE REVIEW (11)
    • 2.1. Scientific basis of the topic (11)
      • 2.1.1. Candlestick Overview (11)
      • 2.1.2. Essential Oil Overview (16)
    • 2.2. Domestic and foreign research works (23)
      • 2.2.1. Overview of domestic research (23)
      • 2.2.2. Overview of the research situation in the world (24)
  • CHAPTER III. MATERIALS, RESEARCH CONTENT AND (25)
    • 3.1. Subjects and scope of study (25)
      • 3.1.1. Research subjects and research materials (25)
      • 3.1.2. Chemicals used (25)
      • 3.1.3. Research equipment and instruments (26)
    • 3.2. Scope of study location and time (28)
      • 3.2.1. Scope of research (28)
      • 3.2.2. Research location (28)
      • 3.2.3. Study period (28)
    • 3.3. Research content (28)
    • 3.4. Research methodology (29)
      • 3.4.1. The process of separating essential oils by steam attraction method (29)
      • 3.4.2. Production method of scented candles (34)
      • 3.4.3. Proposal for the production process of scented candle (35)
      • 3.4.4. Experimental layout method (36)
    • 3.5. Data processing methods (43)
  • CHAPTER IV. RESULTS AND DISCUSSION (44)
    • 4.1. Research results on the production process of aromatic candles from (44)
      • 4.1.1. Research results optimize the conditions in the production process of (44)
      • 4.1.2. Building the production process of scented candles (47)
    • 4.2. Results of development of scented candle products from natural materials . 48 (53)
  • CHAPTER V. CONCLUSION AND RECOMMENDATIONS (55)
    • 5.1. Conclusions (55)
    • 5.2. Recommendations (55)

Nội dung

THAI NGUYEN UNIVERSITY UNIVERSITY OF AGRICULTURE AND FORESTRY PHAM THI HONG HANH RESEARCH AND PRODUCTION OF SCENTED CANDLE PRODUCTS FROM CERTAIN ESSENTIAL OILS... During the process of i

INTRODUCTION

Research rationale

A candle is a solid material, usually a combination of candle-making materials, with a heart in the middle, lit to provide light and sometimes to warm up Candles today are mostly made of paraffin It can also be made from beeswax, plant wax, and gels Along with the progress of the world economy, candles also have a history of annual development Since ancient times, people have used coconut oils and fats, cows, goats, and various other animals to make candles In respect of the nobility, people used Beeswax Candles are known to have originated in China around 200 BC and were obtained from whale fat By the 19th century, winter fat was the main raw material for making candles

The advancement in raw materials was made in 1820, when stearin was mined Stearin was a chemical compound created from refined fat and used in candle making

Previously, in Vietnam, candles were often used to worship ancestors and to light weddings In times of modern social development such as the present, when people's lives are increasingly improved, the use of candles is becoming increasingly popular

The scent of the harmonious combination of candles and flowers gives people a feeling of romance and coziness Thanks to their level of sophistication, candles are not simply lit objects but also considered a product of art Despite its small size, a candle can accentuate an entire interior space, even a room with a magnificent and wonderful view

4 On that basis, I propose to implement the topic: Research and produce scented candle products from some essential oils

Aiming to optimize and enhance the production process of scented candles from some essential oils and bring the most practical benefits to consumers.

Research’s Objectives

Research and production of scented candle products from a number of essential oils

Content 1: Research and develop the process of producing scented candles from natural materials

A Research on optimizing the conditions in the production process of scented candles from natural materials

Experiment 1: Research on the selection of waxes to use to produce scented candles

Experiment 2: study the mixing ratio of beeswax and soy wax Experiment 3: Study on the ratio of essential oil blends in scented candles B Develop the production process of scented candles

Content 2: Develop scented candle products from natural ingredients

- Research and manufacture scented candle products from a number of essential Oils

Scientific and practical significance

1.3.1 Scientific significance of the topic

- The results of the study will provide new scientific data on: the ingredients in candle wax

5 - The influence of factors on the ability to extract essential oils

- Long-term and effective storage method - Develop the essential oil extraction process and candle wax production process with the most optimal conditions

1.3.2 Practical significance of the topic

- Help students improve their experience and skills in practicing scientific research, consolidate theoretical knowledge, and apply it in practice to improve themselves

- From the research results of the project, it will contribute a part of the research into the aromatic candle production process and essential oil extraction process, health and economic benefits for the community

LITERATURE REVIEW

Scientific basis of the topic

2.1.1 Candlestick Overview 2.1.1.1 General introduction to scented candles

Scented candles are a solid mass of fuel, usually waxy and have hearts in the middle to light sometimes using heat Today candles are usually made from paraffin wax, which can also be made from soy wax, beeswax, and animal fats

Since humans found and refined petroleum from nature, candles have been mass-produced to serve humans In the filtration process, in addition to the main products of lock oil, there are also countless products used in different industries, paraffin and gels are byproducts of petroleum but it is the main raw material in the candle manufacturing industry In addition to paraffin and gels, people also use some other materials to produce candles such as soy wax, which is a cloudy color material derived from nature, has a natural aroma and does not harm human health

Paraffin candles and soy wax candles, pillar candles, tea lamp candles, flower candles, water drop candles Disposable candles have a high gel density, non- receptive candles have a low gel density To increase the aesthetics of candles, people often add colors and ornaments, add essential oils to create aroma for candles Therefore, in addition to the role of lighting candles, it is also used to decorate in formal places and on special days

The faint scent of candles is now popular with many households However, if used too much, it will affect health The Vietnam Institute of Scientific Research said that the cause of toxicity of scented candles is due to the candle heart made of the core, especially materials that do not have a clear origin Especially many

7 substances contained in scented candles are toxic to the human body such as toluene (C6H5CH3), acetone (CHCOCH3), formaldehyde (HCHO), methylene chloride (CH2Cl2) Many of these substances have been shown to cause cancer, inadvertence, and damage to the nervous system, Using scented candles too much can provoke asthma attacks, candles with synthetic aromas from chemicals are highly pathogenic

The Vietnam Institute of Industrial Sciences said that the more fragrant the smell, the more toxic it is, especially candles with synthetic aromas from chemicals

2.1.1.2 The composition of scented candles

- Soybean wax: To make soy wax, we need some materials such as stoves, kettles, cups, rubber powder, paraffin oil, soybean oil

Steps to make soy wax Step1: Blend rubber powder with paraffin oil in the right proportions to avoid the mixture clumping and help dissolve the raw materials most effectively

Step 2: Pour the mixture into a saucepan, heat the mixture over low heat and stir your hands constantly

Step 3: Stir while pouring soybean oil into the mixture Step 4: Stir while keeping the mixture boiled moderately at a rolling foam level, continue to stir well so that the main burn Pay attention not to let water fall in because if water falls, it will lead to a state of fire, fire and explosion

Step 5: After 30 minutes of cooking the mixture, check the mixture if the wax has been re-cleared

Step 6: Pour the wax into a cup and let it cool

8 - Beeswax is a colorless liquid created by worker bees when they build walls in the hive, beeswax is located below the film that surrounds the outside of the hive they are in the form of blocks consisting of many hexagonal cells on the surface

For beeswax bees act as a natural antibiotic to help protect their nests from the invasion of other organisms, to be able to make 1kg of beeswax they need to spend 3kg of honey and pollen so beeswax is considered to have many nutritional components no less than honey

- Essential oils: Essential oils are aromatic substances or odorants present in some parts of plants (seeds, roots, tubers, bark, flowers, leaves, fruits, oils, sap ) or animals (essential oil bags) The flora has essential oils of about 3000 species, of which 150-200 species have industrial significance Essential oils are present in the above raw material sources in very different concentrations, which can vary from parts per million to percent and essential oils are relatively volatile Essential oils are concentrated in several families such as canopy family, chrysanthemum, lip flower family, Camphor family, Sim family, Learn Cam, they Ginger

Essential oils are extracted from some parts of the plant such as petals, leaves, branches, roots, fruit peel, seed stalks, bark

- Candle hearts: Candle hearts are made from different materials but are usually made from cotton fibers, paper, silk threads, The size of the candle heart must be balanced with the amount of candle wax, if the heart is too small, the candle will hardly burn or not burn, if the heart is too big, it will burn quickly and may create a lot of black smoke The length of the candle heart also affects the burning speed of the candle, to maintain the burning speed and a stable flame, it is necessary to regularly observe and cut the candle heart to about 0.4cm for the

9 candle to burn slowly and limit smoke

- Candle mold: Candles are usually made of metal or glass with different shapes but most people often use cylindrical porters, aluminum porters are very light, smooth surfaces do not leave marks when pouring wax and can be reused

- In our daily life, dyes are used in many different fields Dyes are the names of organic compounds whose colors are very diverse in color and types, they have the ability to dye means to cling to color or to attach color directly to other materials Dyes are mainly used to dye materials from nature In addition, they are used to dye rubber, plastics, fats, waxes, and soaps To color the wax one uses pigment and dyes that are insoluble in water in this case the pigment is attached to the wax thanks to the film-forming agent

2.1.1.3 The effect of scented candles

Benefits of using scented candles:

The most obvious use of scented candles is to radiate incense The gentle scent of scented candles makes your home space sweet and fragrant Many types of candles are uniquely shaped and colorful, so they are often used as decorations

They can be scented candles to decorate cabinet shelves, bookshelves, desks, etc

Especially in the rainy season, your home will be prone to moldy odors, and scented candles are one of the most effective solutions for good deodorizing ability Besides deodorizing, some scented candles also work very well at repelling insects and mosquitoes

The fragrant scent from candles also has an effect on the brain to help the spirit relax and increase concentration After a stressful and tiring working day, go home to inhale the scent from your body's scented candles as if to recharge energy

10 and reduce stress caused by working too much

Domestic and foreign research works

In the process of searching for information and references, there is currently no publication that accurately describes the percentage of materials that constitute scented candles This can be explained by the trade formula security of scented candles

Currently, people produce scented candle products on a small scale or

19 medium and large scale but still use labor to produce products

2.2.2 Overview of the research situation in the world

In the world of candle culture with thousands of years of history, the habit of using candles has penetrated into the subconscious of consumers In addition to creating luxury with candles, it also has the effect of purifying the air to create romance Consumers in Europe and the United States and other regions with a developed candle culture, enter supermarkets, first displaying and selling candle products At home, candle towers in the garden, in the hallway, stairs, in the kitchen, in the bedroom In terms of production, in a small production area of 500 square meters, his company in Hong Kong produces 500 tons of products per year, while his factory in Vietnam produces 3 containers of 40 tons per month, none of which are sold in Vietnam In terms of cost, foreign-made candles are 3 times more expensive than candles produced in Vietnam

MATERIALS, RESEARCH CONTENT AND

Subjects and scope of study

3.1.1 Research subjects and research materials

● The subjects of study are:

- The process of producing and processing essential oils with the conditions (temperature, salt concentration, storage time, etc.) impacts the process

- The process of producing scented candles from some essential oils

● Materials: essential oils, soybean wax, heart candles, porters, beeswax

The chemicals used for experiments and manufacturing processes are shown in table 3.1 below

No Name of chemical Original

The equipment and instruments used for the study are shown in table 3.2 below:

Table 3.2: Research equipment and instruments

Instruments (general use for experiments|)

1 Pressure cooker 20 liters 20 Liter Vietnam

4 Gas cylinder set 13kg and safety valve Vietnam

5 Pear flask 500ml 500ml China

6 Erlenmeyer Flask 250ml 250ml China

9 Volumetric Flask 250ml 250ml China

10 Volumetric Flask 50ml 50ml China

11 Volumetric Flask 25 ml 25ml China

13 Glass pipette 10ml 10ml China

14 Glass pipette 5ml 5ml China

15 Glass pipette 2ml 2ml China

Instruments (general use for experiments|)

16 Glass pipette 1ml 1ml China

24 Flat bottom florence flask 500ml 500ml Germany

23 Along with other equipment and tools for research in the laboratory of the Department of Biotechnology and Food Technology

Scope of study location and time

Scope of laboratory-scale research

Location: laboratory of the Faculty of Biotechnology - FT

Research content

Research and develop a process for producing scented candles from some essential oils, including the following two contents:

• Content 1: Research on optimizing conditions in the scented candle production proces

Research on optimizing conditions in the production process of scented candles from natural raw materials

+ Experiment 1: The study evaluated the burning time of beeswax and soy wax

+ Experiment 2: Study the mixing ratio between beeswax and soybean wax and the burning time of candles after mixing

+ Experiment 3: Study the proportion of essential oil mixing in scented candle products

• Content 2: Development of scented candle products from natural materials

Research and manufacture scented candle products from certain essential oils

Research methodology

3.4.1 The process of separating essential oils by steam attraction method

In this study, we used steam charismatic distillation without its own boiler:

Development of essential oil extraction process:

Based on the research results optimized in section 3.1, conduct a trial production of the essential oil extraction process in the practice of household-scale and industrial-scale production:

- Producing essential oils with raw material volumes of 100 kg and 200 kg respectively

- Use a distillation system and a distillation pot corresponding to the above volume of raw materials of 220 liters and 300 liters, respectively

The stages of the distillation of essential oils from Cao Bang mandible peels are carried out with the following steps:

Materials are washed, when the shell needs to be washed to remove stains of impurities on the shell, gloves and masks must be worn when preparing to ensure the safety of specimens and people causing contamination Small research for some types of ingredients and some types of ingredients is immediately distilled

Peel off the flesh of the fruit and take only the pods

Step 2: Grind and soak the raw materials:

Crushing: Raw materials after being preliminarily processed are crushed with water so that the water/material ratio is 5/1 (v/w) Grind raw materials within 1 minute

25 Because essential oils in plants are usually located in cell tissues, grinding aims to release essential oils from the tissue so that when distillation is carried out, essential oils are easy to escape, thereby shortening the distillation process time to achieve high efficiency The smaller the grinding, the higher the efficiency of breaking cell tissues, but it is easy to clog the steam ducts (essential oil + water) and the porosity affects the distillation process Therefore, it is necessary to grind raw materials with the right size to achieve the highest performance

Immersion of raw materials: Raw materials After being crushed, it will be soaked in NaCl solution (6%) for 5 hours The purpose of this stage is to make the essential oil penetrate from the secretory sac to the outside, making the distillation process more thorough

Raw materials after being soaked will be put into the distillation equipment

So that the material is on top of the micro-support, separated from the bottom layer of the pot The raw materials contained in the device must not exceed 85% of the equipment capacity to avoid foaming, spilling into the cooling pipe, do not put the raw materials too tightly, making it difficult for steam to distribute evenly throughout the material block and not too liquid, too porous will make the vapor easy to follow the hollow places out without contact with the whole raw materials

When loading ingredients, it is necessary to cover the pot tightly to avoid evaporation and loss of essential oils during distillation Then install and install the refrigeration system

Proceed to distillation and collection of essential oil mixtures:

At the beginning of distillation essential oils can provide a large amount of

26 heat to boil distilled water After about 30 minutes the distiller starts to boil, the temperature of the steam measured at the distillation pipe reaches from 100 – 110 o C and then the boiling steam wraps the essential oil away to the refrigeration tube and follows out to the extractor we obtain a mixture of water and essential oils Essential oils lighter than water will rise out of the water, the first 1 hour of heating is the most time the essential oil comes out Then lower the temperature, maintain the pot at a sufficient boiling point because when at high temperatures the essential oil will easily decompose Therefore, it is necessary to monitor the distillation pot temperature meter and maintain it at 95-100 o C During the distillation process, attention should be paid to adjusting the condensation temperature to be in the range of 30-40 o C (by adjusting the cooling water rate) because if the condensation is too hot, it will increase the solubility of the essential oil into the water and evaporate the essential oil To check that the distillation process is finished, it is not possible to use a glass to catch a little condensate, if it is seen on the glass with oil, the distillation process is not finished

After distillation is completed, close the cooling water supply valve, turn off the stove, let it cool for 15-30 minutes, open the lid and remove the pulp, then use clean water to clean the equipment first to continue loading the ingredients to distill the new batch

Condensation: The resulting mixture of steam and essential oils enters the welding bio-tube of the distillation equipment, under the action of water contained in the low-temperature welded bio-tube, which will convert the mixture from vapor to liquid form and then flow into the condenser of the equipment

Dissociation: Let the resulting mixture remain in the condenser until it is

27 completely separated into two phases: the essential oil lighter than water will be at the top, the water will be at the bottom Open the drain valve of the extraction tank so that the essential oil flows into the catch tank to collect the crude essential oil

Develop the process of processing essential oils after storage:

Step 4: Purify essential oils - Make anhydrous: Make anhydrous with Na2SO4 because Na2S04 has the ability to absorb water Add anhydrous Na2S04 to the crude oil container, and shake it until Na2S04 salt crystals begin to come out The amount of Na2S04 depends on how much or how little water is dissociated and at our experiment the amount of anhydrous Na2S04 used was 5% (the amount of Na2S04 is residual to be able to fully absorb the water contained in the original crude essential oil)

- Strain and recover essential oils: To settle the mixture above Let the anhydrous essential oil above flow through the glass funnel with the filter paper on top, pour it slowly through the funnel, to avoid letting the essential oil flow out, there is a glass jar underneath to store essential oils

Step 5: Storage Essential oils have removed water and put them in glass jars, closed to avoid evaporation of essential oils, and avoid direct contact with light and air

The finished essential oil production process is depicted in the diagram below:

Figure 3.1: Orange essential oil production process

Figure 3.2: Essential oil distillation equipment

3.4.2 Production method of scented candles

• Preparation of equipment and materials:

+ Equipment: Crazy stove, wax cooker, thermometer, measuring cup with beak, micropipette to suck essential oils, glass chopsticks

+ Materials: soy wax, beeswax, essential oils, candle porters, candle hearts Purpose: To obtain products with stable structure and soothing scents to bring to market The method of candle production is conducted with the following sequence

+ Step 1: Prepare raw materials for soy wax, beeswax, essential oils, heart candles, mold

+ Step 3: Add essential oils and stir

+ Step 4: Pour the wax into the area

30 + Step 5: Allow to cool at room temperature

Figure 3.3: Diagram of the expected production of aromatic candles from several essential oils

3.4.3 Proposal for the production process of scented candle

Step 1: Preparation of raw materials Raw materials used for the production of aromatic candles are soy wax, beeswax, and essential oils

Take the right amount of wax to put in a glass cup and then melt it by water insulation method at a temperature of 90°C

Essential oils are added when the wax temperature is below 70°C and stir the mixture well so that the essential oil dissolves in the wax

Pour the molten wax mixture into the already candle heart

Step 5: Let the candle cool at room temperature

After cooling at room temperature we obtain a complete scented candle product

3.4.4 Experimental layout method 3.4.4.1 Content 1: Research on optimizing the conditions in the aromatic candle manufacturing process

A Research on optimizing the conditions in the production process of scented candles from natural materials

Experiment 1: Study assessing the burning time of beeswax and soy wax

This experiment aimed to find the right wax material for scented candles

Beeswax and soy wax are two materials commonly used to produce fragrance products because beeswax and soybean wax are the fuels that sustain the burning of candles Does not cause black smoke or harmful substances during combustion and has a good ability to retain and emit fragrance A few studies have shown that flames from beeswax and soybean wax produce amounts of CO2, SO2, NO, etc that are about 60% less than those produced by burning wood Use beeswax and soybean wax with less shrinkage for a flat, beautiful candle surface in just one pour Environmentally friendly, benign and safe for health, non-irritating, and not harmful to consumers' health, so I chose these two types of wax to conduct research to evaluate the burning time of each type to find the best raw materials for the scented candle production process

Figure 3.5: Diagram of the study of the burning time of two types of wax

Weigh two types of wax 10g each, then melt at a temperature of 90 o C and then pour it to obtain the candle product Cut the wicks of two equal candles and then burn them at the same time the burning time is calculated from the time the candle is burned to the time the candle is completely extinguished, we get the table below

Table 3.3: The result of obtaining the combustion time of two types of wax

Type of wax Bee wax Soy wax

The criteria for comparison between formulas is the burning time, the experiment is repeated 3 times, the total number of formulas is 6, the optimal research results are used for the following formulas

Experiment 2: Studying the mixing ratio of beeswax and soy wax

After studying the burning time of beeswax and soybean wax, we conduct an experiment to study the ratio of beeswax and soybean wax to find the right ratio of beeswax and soybean wax to obtain a product with perfect structure and relative durability When completely using soybean wax to produce candles, storage and transportation will greatly affect the product structure On the other hand, beeswax is difficult to burn, but when mixed with soybean wax, the product structure will be more stable and less affected by environmental conditions, during transportation, the product is less prone to structural changes The percentage of beeswax more or less affects the product structure and burning time

Figure 3.6: Wax ratio study diagram

Insulate each wax mixture at 90°C at a fixed ratio according to each recipe:

Data processing methods

The data collected using the above research methods is processed using Excel The results are presented in the tables in the sections in Part IV Research Results and Discussions, and the results of the detailed analysis of the experiments are shown in Appendix 2

RESULTS AND DISCUSSION

Research results on the production process of aromatic candles from

4.1.1 Research results optimize the conditions in the production process of scented candles from natural materials

4.1.1.1 Results of research on the selection of waxes for use in the production of aromatic candles

In order to study the burning time of the two types of wax, after consulting in other studies, I heated the soy wax and poured it into a mold with a candle heart and waited for it to dry then proceeded to burn and timer, beeswax did the same

Table 4.1: The result of obtaining the combustion time of two types of wax

The results of the study showed that soy burns better and the flame is larger than beeswax but beeswax is in better shape than soy wax Specifically, Table 4.1 shows that beeswax burns for a very short period of time, soy wax burns for a long time

Figure 4.1 Burning two types of wax

Type of wax Bee wax Soy wax

4.1.1.2 Results of the study on the mixing ratio of beeswax and soy wax

To study the mixing ratio of beeswax and soy wax, after studying the burning time of the two waxes in the above experiment, I mixed two types of beeswax and soy wax materials with different ratios and then proceeded to melt and pour the results obtained in Table 4.2

Table 4.2: Results of wax ratio study

Looking at the results on table 4.2 I see The higher the percentage of beeswax, the higher the state and hardness, but the shorter the burning time Specifically, when increasing the amount of beeswax and decreasing the amount of soy wax in turn, we see that the color fades and the hardness gradually increases So we decided to choose a beeswax/soybean wax ratio of 1/9 during the experiment

4.1.1.3 Results of the study on the ratio of essential oil blends in scented candle products

To study the blending ratio of essential oils into candles, after studying the burning time and blending ratio of beeswax and soybean wax, I studied the ratio of mixing essential oils with different ratios Melt the wax and add the proportional amount of essential oil to the wax at 70 oC, and let it cool to a normal temperature

The results are in Table 4.3

Beeswax/soy wax ratio Sensory

4.1.1.3 Results of the study on the ratio of essential oil blends in scented candle products

To study the blending ratio of essential oils into candles, after studying the burning time and blending ratio of beeswax and soybean wax, I studied the ratio of mixing essential oils with different ratios Melt the wax and add the proportional amount of essential oil to the wax at 70 oC, and let it cool to a normal temperature

The results are in Table 4.3

Table 4.3: results of sensory assessment of essential oil ratios

After conducting an organoleptic evaluation of the blend of cinnamon, rosemary, and orange essential oils, I obtained the results in Table 4.3 Looking at Table 4.3, I see that the ratio of mixing cinnamon essential oil and rinse at 3% (due to the fact that cinnamon essential oil and flushing are difficult to dissolve in candles) and orange essential oil in scented candles at 5% (because orange

Essential oil ratio Name of essential oil

42 essential oil is easily soluble in candles) are the candles that achieve the best status, color, and scent

4.1.2 Building the production process of scented candles

After studying the optimization of the production process conditions of aromatic candles in content 1 I used the optimized conditions to build the aromatic candle manufacturing process and initially produced a test of aromatic candles from several essential oils, then evaluated the product senses according to (Aromatic fats obtained from flowers, by the method of "cold effleurage" (namely, diffusion of aromatic compounds of flowers in fat) or by the method of "hot effleurage" (impregnating or soaking flowers in molten fat) Process development results, test products and product evaluation results are detailed in section 4.2 of Part IV results and discussion

After studying the optimization of the production process conditions of aromatic candles in content 1 I use the conditions that have been optimized to build the aromatic candle production process, the procedure of which is depicted in the diagram below:

Figure 4.2: Diagram of the production process of aromatic candles

Step 1: Preparation of raw materials

To select raw materials that meet safe quality criteria and reserve raw materials in the process of making primary raw materials in case of waste of raw materials

The raw materials used for the production of scented candles are soy wax, beeswax, essential oils, wax cookers, wax chopsticks, sap boils

Because wax is hydrophobic, it is forbidden to put water in a wax pot The

44 boiling point of water is 100oC, and the melting point of wax is 90oC, so the purpose of hydronic heating is: Keep the wax liquid without overheating leading to fire and explosion, while maintaining a stable color

Add the weighed and mixed ingredients to the water heater, stir gently and evenly to create foam during the wax heating process

Helping users concentrate, unlike sunlight or crazy light bulbs that bind the eyes, the light emitted by candles makes the eyes pleasant At the same time, the scent of candles also helps users increase their ability to concentrate, bringing a great source of energy and abundant ideas

Repelling insects, scented candles are a good remedy to repel insects especially aromatic candles that use essential oils that have antibacterial properties and prevent fungi

Essential oils are added when the wax temperature is below 70°C and stir the mixture well so that the essential oil dissolves in the wax

- The essential oil collection tool must be made of glass to avoid oxidation - Small slowly because after the candle stirs unevenly will foam

Shape the product and increase the aesthetics of the product

45 Pour the molten wax mixture into the already candle heart

- Use a candle heart clip to position the candle heart then pour it slowly into the candle heart to top it

Step 5: Let the candle cool at room temperature

In order for the wax to return to solid form, when in solid state, the wax has a very good ability to fix odors easily for storage and transportation

In the process of cooling candles, the candle must be left in a fixed place, causing vibrations that affect the final structure of the product

1 Ingredients Bee wax, soy wax, essential oil

Opt for a sturdy glass candle case

Make sure to burn scented candles only for 20 minutes to 3 hours

Keep the length of the wick appropriate

Store candles always like new

Turn off the candle when the burning wick is close to the wax

Well-preserved scented candles can be used within 2 years from the date of manufacture and if stored moderately, they can be used within 6 months from the date of manufacture

- Help the room become warmer

- Deodorize, help the room have a pleasant aroma

- Create a sense of comfort for users

- Some types can repel insects

Before burning the candle, use scissors to cut the wick to about 0.5cm, the next times of burning the candle must ensure that the candle melts evenly into a candle to prevent the heart of the candle and keep the time to radiate

6 Objects of use Be 10 years old or older 7 Contraindications Keep scented candles out of the

No Character Description reach of children and pets to avoid burns

Other notes on the packaging

Note: tested product if not certified by competent authorities

- Based on the above process, initially produce test scented candles from some essential oils:

The essential oils selected for the manufacture and evaluation of aromatic candles produced according to the above process are:

Cinnamon essential oil: cinnamon essential oil is an essential oil extracted from the bark of the cinnamon tree, cinnamon essential oil has a yellow color, a characteristic strong aroma, the main ingredient in cinnamon essential oil is cinnamic aldehyde This essential oil is widely used in daily life

Cinnamon essential oil has the use of supporting the immune system to prevent bacteria and many harmful fungi, because cinnamon essential oil has hot spicy properties and effective antibacterial ability, so cinnamon essential oil is very good for treating colds and flu Cinnamon essential oil also has the effect of deodorizing and repelling insects The aroma of cinnamon essential oil also helps the mind to be clear, comfortable, and the brain's ability to function is improved

In addition to its practical uses for health, cinnamon is also used in the medicinal and beauty care industries

48 Citronella essential oil: citronella essential oil is an essential oil extracted from the stems and leaves of the citronella tree that is most commonly used today with a gentle and pleasant scent Lemongrass essential oil is called lemongrass essential oil In which lemongrass is a plant of the lemongrass family This is a type of lemongrass native to southeast Asia

Results of development of scented candle products from natural materials 48

In this content, I researched some fragrant candle product lines that use natural aromatherapy are some essential oils that are commonly used today The

49 product lines of scented candles are manufactured according to the use of each different essential oil:

The first product line includes two types Citronella essential oil: Creates a scent with some active ingredients that repel mosquitoes: citral, geranial has a repellent effect on insects, especially against mosquitoes and ants The scent of citronella essential oil annoys many insects, keeping them away

Cinnamon essential oil: Create a scent to prevent, fight mold, Ingredients in cinnamon essential oil have cinnamaldehyde, eugenol, safrole, furfural in which the main component is cinnamaldehyde (70-80%), which determines the resistance to microorganisms of cinnamon essential oil In addition, eugenol is also an ingredient capable of inhibiting the growth of bacteria and fungal fibers

CONCLUSION AND RECOMMENDATIONS

Conclusions

The research and production of aromatic candles from some essential oils obtained the following results

• The results of the study to optimize the proportion of wax and concentration of essential oils added to scented candles are as follows

- The beeswax/soy wax ratio is 1/9 - The wax melting point is 90°C - The amount of essential oils added is 3%, some essential oils have a light scent, I raise it to 5%

• From the results achieved in the above studies, complete the process of producing scented candles from some essential oils.

Recommendations

Due to limited research time, limited internship time, there are many unfinished jobs In the coming time, I propose to carry out further research with the following contents:

1 Faraday, M and Crookes, W., 1957 The chemical history of a candle New York: Crowell

2 Sekimoto, H., Ryu, K and Yoshimura, Y., 2001 CANDLE: the new burnup strategy Nuclear science and engineering, 139(3), pp.306-317

3 Wilson-Hodge, C.A., Cherry, M.L., Case, G.L., Baumgartner, W.H., Beklen, E., Bhat, P.N., Briggs, M.S., Camaro-Arranz, A., Chaplin, V., Connaughton, V and Finger, M.H., 2011 When a standard candle flickers The

4 Mulay, Manasi R., Aditya Chauhan, Satyanarayan Patel, Viswanath Balakrishnan, Aditi Halder, and Rahul Vaish "Candle soot: Journey from a pollutant to a functional material." Carbon 144 (2019): 684-712

5 Faraday, M., 2002 The chemical history of a candle Courier Corporation

6 Hamins, Anthony, Matthew Bundy, and Scott E Dillon "Characterization of candle flames." Journal of Fire Protection Engineering 15, no 4 (2005): 265- 285

7 Fleck, J.I and Weisberg, R.W., 2004 The use of verbal protocols as data: An analysis of insight in the candle problem Memory & cognition, 32, pp.990- 1006

8 Deng, Xu, Lena Mammen, Hans-Jürgen Butt, and Doris Vollmer "Candle soot as a template for a transparent robust superamphiphobic coating." Science 335, no 6064 (2012): 67-70

52 9 Lau C, Fiedler H, Hutzinger O, Schwind KH, Hosseinpour J Levels of selected organic compounds in materials for candle production and human exposure to candle emissions Chemosphere 1997 Mar 1;34(5-7):1623-30

10 Meyer, M., Horns, D and Zechlin, H.S., 2010 The Crab Nebula as a standard candle in very high-energy astrophysics Astronomy &

11 Kang, Min Jeong, Ming Hsu, Ian M Krajbich, George Loewenstein, Samuel M McClure, Joseph Tao-yi Wang, and Colin F Camerer "The wick in the candle of learning: Epistemic curiosity activates reward circuitry and enhances memory." Psychological science 20, no 8 (2009): 963-973

12 MacKisack, Matthew, Susan Aldworth, Fiona Macpherson, John Onians, Crawford Winlove, and Adam Zeman "On picturing a candle: The prehistory of imagery science." Frontiers in Psychology (2016): 515

13 Wei, Jiaxing, Meirong Cai, Feng Zhou, and Weimin Liu "Candle soot as particular lubricant additives." Tribology Letters 53 (2014): 521-531

14 Linán, Amable, Marcos Vera, and Antonio L Sánchez "Ignition, liftoff, and extinction of gaseous diffusion flames." Annual Review of Fluid

15 Griffiths, John F., and John Allan Barnard Flame and combustion CRC Press, 1995.

Ngày đăng: 02/07/2024, 05:49

Nguồn tham khảo

Tài liệu tham khảo Loại Chi tiết
1. Faraday, M. and Crookes, W., 1957. The chemical history of a candle. New York: Crowell Sách, tạp chí
Tiêu đề: The chemical history of a candle
2. Sekimoto, H., Ryu, K. and Yoshimura, Y., 2001. CANDLE: the new burnup strategy. Nuclear science and engineering, 139(3), pp.306-317 Sách, tạp chí
Tiêu đề: Nuclear science and engineering, 139
3. Wilson-Hodge, C.A., Cherry, M.L., Case, G.L., Baumgartner, W.H., Beklen, E., Bhat, P.N., Briggs, M.S., Camaro-Arranz, A., Chaplin, V., Connaughton, V. and Finger, M.H., 2011. When a standard candle flickers. TheAstrophysical Journal Letters, 727(2), p.L40 Sách, tạp chí
Tiêu đề: The "Astrophysical Journal Letters, 727
6. Hamins, Anthony, Matthew Bundy, and Scott E. Dillon. "Characterization of candle flames." Journal of Fire Protection Engineering 15, no. 4 (2005): 265- 285 Sách, tạp chí
Tiêu đề: Characterization of candle flames
Tác giả: Hamins, Anthony, Matthew Bundy, and Scott E. Dillon. "Characterization of candle flames." Journal of Fire Protection Engineering 15, no. 4
Năm: 2005
7. Fleck, J.I. and Weisberg, R.W., 2004. The use of verbal protocols as data: An analysis of insight in the candle problem. Memory & cognition, 32, pp.990- 1006 Sách, tạp chí
Tiêu đề: Memory & cognition, 32
8. Deng, Xu, Lena Mammen, Hans-Jürgen Butt, and Doris Vollmer. "Candle soot as a template for a transparent robust superamphiphobic coating." Science 335, no. 6064 (2012): 67-70 Sách, tạp chí
Tiêu đề: Candle soot as a template for a transparent robust superamphiphobic coating
Tác giả: Deng, Xu, Lena Mammen, Hans-Jürgen Butt, and Doris Vollmer. "Candle soot as a template for a transparent robust superamphiphobic coating." Science 335, no. 6064
Năm: 2012
10. Meyer, M., Horns, D. and Zechlin, H.S., 2010. The Crab Nebula as a standard candle in very high-energy astrophysics. Astronomy &Astrophysics, 523, p.A2 Sách, tạp chí
Tiêu đề: Astronomy & "Astrophysics, 523
11. Kang, Min Jeong, Ming Hsu, Ian M. Krajbich, George Loewenstein, Samuel M. McClure, Joseph Tao-yi Wang, and Colin F. Camerer. "The wick in the candle of learning: Epistemic curiosity activates reward circuitry and enhances memory." Psychological science 20, no. 8 (2009): 963-973 Sách, tạp chí
Tiêu đề: The wick in the candle of learning: Epistemic curiosity activates reward circuitry and enhances memory
Tác giả: Kang, Min Jeong, Ming Hsu, Ian M. Krajbich, George Loewenstein, Samuel M. McClure, Joseph Tao-yi Wang, and Colin F. Camerer. "The wick in the candle of learning: Epistemic curiosity activates reward circuitry and enhances memory." Psychological science 20, no. 8
Năm: 2009
12. MacKisack, Matthew, Susan Aldworth, Fiona Macpherson, John Onians, Crawford Winlove, and Adam Zeman. "On picturing a candle: The prehistory of imagery science." Frontiers in Psychology (2016): 515 Sách, tạp chí
Tiêu đề: On picturing a candle: The prehistory of imagery science
Tác giả: MacKisack, Matthew, Susan Aldworth, Fiona Macpherson, John Onians, Crawford Winlove, and Adam Zeman. "On picturing a candle: The prehistory of imagery science." Frontiers in Psychology
Năm: 2016
13. Wei, Jiaxing, Meirong Cai, Feng Zhou, and Weimin Liu. "Candle soot as particular lubricant additives." Tribology Letters 53 (2014): 521-531 Sách, tạp chí
Tiêu đề: Candle soot as particular lubricant additives
Tác giả: Wei, Jiaxing, Meirong Cai, Feng Zhou, and Weimin Liu. "Candle soot as particular lubricant additives." Tribology Letters 53
Năm: 2014
14. Linán, Amable, Marcos Vera, and Antonio L. Sánchez. "Ignition, liftoff, and extinction of gaseous diffusion flames." Annual Review of FluidMechanics 47 (2015): 293-314 Sách, tạp chí
Tiêu đề: Ignition, liftoff, and extinction of gaseous diffusion flames
Tác giả: Linán, Amable, Marcos Vera, and Antonio L. Sánchez. "Ignition, liftoff, and extinction of gaseous diffusion flames." Annual Review of FluidMechanics 47
Năm: 2015
15. Griffiths, John F., and John Allan Barnard. Flame and combustion. CRC Press, 1995 Sách, tạp chí
Tiêu đề: Flame and combustion

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