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BỘ GIÁO DỤC VÀ ĐÀO TẠO TRƯỜNG ĐẠI HỌC SƯ PHẠM KỸ THUẬT THÀNH PHỐ HỒ CHÍ MINH ĐỒ ÁN TỐT NGHIỆP NGÀNH CNKT HÓA HỌC VI BAO TINH DẦU QUẾ BẰNG PHỨC ĐA ĐIỆN TÍCH GIỮA GELATIN VÀ MỦ TRÔM THỦY PHÂN GVHD: PGS TS NGUYỄN VINH TIẾN SVTH: NGUYỄN HỒNG VŨ PHÚC SKL008819 Tp.Hồ Chí Minh, tháng 8/2022 h BỘ GIÁO DỤC VÀ ĐÀO TẠO TRƯỜNG ĐẠI HỌC SƯ PHẠM KỸ THUẬT TP HỒ CHÍ MINH KHOA CƠNG NGHỆ HÓA HỌC VÀ THỰC PHẨM - - LUẬN VĂN TỐT NGHIỆP VI BAO TINH DẦU QUẾ BẰNG PHỨC ĐA ĐIỆN TÍCH GIỮA GELATIN VÀ MỦ TRƠM THỦY PHÂN SVTH: Nguyễn Hồng Vũ Phúc MSSV: 18128048 GVHD: PGS TS Nguyễn Vinh Tiến Tp Hồ Chí Minh, tháng 08 năm 2022 h h h h h h 37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.C.33.44.55.54.78.655.43.22.2.4.55.2237.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.66 h 37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.99 37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.C.33.44.55.54.78.655.43.22.2.4.55.2237.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.66 TÓM TẮT Trong nghiên cứu này, tiến hành vi bao tinh dầu quế phức đa điện tích mủ trôm gelatin nhằm hạn chế biến đổi không mong muốn kéo dài thời gian bảo quản tinh dầu quế Q trình hình thành phức mủ trơm – gelattin tối ưu pH khoảng 3.4 – 3.8 với tỉ lệ polymer 1:1, xác định thông qua độ đục, zeta hiệu suất thu hồi phức Sau đó, chúng tơi tiến hành khảo sát q trình vi bao tinh dầu quế phức tỷ lệ vỏ : nhân 1:1, 2:1, 4:1 8:1 phương pháp sấy đối lưu sấy thăng hoa Chúng thực đo phổ hồng ngoại FTIR, hiêu suất vi bao, đo kính hiển vi để chứng minh tinh dầu vi bao gelatin – mủ trôm Kết nghiên cứu cho thấy, hiệu suất thu hồi bột vi bao cao mẫu có tỷ lệ vỏ : nhân 8:1 75.03% Đồng thời, mẫu thể lượng tinh dầu bề mặt, dầu lại dung dịch hiệu suất vi bao tinh dầu 3.14%, 24.14% 72.11% Các mẫu sau vi bao thể khả hòa tan khả trương nở tốt Cụ thể mẫu có tỷ lệ 1:1 có khả hịa tan tốt cịn mẫu có tỷ lệ 8:1 có khả trương nở tốt i h 37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.99 37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.C.33.44.55.54.78.655.43.22.2.4.55.2237.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.66 LỜI CẢM ƠN Để hoàn thành q trình nghiên cứu hồn thiện luận văn, lời xin chân thành cảm ơn sâu sắc đến quý thầy cô môn kỹ thuật hố học thuộc khoa Cơng Nghệ Hóa Thực Phẩm trường Đại học Sư Phạm Kỹ Thuật Thành phố Hồ Chí Minh tạo điều kiện sở, vật chất cho học tập nghiên cứu trường Cảm ơn thầy nhiệt tình giảng dạy, truyền đạt kiến thức tảng cho suốt năm học Đặc biệt, xin bày tỏ lòng biết ơn sâu sắc đến thầy TS Nguyễn Vinh Tiến tận tình bảo, hướng dẫn, truyền đạt kinh nghiệm kiến thức chuyên môn kỹ cần thiết để chúng tơi thực thí nghiệm cách hiệu Ngồi ra, xin chân thành cảm ơn gia đình, bạn bè ln động viên, giúp đỡ chúng tơi mặt suốt thời gian qua Vì kiến thức kinh nghiệm hạn hẹp nên luận văn tránh khỏi sai sót Kính mong thầy thơng cảm bỏ qua sai sót tơi mong nhận góp ý từ q thầy để đề tài chúng tơi hồn thiện Một lần nữa, xin chân thành cảm ơn q thầy cơ, gia đình bạn bè bên cạnh suốt thời gian qua ii h 37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.99 37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.C.33.44.55.54.78.655.43.22.2.4.55.2237.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.66 CHƯƠNG 4: KẾT LUẠN VÀ KIẾN NGHỊ 4.1 Kết luận Tinh dầu quế hợp chất nhạy với yếu tố môi trường nhiệt độ, ánh sáng,,… tính kỵ nước mùi tinh dầu quế yếu tố quan trọng ứng dụng vào thực tế Vì lý này, mà tinh dầu quế phân tán vào nước với có mặt có tween 80 bao bọc lớp vỏ polymer Kết nghiên cứu cho thấy, việc bao lại phức gelatin – mủ trôm có khả bao lượng tinh dầu tốt với suất cao Đồng thời việc vi bao giúp tinh dầu quế hạn chế bị oxy hóa nhiệt độ Ngồi ra, tinh dầu quế cịn ứng dụng đời sống như: kháng khiển, kháng nấm, chống đái tháo đường, thuốc diệt trùng muỗi, diệt côn trùng 4.2 Kiến nghị Bên cạnh kết khảo sát thời gian tìm hiểu, thực hành điều kiện máy móc, thiết bị khơng cho phép, phạm vi nghiên cứu cịn hạn chế Vi chúng tơi kiến nghị sau để mở rộng phâm vi nghiên cứu: - Sử dụng phương pháp sấy lạnh sấy nhiệt độ thấp để hạn chế mức độ oxy hóa tinh dầu quế - Đo thêm số phép đo TGA, DSC để xác định thêm tính chất bột vi bao - Chụp SEM, TEM tất tỷ lệ để thấy rõ cấu trúc bên ngồi lẫn bên để nhìn trực quan hiệu vi bao - Tinh dầu quế thay số loại tinh dầu khác tinh dầu tràm, tình dầu bạc hà, tinh dầu gừng,… 82 h 37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.99 37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.C.33.44.55.54.78.655.43.22.2.4.55.2237.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.66 DANH MỤC TÀI LIỆU THAM KHẢO Zeta Potential An Introduction in 30 Minutes Aziz, A., A Jusoh, R Mamat and A A Abdullah (2014) "Effect of Water Content and Tween 80 to the Stability of Emulsified Biodiesel." 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Polymer Bulletin 77(10): 5227-5244 84 h 37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.99 37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.C.33.44.55.54.78.655.43.22.2.4.55.2237.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.66 28 Popelka, A., I Novak, M Lehocky, I Chodak, J Sedliacik, M Gajtanska, M Sedliacikova, A Vesel, I Junkar, A Kleinova, M Spirkova and F Bilek (2012) "Anti-bacterial treatment of polyethylene by cold plasma for medical purposes." 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Food Control 123: 107783 85 h 37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.99 37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.C.33.44.55.54.78.655.43.22.2.4.55.2237.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.66 PHỤ LỤC Phụ lục Thế zeta gelatin, mủ trôm thủy phân phức gelatin – mủ trôm thủy phân dung dịch pH Gelatin Mủ trôm thủy phân Phức gelatin – mủ trôm thủy phân 2.5 17.22 - 4.723 - 8.675 3.0 16.07 - 11.55 - 6.28 3.5 17.2 - 30.81 - 3.844 4.0 14.52 - 37.61 - 12.36 4.5 11.65 - 48.24 - 18.32 5.0 5.706 - 68.69 - 25.31 5.5 - 0.094 - 80.58 - 48.57 6.0 - 5.087 - 83.13 - 58.91 6.5 - 7.273 - 87.01 - 65.25 7.0 - 7.614 - 94.38 - 67.86 7.5 - 8.642 - 95.5 - 68.65 8.0 - 9.674 - 97.13 - 71.2 8.5 - 10.78 - 106.12 - 80.77 86 h 37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.99 37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.C.33.44.55.54.78.655.43.22.2.4.55.2237.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.66 Phụ lục Khi chuẩn độ acid sau chuẩn độ base Độ lệch chuẩn pH Độ hấp thụ 10.812 0.001 0.003 9.772 0.002 0.002 7.823 0.003 0.001 7.072 0.003 0.001 5.860 0.005 0.0032 5.590 0.012 0.002 5.220 0.069 0.006 5.115 0.138 0.015 5.022 0.262 0.012 4.935 0.483 0.005 4.858 0.932 0.001 4.805 1.16 0.001 4.745 1.286 0.001 4.634 1.325 0.002 4.564 1.308 0.002 4.454 1.248 0.02 4.345 1.264 0.08 4.227 0.801 0.083 4.104 0.397 0.075 3.658 0.045 0.003 3.254 0.351 0.01 3.046 0.018 0.004 2.400 0.012 0.005 (STD) 87 h 37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.99 37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.C.33.44.55.54.78.655.43.22.2.4.55.2237.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.66 Độ lệch chuẩn pH Độ hấp thụ 2.400 0.012 0.005 3.063 0.015 0.01 3.273 0.02 0.015 3.545 0.472 0.001 3.722 0.615 0.003 3.95 0.522 0.04 4.175 0.466 0.036 4.43 0.827 0.011 4.681 0.987 0.01 4.96 0.486 0.006 5.29 0.079 0.001 5.341 0.093 0.002 6.03 0.045 0.004 9.257 0.039 0.002 10.323 0.041 0.001 10.812 0.038 0.003 (STD) 88 h 37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.99 37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.C.33.44.55.54.78.655.43.22.2.4.55.2237.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.66 Phụ lục Chuẩn độ base sau chuẩn độ acid Độ lệch chuẩn pH Độ hấp thụ 2.505 0.015 0.001 2.965 0.017 0.006 3.011 0.139 0.003 3.56 0.125 0.011 3.877 0.154 0.003 3.906 0.192 0.017 4.036 0.214 0.004 4.155 0.264 0.032 4.3 0.384 0.026 4.477 0.342 0.021 4.525 0.306 0.009 4.827 0.187 0.001 4.895 0.166 0.002 5.105 0.133 0.001 5.685 0.075 0.001 6.088 0.073 0.001 6.538 0.072 0.003 6.994 0.073 0.005 7.07 0.076 0.002 7.535 0.081 0.009 7.958 0.079 0.001 8.061 0.085 0.003 8.453 0.096 0.002 8.973 0.097 0.002 9.971 0.092 0.003 (STD) 89 h 37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.99 37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.C.33.44.55.54.78.655.43.22.2.4.55.2237.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.66 Độ lệch chuẩn pH Độ hấp thụ 10.347 0.087 0.001 9.865 0.079 0.003 9.079 0.081 0.009 8.44 0.084 0.001 7.94 0.083 0.003 7.634 0.085 0.008 0.087 0.008 6.634 0.089 0.004 6.166 0.096 0.007 5.511 0.101 0.001 5.075 0.107 0.001 4.93 0.105 0.003 4.87 0.11 0.006 4.705 0.113 0.006 4.64 0.117 0.005 4.56 0.185 0.005 4.42 0.186 0.005 4.354 0.192 0.001 4.19 0.205 0.004 4.035 0.209 0.004 3.926 0.215 0.002 3.848 0.215 0.001 3.742 0.212 0.001 3.653 0.215 0.003 3.502 0.226 0.002 3.017 0.221 0.002 2.501 0.213 0.005 2.018 0.213 0.003 (STD) 90 h 37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.99 37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.C.33.44.55.54.78.655.43.22.2.4.55.2237.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.66 Phụ lục Hiệu suất thu hồi phức mủ trôm – gelalin tỷ lệ polymer khác pH 3.4 3.5 3.6 3.7 3.8 Tỷ lệ Khối lượng Khối lượng Hiệu suất thu hồi gelatin – mủ đĩa petri đĩa petri sau phức trôm trước sấy sấy gelatin – mủ trôm 1:4 39.1378 39.4095 45.28333 1:2 39.0434 39.4414 66.33333 1:1 41.1205 41.5826 77.01667 2:1 48.1658 48.6721 84.38333 4:1 39.133 39.3593 37.71667 1:4 39.2604 39.4334 28.83333 1:2 39.3863 39.6661 46.63333 1:1 44.5402 44.9418 66.93333 2:1 39.2831 39.6696 64.41667 4:1 39.2059 39.3902 30.71667 1:4 39.2709 39.4715 33.43333 1:2 39.2388 39.5618 62.63333 1:1 39.2907 39.7279 72.86667 2:1 41.7213 42.0703 58.16667 4:1 49.1709 49.3353 27.4 1:4 38.9909 39.2208 38.31667 1:2 39.13 39.4873 59.55 1:1 39.29 39.748 76.33333 2:1 39.1222 39.439 52.8 4:1 39.1038 39.2328 21.5 1:4 39.2843 39.5456 43.55 1:2 39.2384 39.6292 65.13333 1:1 41.1911 41.6437 75.43333 2:1 39.3879 39.6631 45.86667 4:1 41.7227 41.8478 20.85 91 h 37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.99 37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.C.33.44.55.54.78.655.43.22.2.4.55.2237.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.66 Phụ lục Ảnh hưởng nhiệt độ đến hình thành phức polyelectrolyte mủ trôm gelatin Nhiệt độ (oC) Độ hấp thụ (600nm) Độ lệch chuẩn (STD) 10 2.18367 0.04028 20 1.97667 0.039 30.5 1.82 0.00173 40 1.66067 0.00751 49 1.636 0.007 60 1.59167 0.01914 70 1.489 0.013 79 1.10767 0.00551 Phụ lục pH dung dịch phức mủ trôm – gelatin thay đổi theo thời gian ảnh hưởng glucono-δ-lactone pH Abs (600nm) Thời gian (h) Độ lệch chuẩn (STD) 4.621 0.512 0.013 3.957 1.223 0.005 3.8 0.34 0.035 3.719 0.156 0.03 3.675 0.201 0.008 3.65 0.037 0.017 3.633 0.016 0.002 3.618 0.02 0.004 3.598 0.027 0.001 3.58 0.025 0.002 3.563 0.033 10 0.002 3.544 0.034 11 0.003 92 h 37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.99 37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.C.33.44.55.54.78.655.43.22.2.4.55.2237.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.66 Phụ lục Hiệu suất vi bao, hiệu suất thu hồi hàm lượng tinh dầu có bề mặt bột phức dung dịch Tỷ lệ Tinh dầu Tinh dầu lại Hiệu suất vi bao Hiệu suất vỏ:nhân bề mặt dung dịch tinh dầu thu hồi 1:1 10.64 55.19 34.07 53.041 2:1 9.25 46.89 42.86 57.966 4:1 5.06 33.42 61.32 65.046 8:1 3.14 24.15 72.11 75.03 Phụ lục Độ tan bột vi bao pH = 2, Sấy đối lưu Tỷ lệ pH = vỏ:nhân pH = pH =6 1:1 43.10 44.80 43.60 37.72 36.75 36.43 44.88 47.07 45.42 2:1 41.10 42.30 40.80 30.21 31.01 31.25 41.84 42.26 41.68 4:1 39.50 38.20 37.40 28.00 29.11 27.29 40.35 39.42 39.78 8:1 31.10 32.10 30.40 25.87 26.10 24.79 32.32 33.11 33.26 Sấy thăng hoa pH = pH = pH =6 1:1 47.70 46.10 45.60 39.94 39.53 38.64 45.90 46.07 46.74 2:1 43.20 44.60 44.20 34.27 34.44 35.32 45.90 45.25 46.12 4:1 43.10 43.50 42.50 34.00 34.72 34.40 43.85 42.50 44.06 8:1 37.80 35.60 36.70 27.69 27.14 28.63 37.31 37.87 37.56 93 h 37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.99 37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.C.33.44.55.54.78.655.43.22.2.4.55.2237.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.66 Phụ lục Độ tan mẫu bột vi bao theo nhiệt độ (oC) Sấy đối lưu Tỷ lệ vỏ:nhân t = 30oC t = 60oC t = 90oC 1:1 8.61 9.70 7.50 11.44 10.01 12.86 13.28 13.24 13.32 2:1 5.71 5.60 5.80 6.93 6.31 7.53 8.41 8.07 8.73 4:1 3.09 3.80 2.40 5.64 5.47 5.80 6.46 5.96 6.94 8:1 2.14 1.80 2.50 3.41 3.78 3.05 4.48 4.38 4.55 Sấy thăng hoa t = 30oC t = 60oC t = 90oC 1:1 9.23 9.88 8.51 12.68 13.67 11.70 14.44 15.81 13.10 2:1 6.62 6.41 6.32 8.06 8.21 7.89 9.14 10.12 8.13 4:1 4.27 4.04 4.17 5.98 5.42 6.55 7.26 7.80 6.73 8:1 3.36 3.19 3.26 4.64 5.32 3.95 5.70 4.41 7.02 94 h 37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.99 37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.C.33.44.55.54.78.655.43.22.2.4.55.2237.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.66 Phụ lục 10 Độ trương nở mẫu bột vi bao nước Tỷ lệ Độ trương nở nước (%) vỏ:nhân Lần Lần Lần 1:1 53.85 58.23 50.31 2:1 122.73 126.75 118.34 4:1 146.67 150.14 141.25 8:1 234.00 239.34 229.64 95 h 37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.55.77.77.99.44.45.67.22.55.77.C.37.99.44.45.67.22.99 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