ad7fead0-d431-4565-8e14-f82f9143a89f-oral-sessions-pp-7.21.-2014

2014 EAS Preliminary Technical Oral Program    2014 Preliminary Technical Oral Program MONDAY MORNING, NOVEMBER 17 Time Title, Author(s) American Microchemical Society Benedetti-Pichler Award Honoring Gene Hall, Rutgers University Session Chair: Robert Vetricin 9:00 Finger Prick Blood Analysis: The Omega-3 Index, Ken D Stark, University of Waterloo Forensic DNA Analysis: The Gold Standard for Criminal Investigation of Biological Evidence, Lawrence 9:30 Kobilinsky, John Jay College 10:00 Break 10:20 Doing a Lot with a Little: Ambient Ionization and Microchemistry, Robert B Cody, Jeol USA Inc Chemical Microscopy for the 21st Century: Surface-Enhanced Raman Microspectroscopy for the 10:50 Ultrasensitive Detection of Organic Colorants, Marco Leona, The Metropolitan Museum of Art From Archimedes Palimpsest to Water Analysis: My 35 Years of Instrumental Analytical Chemistry at 11:20 Rutgers, Gene S Hall, Rutgers University New York Section of the Society for Applied Spectroscopy Gold Medal Award Honoring Larry A Nafie, Syracuse University Session Chair: Deborah A Peru, Colgate-Palmolive Co Vibrational Optical Activity: An Established Tool for Research and Routine Analytical Applications, 9:00 Laurence A Nafie, Syracuse University Two-Dimensional Correlation Spectroscopy in Materials Development, Isao Noda, University of 9:30 Delaware 10:00 Break Electrospun PHA (polyhydroxyalkanoate) Fibers: Influence of Processing on Structure, Bruce Chase, 10:20 Liang Gong, Isao Noda, John Rabolt, University of Delaware UV Resonance Raman Spectroscopic Studies of Protein Structure and Dynamics, Sanford (Sandy) A 10:50 Asher, University of Pittsburgh Quality Control and Bioanalysis of Protein Therapeutics Chair: Naidong Weng, Janssen Application of UPLC-High Resolution MS in Drug Product Comparability Studies, Pilsoo Kang, Jianmei 9:00 Kochling, Yimin Hua, Robert W Donaldson, Genzyme Quality-by-Design Method Development of the 2nd Generation Peptide Map Assays for Therapeutic 9:20 Proteins, Yimin Hua, Francisca Gbormittah, Alekhya Pochiraju, Qian Guan, Robert W Donaldson, Jianmei Kochling, Genzyme A Novel HILIC Column for the High Speed Analysis of N-Linked Glycans, James Martosella, Oscar 9:40 Potter, Jia Liu, Agilent Technologies 10:00 Break The Influence of Biocompatible Coating Thickness of Non-porous Polymer Beads on Protein Recoveries 10:20 and Resolution, Michael Lu, BioChrom Labs Development, Validation and Comparison of a Competitive Ligand Binding and a Functional Cell-Based 10:40 Assay for Neutralizing Antibody (NAb) Detection, Weifeng Xu, Michael Sank, Jennifer Cummings, Xuefeng Li, Robert Dodge Renuka Pillutla, Binodh DeSilva, Merck Okra Seed Phytochemicals: Potential Treatments for Glycemic Control and Regulators of Enzyme 11:00 Cholesterol 7-alpha-Hydroxylase in Bile Acid Biosynthesis, Bishambar Dayal, Rutgers Medical School As of July 21, 2014 2014 EAS Preliminary Technical Oral Program    Monday Morning Continued Elemental Impurities in Pharmaceuticals: Requirements, Applications, Techniques Chair: Nancy Lewen, Bristol-Myers Squibb Pilot Study for Using Portable XRF for Screening for Elemental Impurities, James Morykin, Bristol-Myers 9:00 Squibb Determination of Elemental Impurities: A Practical Approach from a Contract Lab, Samina Hussain, 9:30 Exova 10:00 Break Method Development and Validation for the Quantification of Elemental Impurities in Large and Small 10:20 Molecule Drug Substance and Drug Product, Timothy Shelbourn, Eli Lilly An Update on General Chapters and and Implementation Timelines, Kahkashan Zaidi, 10:50 United States Pharmacopeia Microscopy and Microanalysis for Cultural Heritage, Part I, organized with the New York Conservation Foundation and New York Microscopical Society Chair: John Scott, NYCF Simple Magnification, Optical Phase Contrast Microscopy, and Desktop SEM-EDS: Characterizing a 9:00 Cleaning Agent, John Scott, New York Conservation Foundation SEM-EDS and Multi-Instrumental Analysis: Studying the Corrosion of Ag 999 and Ag 925 Inside and 9:30 Outside Vitrines, Paula Homem, Universidade Porto 9:50 Break Accessible Microanalysis in Authentication and Attribution: A Case Study, Soraya Alcalá, Hèléne 10:10 Fontoira, The Hispanic Society of America, Thiago Assan Piwowazrczyk, Marcelo Myada Redígolo, Interface Research Analysis Solutions 10:40 Scientific Analysis of Pietro da Cortona’s The Triumph of David, Kristen E Watts, Amanda Norbutus, Anthony Lagalante, Villanova University, Kristin deGhetaldi, University of Delaware Morphology of Fungal Stains on Paper Characterized With Multi-Scale and Multi-Sensory Surface 11:00 Metrology, Hanna M Szczepanowska, Smithsonian Institution, Brian Renegar, National Institute of Standards and Technology Analysis of Textiles and Other Materials Chair: Sandra Ferris, The Dow Chemical Company Investigation of Body Products on Worn Clothing Substrate Found at a Fire Scene Conflicting with 9:00 Ignitable Liquid Residue Identification by GC/MS, Gina M Guerrera, Brooke W Kammrath, University of New Haven, Erika Chen, Michael Valetutti, New York City Police Department Differentiation of Human, Animal, and Synthetic Hair by ATR FTIR Spectroscopy, Jeremy M Manheim, 9:20 Kyle Doty, Greg Mclaughlin, Igor K Lednev, University at Albany Quantitation of Dyes in Forensic Fibers Using UHPLC-TOF MS and Building a Dye Database with 9:40 AxION EC ID Software, Sharanya Reddy, Joanne Mather, Bonnie Marmor, PerkinElmer 10:00 Break Characterization of the Binding Medium Used in Roman Encaustic Paintings on Wall and Wood, Ruben 10:20 M Savizky, John L Bove, Pedro Cuni, Jorge Cuni, Brielle Eisen, The Cooper Union Structural Characterization of Manmade Fiber Using Fluorescence Microscopy and Image Analysis, 10:40 Shailesh P Nagarkar, Prasad Panzade, Aditya Birla Science and Technology Company Non-Destructive Testing with Ultrasound and Visual Inspection, an Approach to Historic Buildings, Eloisa 11:00 Dezen-Kempter, Gisleiva C S Ferreira, State University of Campinas Differentiating Authentic from Counterfeit Drugs by Raman Microscopy, Fran Adar, HORIBA Scientific, 11:20 Pauline E Leary, The Graduate Center, City University of New York, John A Reffner, John Jay College Handheld Vibrational Spectrometers and Imagers: Innovations and Novel Applications Chair: Heinz W Siesler, University of Duisburg-Essen Fit-for-Purpose Miniature NIR Spectroscopy for Solid Dosage Continuous Manufacturing, Krizia Karry, 9:00 Rutgers University The Next Generation of Long Wavelength Handheld Raman Spectrometers for Raw Material Inspection 9:30 and Beyond, Claire Dentinger, Rigaku Raman Technologies 10:00 Break 10:20 Mixture Analysis Using Handheld Raman Spectrometer, Dawn Yang, B&W Tek Miniaturized Multi-Spec (UV-NIR, Raman and Hyperspectral) Instruments in Practical In-Situ Analysis, 10:50 Fredrick Haibach, BaySpec As of July 21, 2014 2014 EAS Preliminary Technical Oral Program    Monday Morning Continued Process Analysis and Instrumentation Chair: Yuwen Wang, Boehringer Ingelheim Off-Line and In-Line Monitoring of Mulling Processes, Savitha S Panikar, Suyang Wu, Benjamin J 9:00 Glasser, Rohit Ramachandran, Rutgers University Achieving Greater Process Understanding Through On-Line Reaction Monitoring, Michael L Hall, Nancy 9:20 L Jestel, Eylem Tarkin-Tas, Mark Denniston, Carolyn Degonzague, SABIC In-Line PAT Method Development for Flowing Pharmaceutical Blend Homogeneity Monitoring, Fan 9:40 Zhang-Plasket, John P Higgins, Cat MacConnell, Mano Ramasamy, Robert F Meyer, Charles E Miller, Jennifer Pai, Merck 10:00 Break NIR Analyses in the Field; how to get better Answers, Franklin E Barton, James A de Haseth, Light 10:20 Light Solutions Instruments High-Throughput Virtual Slit Technology: Benefits for Polymer Extrusion, Yusuf Bismilla, Jeffrey T 10:40 Meade, Bradford B Behr, Andrew T Cenko, Brandon DesRoches, Jared Slaa, Arsen R Hajian, Tornado Spectral Systems Innovative Practices in Analytical Testing Chair: Richard B Nguyen, Merial Analytical Testing for the Cannabis Industry: A New Era Presents New Opportunities, Christopher J 9:00 Hudalla, Nathan M LaCroix, ProVerde Laboratories Impact of Method Robustness to the Success of Product Commercialization - Lesson Learned, Xin Bu, 9:20 John Castoro, Joel Young, Bristol-Myers Squibb Incorporation of Benchtop NMR Spectroscopy into Undergraduate Laboratories: An Active-Learning 9:40 Approach, Susanne Riegel, Nanalysis 10:00 Break Analytical Pipetting of Serum and Serum-Like Liquids, John T Bradshaw, Richard H Curtis, Rachel 10:20 Parshley, Artel Inc 10:40 S.M.A.R.T Laboratory Practices, Julius Neil Buenconsejo, Keppel Seghers Engineering Taking the Pain Out of Chromatographic Peak Integration, Peter Bodsky, Shaun Quinn, Thermo Fisher 11:00 Scientific Innovative Approach to Helium Carrier Gas Conservation in Analytical Gas Chromatography, Lori Dolata, 11:20 Edward B McCauley, Massimo Santoro, Paolo Magni, Alexander N Semyonov, Thermo Fisher Scientific Automated, Rapid, Reliable Determination of Dissolved Gases in Water by Static Headspace Gas 11:40 Chromatography, Lori Dolata, Andrea Caruso, Richard Jack, Massimo Santoro, Thermo Fisher Scientific NMR Spectroscopy of Molecules Small and Large: Methods and Applications, Part I Chair: Bernie O'Hare, Bruker Assessing Qualitative and Quantitative NMR Limits in a Drug Metabolism Environment, Gregory Walker, 9:00 Pfizer Pulsed Field Gradient Nuclear Magnetic Resonance (PFGNMR) Studies of Nanoparticle Surfaces and 9:30 their Interactions, Kebede Beshah, Aslin Izmitli, Antony Van Dyk, The Dow Chemical Company 10:00 Break High-Throughput Screening of Solid Pharmaceuticals with 35Cl Solid-State NMR, Robert W Schurko, 10:20 Michael J Jaroszewicz, Anthony R Sandre, Andrew M Namespetra, Kristopher J Harris, University of Windsor, Adonis Lupulescu, Lucio Frydman, Weizmann Institute 10:40 Strategies to Enhance the Sensitivity and Reduce the Ambiguity of NMR Spectra of Complex Biological Assemblies, Galia Debelouchina, Princeton University Understanding the Behavior of Different Tablet Disintegrants Using High-Resolution FLASH Magnetic 11:00 Resonance Imaging, Anuji Abraham, Dolapo Olusanmi, David Good, Denette Murphy, Daniel McNamara, Venkatramana Rao, Bristol-Myers Squibb, Andrew J Ilott, Alexej Jerschow, New York University As of July 21, 2014 2014 EAS Preliminary Technical Oral Program    MONDAY AFTERNOON, NOVEMBER 17 EAS Award for Outstanding Achievements in the Fields of Analytical Chemistry Honoring Joseph A Caruso, University of Cincinnati Sponsored by Bristol-Myers Squibb Session Chair: William R Heineman, University of Cincinnati Plenary Lecture and Awards Presentation to Joseph Caruso, University of Cincinnati, immediately follow this session New Sources for Ambient Desorption/Ionization Mass Spectrometry, Gary M Hieftje, Jacob T Shelley, 2:00 Steven J Ray, Kevin P Pfeuffer, Indiana University, Gregory T Schilling, Leco Corp The Liquid Sampling-Atmospheric Pressure Glow Discharge (LS-APGD) Microplasma: An Example of 2:30 What I Learned from Joe Caruso - Its More Fun Living (a little) Outside of the Box, R Kenneth Marcus, Clemson University 3:00 Break Plasma Sources Pushing the Limits in Analytical Chemistry, David W Koppenaal, Pacific Northwest 3:20 National Laboratory Spectroelectrochemistry as a Strategy for Improving Sensor Selectivity, William R Heineman, University 3:50 of Cincinnati, Samuel A Bryan, Pacific Northwest National Laboratory 4:30 Presentation of the EAS Award in the Fields of Analytical Chemistry From Solution Chemistry to Mass Spectrometry – My Fields of Analytical, Joseph A Caruso, University 4:35 of Cincinnati Development of Pharmaceutical Generics: Analytical Challenges Chairs: Leonel M Santos, United States Pharmacopeia and Kim Huynh-Ba, Pharmalytik 2:00 Key Issues of Generic Drug Development, Saji Thomas, Par Pharmaceuticals 2:30 Stability Requirements of ANDA Products, Kim Huynh-Ba, Pharmalytik 3:00 Break 3:20 Advances on the Modernization of USP Monographs, Leonel Santos, US Pharmacopeia Comparison of Dissolution Profiles Including Bioequivalence, Method Transfer/Validation, and f2, Vivian 3:50 Gray, V A Gray Consulting Microscopy and Microanalysis for Cultural Heritage, Part II, organized with the New York Conservation Foundation and New York Microscopical Society Chair: Soraya Alcalá, The Hispanic Society of America 3-D Digital Microscopy and Cultural Heritage: A Successful Marriage, Ilaria Cacciari, Salvatore Siano, 2:00 IFAC-CNR Pairing 3-D Laser Scanning Confocal Microscopy with Reflectance Transformation Imaging to Gain 2:30 Insight into the Techniques Used to Create Relief and Contour Lines on Greek Red-Figure Vases, Philip A Klausmeyer, Paula Artal-Isbrand, Worcester Art Museum 3:00 Break Optical Coherence Tomography for the Non-Invasive 3-D Volume Imaging of Cultural Heritage, Haida 3:20 Liang, Nottingham Trent University 3:50 Pump-Probe Microscopy Enables Noninvasive, Three-Dimensional Imaging of Artwork, Warren S Warren, Tana Villafana, Martin Fischer, Duke University Coblentz 60th Anniversary Session Development of Vibrational Micro Spectroscopy and Imaging, organized by the Coblentz Society Chair: James Rydzak, GlaxoSmithKline 2:00 Diffuse Reflections on Chemical Imaging, Neil Lewis, Malvern 2:30 Historical Development of Mid-Infrared Spectroscopy, John Reffner, John Jay College 3:00 Break Historical Development of Raman Imaging - the Impact of the Instrumentational Developments on the 3:20 Quality of the Results, Fran Adar, J Y Horiba 3:50 Terahertz Spectroscopy: Past, Present and a Very Bright Future, Richard A McKay, Advantest America As of July 21, 2014 2014 EAS Preliminary Technical Oral Program    Monday Afternoon Continued Electronic Workflow – A New Frontier of Lab Management, organized by ALMA Chairs: Dennis Swijter, International Flavors and Fragrances and Judy Lin, Bristol-Myers Squibb Paper on Glass: A Practical Guide to the Implementation on Electronic Lab Notebook, James 2:00 Exarchakis, Colgate-Palmolive Company Implementing a Process Intelligence System for Pharmaceutical Development, Edward Keefe, Megerle 2:30 Scherholz, Bristol-Myers Squibb 3:00 Break The Role of the BIOVIA (Accelrys) Laboratory Execution System (LES) and Inventory Management 3:20 System (IM) in a CRO cGMP Environment, Kathy Shanks, PPD Electronic Orchestration of Knowledge Creation and Management, Joel Young, Ronald Behling, Larry 3:50 Fulton, Bristol-Myers Squibb Integrating Analytical Chemistry Research into Curriculum Chair: Dil Ramanathan, Kean University Incorporating Research Method Development into the Analytical Lab, Kimberley Frederick, Maryuri 2:00 Roca, Lisa Quimby, Skidmore College Integrating Teaching and Research: Strategies and Practices for Building a Research-Supportive 2:30 Curriculum, Roger S Rowlett, Colgate University 3:00 Break Integration of Research into the Curriculum Using XRD and NMR Structural Analysis, Benny Chan, Abby 3:20 R O'Connor, The College of New Jersey Involving Undergraduate Students in Collaborative Research: The Union College Aerogel Team, Mary 3:50 K Carroll, Union College NMR Spectroscopy of Molecules Small and Large: Methods and Applications, Part II Chair: David Rovnyak, Bucknell University 2:00 Structure/Function Studies of Obscurin Ig58/59, Nathan T Wright, James Madison University Working with Two and Many Dimensions: Non-Uniform Sampling for Sharper Spectra More Quickly and 2:30 Principal Component Analysis to Explore Spectral Series, Frank Delaglio, Agilent Technologies 3:00 Break Liquid State, High-Resolution 14N-NMR of Symmetrically Substituted Nitrogen-Containing Compounds, 3:20 Benjamin Liu, Princeton University Noncanonical Polyubiquitin Chains: Insights from Structural and Dynamical Studies, Carlos Castañeda, 3:40 Syracuse University, Susan Krueger, National Institute of Standards and Technology, Ashton Cropp, Virginia Commonwealth University, David Fushman, University of Maryland TUESDAY MORNING, NOVEMBER 18 EAS Award for Outstanding Achievements in Separation Science Honoring Thomas L Chester, University of Cincinnati Sponsored by Agilent Technologies Chair: J David Pinkston, Kellogg Company 9:00 Presentation of the EAS Award for Outstanding Achievements in Separation Science 9:05 Using Complexity To Make Separations Simpler, Thomas L Chester, University of Cincinnati Liquid Chromatographic Estimates of Octanol - Water Partitioning: Is there a Rational Stationary Phase 9:30 Choice?, John G Dorsey, Florida State University 10:00 Break Ultrahigh Performance Supercritical Fluid Chromatography of Lipophilic Compounds with Emphasis on 10:20 Synthetic and Commercial Biodiesel, Larry T Taylor, Mehdi Ashraf-Khorassani, Virginia Tech, Kenneth J Fountain, Giorgis Isaac, Waters Thinking Outside the Valve: Pressure Control and Other Important Questions in Supercritical Fluid 10:50 Chromatography/Mass Spectrometry (SFC/MS), J David Pinkston, Kellogg Company As of July 21, 2014 2014 EAS Preliminary Technical Oral Program    Tuesday Morning Continued EAS New Faculty Award In NMR Spectroscopy Honoring Megan Macnaughtan, Louisiana State University Sponsored by Agilent Technologies Session Chair: Patrick van der Wel, University of Pittsburgh Spherical Nanoparticle Supported Lipid Bilayers for the Study of Membrane Proteins, Fang Tian, 9:00 Pennsylvania State University Probing Dynamic Protein-Glycosaminoglycan Interactions Using Paramagnetic Ligands, Xu Wang, 9:30 Arizona State University 10:00 Break NMR Studies of Bacterial Masonry that Provide Protective Barriers, Charles V Rice, University of 10:20 Oklahoma 10:50 Presentation of the EAS New Faculty Award in NMR Spectroscopy 10:55 Challenges and Triumphs in Glycoprotein NMR, Megan Macnaughtan, Louisiana State University The Breath of Inhalation Analytical Chair: Justin Pennington, Merck 9:00 Solid-State Characterization Techniques for Inhalation Product Development, Matthew Lamm, Merck Using Particle and Polymer Properties to Tailor Aerosol Formulations, Christopher Kuehl, Nashwa El9:30 Gendy, Laird Forrest, Cory Berkland, University of Kansas 10:00 Break Making Quantitative Inhalation Analytics Measurements in Real-Time Using Single Particle Aerosol 10:20 Mass Spectrometry (SPAMS), David P Fergenson, Livermore Instruments, Maria Balaxi, David Kohler, Solvias AG, Anna Susz, Bradley D Morrical, Novartis Using Spray Pattern Area as a Surrogate for SAC in Optimizing pMDI Test Methods, Zachary Pitluk, 10:50 Proveris Scientific Detecting Counterfeit Pharmaceuticals Chair: Matthew Wood, Ocean County Sheriff's Office Forensic Laboratory Near Real Time Counterfeit Pharmaceutical Detection Along the Supply Chain, William E Mayo, 9:00 Veracity Networks Inc Analytical Testing of Counterfeit Drugs in the Field Using Vibrational Spectroscopy and GC/MS, Pauline 9:30 Leary, Smiths Detection 10:00 Break Paper Test Cards for Presumptive Identification of Falsified and Very Low Quality Pharmaceuticals, 10:20 Marya Leiberman, University of Notre Dame Analysis of Counterfeit Pharmaceutical Products using Visible and Vibrational Spectroscopies Inside and 10:50 Outside of the Laboratory, Adam Lanzarotta, Nicola Ranieri, FDA Forensic Chemistry Center Microscopy and Microanalysis for Cultural Heritage, Part III, organized with the New York Conservation Foundation and New York Microscopical Society Chair: John Scott, NYCF Jackson Pollock’s Number 1A (1948): Using Spatially Resolved XRF and Multivariate Analysis to 9:00 Characterize the Artist Palette and Process, Ana Martins, Jim Coddington, Museum of Modern Art, Donald Dahlberg, Lebanon Valley College, Geert van der Snickt, University of Antwerp, Birgit van Driel, École Polytechnique Fédérale de Lausanne, Joris Dik, Delft University of Technology Multiphoton Microscopy: An Efficient and Promising Tool for In Situ Characterization of Historical Artifacts, Gaël Latour, Laboratory Imagery and Modélisation en Neurobiology et Cancérologie, Laurianne 9:20 Robinet, Museum National Natural History, Jean-Philippe Echard, Marie Didier, Musée de la Musique, Marie-Claire Schanne-Klein, Ecole Polytechnique 9:50 Break Advances in the Imaging and Microscopy of semiconductor Pigments: From Laser-Based TimeResolved Luminescence Imaging to Micro X-Ray Fluorescence Analysis using Synchrotron Radiation, 10:10 Austin Nevin, Sara Bellei, Institute of Nanotechnologies and Photonics, Anna Cesaratto, Valentina Capogrosso, Gianluca Valentini, Daniela Comelli, Politecnico di Milano, Caroline Tokarski, Hervé Vezin, University Lille Laser Ablation Surface-Enhanced Raman Microspectroscopy, Pablo Londero, Marco Leona, The 10:40 Metropolitan The Metropolitan Museum of Art, Anna Cesaratto, Politecnico di Milano, John R Lombardi, City College on New York As of July 21, 2014 2014 EAS Preliminary Technical Oral Program    Tuesday Morning Continued LC Productivity Through Particle Change: Size, Type, Shape Chair: Peter Broske, Agilent Technologies Method Development with Zirconia Based Stationary Phases, Clayton McNeff, Daniel Nowlan, Kelly S 9:00 Johnson, ZirChrom Separations, Richard Henry, Consultant High-Pressure Ion Chromatography: Following the Lead of UHPLC, Peter Bodsky, Frank Hoefler, Maria 9:20 Rey, Thermo Fisher Scientific Achieving Maximum Kinetic Performance from UHPLC Columns, Richard A Henry, William H 9:40 Campbell, David S Bell, Sigma-Aldrich/Supelco 10:00 Break Halophase: A Novel Stationary Phase with Tunable Retention Properties through Functionalized 10:20 Carboxylate Deposition of Halogenated Small Molecules, Brian A Logue, Michael W Stutelberg, Venkataiah Mallam, Robert P Oda, Raj K Bhandari, South Dakota State University The Use of Elevated Temperature in HPLC Biomolecule Separation to Shorten Analysis Time and 10:40 Improve Peak Shape with Wide-Pore, Core-type Silica Columns, Stacy Squillario, Roy Eksteen, Hillel Brandes, Sigma-Aldrich/Supelco Easy Method Transfer and Scalability with Superficially Porous Particles, Anne E Mack, William J Long, 11:00 Wu Chen, Xiaoli Wang, Jason Link, Maureen Joseph, Agilent Technologies Monolithic Silica’s for “Dirty Sample” HPLC Analysis with Less Sample Preparation, Egidijus 11:20 Machtejevas, EMD Millipore Chemometric and Spectroscopic Applications in Forensics, organized by the Coblentz Society Chairs: Brandye Smith-Goettler, Merck 9:00 TBA, TBA Raman Microspectroscopy and Advanced Statistics for the Analysis of Biological Stains and Gunshot 9:30 Residue, Igor K Lednev, Greg McLaughlin, Kyle C Doty, Justin Bueno, University at Albany 10:00 Break Chemometrics in Action: Deployment of Handheld Spectroscopic Devices for First Responders, 10:20 Suzanne Schreyer, Lin Zhang, Michael Hargreaves, Thermo Fisher Scientific Hyperspectral Imaging and its Applications in Forensics Science, Jeffrey Beckstead, ChemImage 10:50 Corporation Detection and Fate of Nanoparticles in Biota Chair: Jason White, Connecticut Agricultural Experiment Station Fate and Effects of Engineered Nanomaterials in Agricultural Systems, Jason White, Joseph Hawthorne, 9:00 Roberto De la Torre-Roche, Connecticut Agricultural Experiment Station Locating Metal Oxide Nanoparticle Transformation in Plants Using Synchrotron X-Rays, Jorge Gardea9:30 Torresdey, Jose Hernadez-Viezcas, University of Texas-El Paso, Hiram Castillo-Michel, European Synchrotron Radiation Facility 10:00 Break Determination of Carbon Nanotube Fate and Exposure Using a Microwave-Induced Heating Method, 10:20 Jacyln Cañas-Carrell, Amanda Parra, Sabrina Deleon, Fahmida Irin, Mohammad Saed, Micah Green, Texas Tech University Identification and Avoidance of Potential Artifacts and Misinterpretations in Nanomaterial Ecotoxicity Measurements, Elijah Petersen, Vincent Hackley, Teresa Kirschling, National Institute of Standards and 10:50 Technology, Theodore Henry, Heriot-Watt University, Jian Zhao, Baoshan Xing, Stockbridge School of Agricultural, Robert MacCuspie, Florida Polytechnic University, Marina Dobrovolskaia, Leidos Biomedical Research Inc., Jason White, Connecticut Agricultural Experiment Station As of July 21, 2014 2014 EAS Preliminary Technical Oral Program    Tuesday Morning Continued Functional Surfaces: Preparation and Analysis Chair: Robert Opila, University of Delaware Silicon Surface Functionalization to Control the Oxidation State of Copper during Metalorganic Chemical 9:00 Vapor Deposition of Cu(I) and Cu(II) Precursors, Yichen Duan, Andrew Teplyakov, University of Delaware Mechanism of Electrical Passivation of Silicon Surfaces with Quinhydrone, Meixi Chen, Nicole A 9:20 Kotulak, Nikolas J Schreiber, Robert L Opila, University of Delaware Electron Beam Induced Reactions of Adsorbed π-Allyl Ruthenium Tricarbonyl Bromide: Towards Design of Electron Beam Induced Deposition (EBID)-Specific Precursors, Julie A Spencer, Rachel Thorman, 9:40 Michael Barclay, D Howard Fairbrother, Johns Hopkins University, Joseph A Brannaka, Lisa McElweeWhite, University of Florida, Oddur Ingólfsson, University of Iceland 10:00 Break Formation of High-Coverage Nanoparticle Monolayers through Click Chemistry, Mackenzie G Williams, 10:20 Yue Liu, Timothy Miller, Andrew Teplyakov, University of Delaware Correlation of Carbon Growth on Ru-Capped Multilayer Mirrors Irradiated by Extreme-Ultraviolet Light 10:40 and Electrons, Michael S Barclay, Nadir S Faradzhev, Howard Fairbrother, Johns Hopkins University, Shannon B Hill, Thomas B Lucatorto, National Institute of Standards and Technology Controlled Synthesis and Optical Studies of ZnO Nanostructures, Zhengxin Li, Jolie Blake, Lars 11:00 Gundlach, University of Delaware Food and Additive Analysis Chair: Michael Ruberto, Materials Need Consulting 9:00 Detection of Olive Oil Adulteration Using Benchtop NMR Spectroscopy, Susanne Riegel, Nanalysis Determination of Perfluorooctanoic Acid (PFOA) from the Surface of Cookware under Simulated Cooking 9:20 Conditions Using Accelerated Solvent Extraction (ASE) and LC/MS/MS, Changling Qiu, Douglas Raynie, South Dakota State University HPLC Analysis of a Commercial Whirlpool Hopping Process in the Beer Brewing Industry, Jessica S 9:40 Henry, Kelsey A Packard, Elizabeth A Brady, Sterling A Tomellini, University of New Hampshire, Austin D Gregoire, Craft Brew Alliance 10:00 Break Development of SERS Methods for Rapid Detection of Multi-Pesticides in Food, Lili He, University of 10:20 Massachusetts-Amherst Very Large Range Pesticide Screening in Food Using GC Triple Quadrupole MS, Lori Dolata, Massimo 10:40 Santoro, Thermo Fisher Scientific Analysis of Beer, Wine and their Agricultural Constituents (Hops, Grapes, Grains) for Pesticides Using 11:00 QuEChERS Extraction and High-Throughput Sample Preparation, Patricia L Atkins, SPEX CertiPrep Vacuum Ultraviolet Detection for the Identification and Quantification of Pesticides by Gas Chroma11:20 tography, Hui Fan, Doug D Carlton, Jr., Ian Sawicki, Kevin A Schug, University of Texas – Arlington, Phillip Walsh, Dale Harrison, VUV Analytics Development of a Sensitive LC/UV Method to Determine Two Trace Aldehydes in Maltitol, George 11:40 Wang, Zhen Wu, Holly M Shackman, Mark S Bolgar, David K Lloyd, Bristol-Myers Squibb TUESDAY AFTERNOON, NOVEMBER 18 EAS Award For Outstanding Achievements in Chemometrics Honoring Marcel Maeder, University of New Castle Sponsored by Eigenvector Research Session Chair: Paul Gemperline, Eastern Carolina University 2:00 Hard-Modelling - from Titrations to Solving Climate Tribulations, Graeme Puxty, CSIRO Hybrid Hard and Soft-Modeling and Local Rank Analysis: Two Relevant Ideas to Describe and Explore 2:30 Chemical Systems, Anna de Juan, University of Barcelona 3:00 Break Calculation of Feasible Bands for Visualizing the Constraint Effects in Model-Free Methods, Hamid 3:20 Abdollahi, Institute for Advanced Studies in Basic Sciences 3:50 Presentation of the EAS Award for Outstanding Achievements in Chemometrics Chemometrics: The Balance Between ‘Chemistry’ and ‘Metrics’, Marcel Maeder, University of New 3:55 Castle As of July 21, 2014 2014 EAS Preliminary Technical Oral Program    Tuesday Afternoon Continued Dried Blood Spot (DBS) Analysis and its Alternatives: Recent Advances in Clinical, Forensic and Pharmaceutical Applications Chairs: Daniel Norwood, Boehringer Ingelheim and Naiyu Zheng, Bristol-Myers Squibb History of DBS and its Development from Clinical to Pharmaceutical Application, Daniel L Norwood, 2:00 Boehringer Ingelheim Dried Blood Spots - From Newborn Screening to Forensic Science, Donald Chace, Pediatrix Medical 2:30 Group 3:00 Break Recent Progress in Overcoming Some Obstacles in Implementing Dried Blood Spot Technology in Drug 3:20 Development, Qin Ji, Bristol-Myers Squibb Automated Bioanalysis of Dried Blood Spots and Dried Plasma Spots Coupled with High Resolution 3:50 Mass Spectrometry and SRM LC/MS Technologies, Jack Henion, Robert Sturm, Regina Oliveira, Quintiles Bioanalytical and ADME Labs Understanding Supercritical Fluid Chromatography and Using It, sponsored by the Chromatography Forum of Delaware Valley Chair: Mary Ellen McNally, E.I DuPont de Nemours and Company Enhanced-Fluidity Liquid Chromatography (EFLC) for Highly Polar Biologically Relevant Compounds, 2:00 Susan Olesik, Martin Beres, Rafael Bennett, Ohio State University 2:30 Recent Advances in SFC Applications, Jennifer Van Anda, Agilent Technologies 3:00 Break Effect of Particle Size on the Speed and Resolution of Chiral Separations Using Supercritical Fluid 3:20 Chromatography, Mirlinda Biba, Erik L Regalado, Christopher J Welch, Merck, Naijun Wu, Celgene The Power of Ultra Performance Convergence Chromatography; Theoretical Considerations and some 3:50 Examples of Use, Francois Huby, The Dow Chemical Company Forensic Toxicology Chair: Barry K Logan, Center for Forensic Science Research and Education Comparison of GCMS, EIA, and LC-QTOF Screening Methods for Novel Psychoactive Substances in 2:00 Urine Samples, Jill Yeakel, Lehigh Valley Toxicology, Mandi Mohr, Center For Forensic Science Research and Education, Barry Logan, NMS Labs Use of Time-of-Flight (TOF) and Quadrupole Time-of-Flight (QTOF) Methodologies for Detection of 2:30 Designer Drugs in Forensic Toxicology Casework, Jared Castellani, South Carolina Law Enforcement 3:00 Break Simultaneous Analysis of 22 Anti-Epileptic Drugs in Post-Mortem Blood, Serum and Plasma, Karen 3:20 Scott, Arcadia University Development and Validation of a Quantitative Method for the Detection of Pyrroldinophenone Designer 3:50 Drugs in Blood Using LC-MS/MS, Donna Papsun, NMS Labs New York Microscopical Society Ernst Abbe Award Symposium on Atomic Force Microscopy Infrared Spectroscopy, organized with the New York Conservation Foundation Honoring Dr Alexandre Dazzi, University of Paris-Sud Session Chair: John Reffner, John Jay College How Photoacoustic and Nanomechanics Combine to Perform IR Spectroscopy at the Nanoscale, 2:00 Alexandre Dazzi, University of Paris-Sud Extending AFM-Based Infrared Spectroscopy to a Wide Range of Applications, Craig Prater, Anasys 2:30 Instruments 3:00 Break AFM-IR: Nanoscale IR Spectroscopy for the Materials and Life Sciences, Curtis Marcott, Light Light 3:20 Solutions, Craig Prater, Qichi Hu, Michael Lo, Kevin Kjoller, Anasys Instruments Tip-Enhanced Infrared Nanospectroscopy via Molecular Expansion Force Detection, Mikhail A Belkin, 3:50 Feng Lu, Mingzhou Jin, University of Texas NanoIR to Investigate Parchment and its Degradation, Laurianne Robinet, Center of Research for 4:20 Conservation, Gaël Latour, Ariane Deniset-Besseau, Alexandre Dazzi, University of Paris-Sud, MarieClaire Schanne-Klein, Laboratory for Optics and Biosciences As of July 21, 2014 2014 EAS Preliminary Technical Oral Program    Tuesday Afternoon Continued Novel Applications of Mass Spectrometry to Solve Analytical Challenges Chair: Fenghe Qiu, Boehringer Ingelheim Quantitating Protein Panels And Normalizing Hematocrit From Dried Blood Spots (DBS) Using An 2:00 Automated SISCAPA® Mass Spectrometry Workflow, Morteza Razavi, Selena S Larkin, Terry W Pearson, Leigh Anderson, SISCAPA Assay Technologies Validated Determination of Dapagliflozin and Qualitative Determination of Its Glucuronide Metabolite in Human Dried Blood Spot: Multiple-Site Pediatric Clinical Experience, Xiaohui Xu, Jane Liu, Jim Shen, 2:20 Melanie Pe Benito, Marsha Epstein, Guowen Liu, David Boulton, Pathanjali Kadiyala, Mark E Arnold, Qin C Ji, Bristol-Myers Squibb, Michael Waldron, PPD Probing Host-Guest Interaction Using Hydrogen-Deuterium Exchange and Mass Spectrometry, Jui S 2:40 Chaugule, Dil Ramanathan, Kean University 3:00 Break Advantages and Challenges of Applying LC-MS/MS to Regulated Protein Bioanalysis, Hao Jiang, 3:20 Jianing Zeng, Craig A Titsch, Linlin Luo, Dharmesh D Desai, Anne F Aubry, Binodh S DeSilva, Mark E Arnold, Bristol-Myers Squibb Improved LC/MS Method Development for Pain Management Panels, Thomas A Russell, Shimadzu 3:40 Scientific Instruments Identification of Volatile Organic Compounds in Beer by TurboMatrix Headspace Trap System-Gas 4:00 Chromatography-Mass Spectrometry, Hetal Rana, Dil Ramanathan, Kean University The Role of Analytical Chemistry in Water Quality, sponsored by Thermo Fisher Scientific Chair: Sut Ahuja, Ahuja Consulting 2:00 TBA, Sut Ahuja, Ahuja Consulting Raising Awareness of Water Issues: The Education Connection, the Educational Potential, Mark A 2:30 Benvenuto, University of Detroit Mercy 3:00 Break Recent Developments in Stationary Phases for Ion Chromatography, Christopher A Pohl, Thermo 3:20 Fisher Scientific Novel Electrochemical and Reflectance Photometric Techniques for the Measurement of Trace Arsenic 4:50 in Water, Abul Hussam, Douglas Mays, Jinsoo Hong, Joan Rozario, George Mason University Pharmaceuticals in Environment and Water Quality: The Role of Analytical Chemistry, Hua Yao, Bristol4:20 Myers Squibb Surface Spectroscopy and Microscopy Chair: Andrew Teplyakov, University of Delaware 2:00 Passivation of Semiconductor Surfaces, Robert Opila, University of Delaware 2:30 Interface Analysis of Nano-scale Materials, Leonard Feldman, Rutgers University 3:00 Break Assembly and Nanocrystallization in Carbon Nanoparticle Films, Janice Reutt-Robey, University of 3:20 Maryland Understanding the Electron Stimulated Surface Reactions of Organometallic Complexes to Enable 3:50 Design of Precursors for Electron Beam Induced Deposition, Howard Fairbrother, Julie Spencer, Mike Barclay, Samantha Rosenberg, Johns Hopkins University, Lisa McElwee-White, University of Florida Frontiers in Biological NMR Spectroscopy Chair: Scott Showalter, Pennsylvania State University Characterizing the Dynamic Formation of Disease Protein Aggregates using Dark-State Exchange 2:00 Saturation Transfer (DEST) NMR, Nicolas L Fawzi, Brown University Structure, Dynamics, and Function of Opa60: A Neisserial Beta-Barrel Membrane Protein that Mediates 2:30 Host Phagocytosis, Linda Columbus, Alison K Criss, Peter M Kasson, University of Virginia 3:00 Break 3:20 Characterization of the Active Site of Vanadium Chloro-peroxidase by 51V Solid-State NMR Spectroscopy, Rupal Gupta, Guangjin Hou, Tatyana Polenova, University of Delaware 13 C-Detect NMR and Mass Spectrometry Applied to Study the Effects of Post-Translational Modifications 3:40 on Disordered Proteins, Eric B Gibbs, Debashish Sahu, Scott A Showalter, The Pennsylvania State University Studying Networks of Weak Protein Interactions by NMR, Assen Marintchev, Nabanita Nag, Jielin Yu, 4:00 Devika Nadkarni, Boston University School of Medicine, Katherine A Edmonds, Indiana University, Boriana Marintcheva, Bridgewater State University As of July 21, 2014 2014 EAS Preliminary Technical Oral Program    Tuesday Afternoon Continued Separation Efficiency, Reagent Reduction, Microfluidics, and Multidimensionality Chair: Nina Gonnella, Boehringer Ingelheim Reducing Solvent Consumption in High-Performance Liquid Chromatography During Column Re2:00 Equilibration after Gradient Elution, Michael R Fletcher, Erin J Ennis, Donna M Blackney, Catherine A Kita, Joe P Foley, Drexel University The Importance of Tolerance Limits in UHPLC Method Modelling for Robustness Evaluation, Imre L 2:20 Molnár, Hans-Jürgen Rieger, Molnár-Institute The Use of Eluent Generation in Ion Chromatography, Peter Bodsky, John Madden, Thermo Fisher 2:40 Scientific 3:00 Break What Performance can we Expect from Microfluidic LC/MS System?, Martin Gilar, Thomas S McDonald, 3:20 Gregory Roman, Jay S Johnson, James P Murphy, Waters Investigation of Multidimensional Chromatography for Chromatographic Separation of Complex Mixtures 3:40 of Closely Related Species, Erik L Regalado, Christopher J Welch, Merck Determination of Common Counter and Impurity Anions in Pharmaceutical Using a High-Pressure 4:00 Modular Capillary Ion Chromatography System (HPIC) with Suppressed Conductivity (CD) and Charge (QD) Detection, Hua Yang, Linda Lopez, Thermo Fisher Scientific Recent Compendial Activity for Dissolution Testing When Gelatin Crosslinking is an Issue, Gregory P 4:20 Martin, Complectors Consulting, Vivian A Gray, VAG Consulting WEDNESDAY MORNING, NOVEMBER 19 EAS Award for Outstanding Achievements in Near Infrared Spectroscopy Honoring Mark Westerhaus, FOSS Sponsored by Metrohm USA Session Chair: Lars Nørgaard, FOSS 9:00 Presentation of the EAS Award For Outstanding Achievements In Near Infrared Spectroscopy 9:05 My Contributions to NIR Spectroscopy, Mark Westerhaus, FOSS Classification and Interpretation of NIR Data: Recursive Weighted Partial Least Squares Discriminant 9:30 Analysis (rPLS-DA), Søren B Engelsen, University of Copenhagen 10:00 Break Two Major Advanced Algorithms in NIRS: Cloning Instruments and Local Calibration, Pierre Dardenne, 10:20 Walloon Agricultural Research Centre Application of Non-Linear Chemometric Models to NIR Data, Lars Nørgaard, Morten With Pedersen, 10:50 Pedro Højen-Sørensen, FOSS EAS Award for Outstanding Achievements in Nuclear Magnetic Resonance Honoring Robert Tycko, National Institutes of Health Sponsored by Bruker BioSpin and New Era Enterprises Session Chair: David Weliky, Michigan State University 9:00 Solid-State NMR of Viral Fusion Proteins, David Weliky, Michigan State University Celebrating a New Era of High-Field Solid-State NMR of Amyloid and Globular Proteins, Yoshitaka Ishii, 9:30 University of Illinois – Chicago 10:00 Break Structural and Dynamic Studies of Protein Assemblies by Solid-State NMR Spectroscopy, Christopher P 10:20 Jaroniec, Ohio State University 10:50 Presentation of the EAS Award for Outstanding Achievements in Nuclear Magnetic Resonance Solid-State NMR of Protein Assemblies: New Methods and New Results, Robert Tycko, Jun-Xia Lu, 10:55 Marvin Bayro, Alexey Potapov, Eric Moore, Dylan Murray, Kent Thurber, Wai-Ming Yau, National Institutes of Health Improving the Applications of Mass Spectrometry Through Fundamentals Chair: Murray Johnston, University of Delaware Matrix-Assisted Ionization: A Simple Low Energy Ionization Approach for Volatile and Nonvolatile 9:00 Compounds, Charles McEwen, Khoa Hoang, Milan Pophristic, University of the Sciences From Laser Ablation and Electrospray Fundamentals to Ambient Ionization by LAESI, Akos Vertes, 9:30 Tarek R Mansour, Sylwia A Stopka, Hang Li, Bindesh Shrestha, George Washington University 10:00 Break 10:20 Mass Spectrometry: A Tool for Studying Metabolomics, Ann M O’Brien, DuPont Biological Applications of FTICR Imaging Mass Spectrometry: Overcoming the Analytical Challenges of 10:50 Direct Tissue Analysis, Jeffrey Spraggins, Raf Van de Plas, Richard Caprioli, Vanderbilt University As of July 21, 2014 2014 EAS Preliminary Technical Oral Program    Wednesday Morning Continued Chromatography Challenges: Large and Small Molecules, organized by North Jersey Chromatography Group Chair: Landon Greene, Rutgers University 9:00 TBA, Brian Buckley, Rutgers University Agroecosystem Analysis Using Chromatographic Methods, Jeffrey S Buyer, United States Department 9:30 of Agriculture 10:00 Break Deciphering 4-Billion Year Old Meteorite Chemistry Through Liquid Chromatography-Mass 10:20 Spectrometry, Michael P Callahan, National Aeronautics and Space Administration Goddard Space Flight Center Utilizing a Semi-Automated Sample Preparation Workflow to Achieve Accurate, Precise, Rugged and 10:50 Robust Analytical Assay Methods for Pharmaceutical Solid Oral Dosage Forms, Khanh Ha, Bristol-Myers Squibb Bioanalytical Applications of Vibrational Spectroscopy Chair: Lydia Breckenridge, Bristol-Myers Squibb Quantitative Analysis of Moisture in Intact Lyophilized Protein Samples by NIRS, Suzanne Schreyer, 9:00 Michelle Pressler, Thermo Fisher Scientific Noninvasive In-Vivo Glucose Sensing on Human Subjects Using Mid-Infrared Light, Sabbir Liakat, Kevin 9:20 A Bors, Callie M Woods, Claire F Gmachl, Princeton University Surface Enhanced Raman Scattering Characterization of one Hydroxyl-polymethoxylflavones, Changchu 9:40 Ma, Hang Xiao, Lili He, University of Massachusetts-Amherst 10:00 Break Bacterial Identification using Raman Spectroscopy: How Does the Technique Perform with many 10:20 Species of Bacteria?, Bradford G Clay, Pierre Mahe, Maud Arsac, Brenna Moss, Olivia Jobes, Chris Huff, Virginia D Shortridge, Ron Robinson, Sonia Chatellier, Alex van Belkum, bioMérieux, Inc Terahertz Spectral Profiling and Imaging of Human Skin for early Detection of Cancer, Aisha Masud, 10:40 Babar Rao, Rao Dermatology, Aunik Rahman, Anis Rahman, Applied Research & Photonics Forensic Microscopy VIII, sponsored by the New York Microscopical Society and TAKA Instructional Agency Chair: Thomas Kubic, John Jay College 9:00 Microscopy's Importance in Cases I Have Worked, Peter DeForest, Forensic Consultant 9:30 Microscopy of Tattoo Inks, Michelle Miranda, SUNY- Farmingdale 10:00 Break Microscopy of Shotgun Buffers (Not your Common pH), Peter Diaczuk, John Jay College, Jack Hietpas, 10:20 Pedico Research Institute 10:50 Microscopy of Dust Samples, Skip Palenik, Micro Trace Spectroscopy: Sample Analysis, Data Analysis, and Detection Chair: Shirley Rodriguez, Boehringer Ingelheim Enhancement of Curcumin Fluorescence by Ascorbic Acid in Bicontinuous Microemulsion, Maurice O 9:00 Iwunze, Morgan State University An Investigation of Solution Phase Copper ESR Spectra as a Means to Study Speciation by Ligands in 9:20 Aqueous Solution, Including those of Geochemical Significance, Christopher J Bender, Fordham University Raman, Infrared and Microwave Spectra, r0 Structural Parameters, and Conformational Stability of 9:40 Isopropylisocyanate, Bhushan S Deodhar, James R Durig, University of Missouri-Kansas City 10:00 Break 10:20 Comparison of Target Detection and Maximum Signal Factors, Neal B Gallagher, Eigenvector Research The Use of Dynamic Imaging Particle Analysis for Characterization of Chromatography Column Packing 10:40 Material, Lew Brown, Fluid Imaging Technologies 11:00 Polymer Gel Permeation Chromatography with Luminescence Detection, Martin Nosowitz, Arkema As of July 21, 2014 2014 EAS Preliminary Technical Oral Program    Wednesday Morning Continued New Approaches to the Analysis of Analytes in Difficult Environmental Matrices Chair: Amy Birch, Boehringer Ingelheim Fast GC/TOFMS For High-Throughput Screening of Environmental Contaminants, Pete Grosshans, 9:00 Nicola Watson, Charles Haws, Laura McGregor, Nick Bukowski, Markes International Using Solid-Phase Extraction to Concentrate Human Hormones in Drinking Water and High9:20 Performance Liquid Chromatography to Analyze the Recovery, Carl A Fisher, Hua Yang, Pranathi Perati, Thermo Fisher Scientific Low Level Chrysotile in Soil: A Method Assessment, Frank Ehrenfeld, Raymond Kennedy, Kristen 9:40 Goedde, Thomas Barkley, International Asbestos Testing Laboratories 10:00 Break 10:20 Direct Mercury Analysis of Gaseous Samples Using Sorbent Tubes, Sumedh P Phatak, Milestone Inc Novel QCell Technology for Inference Removal in ICP-MS - Combining Low Mass Filtration with Kinetic 10:40 Energy Discrimination, Fergus Keenan, Craig Seeley, Thermo Fisher Scientific Single Particle ICP-MS (SP-ICP-MS) a New Analytical Technique for Counting and Sizing Metal Based 11:00 Nanomaterials: Theory and Application, Chady Stephan, PerkinElmer Quad vs Magnet, Battle of the ICPMS Instruments for Superiority of Cr Speciation in NJ Drinking Water 11:20 Samples, Elizabeth McCandlish, Sanjeev Rai, Brian Buckley, Rutgers University, Lee Lippincott, New Jersey Department of Environmental Protection Polyol Induced Extraction (PIE) of Water from Organic Solvents, Mithilesh Deshpande, Seton Hall 11:40 University WEDNESDAY AFTERNOON, NOVEMBER 19 EAS Award for Outstanding Achievements in Mass Spectrometry Honoring Catherine Fenselau, University of Maryland Sponsored by Thermo Fisher Scientific Session Chair: Burnaby Munson, University of Delaware Fourier Transform Ion Cyclotron Resonance and Infra-Red Multiphoton Dissociation Studies of Cadmium 2:00 Sulfide Metal Clusters, Douglas P Ridge, Kaitlin Papsin, Una Kim, University of Delaware, Giel Berden, Jos Oomens, Radboud University Nijmegen Mass Spectrometry of Airborne Particulate Matter: How it Works and What it Tells Us About the Air We 2:30 Breathe, Murray Johnston, University of Delaware 3:00 Break 3:20 Mass Spectrometry to Support Industrial Fermentation, Barbara Larsen, DuPont 3:50 Presentation of the EAS Award for Outstanding Achievements in Mass Spectrometry Mass Spectrometry Explores Communication in the Tumor Environment, Catherine Fenselau, Suzanne 3:55 Ostrand-Rosenberg, Meghan Burke, Rebecca Rose, Lucia Geis-Asteggiante, University of Maryland Pharmaceutical and Biopharmaceutical Applications of Near-Infrared Spectroscopy, organized by the Coblentz Society Chairs: Brandye Smith-Goettler, Merck The Incredible Shrinking NIR Instrument; and Why that is Great for the Pharma Industry, Emil Ciurczak, 2:00 Coblentz Society Validation and Transfer of NIR Methods for Real Time Release Testing for Continuous Manufacture, 2:30 Jianfeng (Frank) Qi, Kelly A Swinney, Henrik T Rasmussen, David E Nadig, Vertex Pharmaceuticals 3:00 Break 3:20 Understanding Hot Melt Extrusion via NIRS, Brandye Smith-Goettler, Merck Advances in Applying Near Infrared Measurements to Cell Cultures and Fermentation Processes, Gary 3:50 Ritchie, Infratrac Separation Challenges in Biopharmaceutics, sponsored by Agilent Technologies Chair: Irena Maksimovic, Bristol-Myers Squibb Fast and Efficient Peptide Mapping With Superficially Porous Particle HPLC Columns, Timothy Rice, 2:00 Agilent Technologies Chromatographic Analysis and Separation of Short RNA Oligonucleotides with Novel Liquid 2:30 Chromatography Methods, Mirlinda Biba, Christopher J, Welch, Merck, Joe P Foley, Drexel University 3:00 Break 3:20 Case Study of Challenges in ADC Method Development, Girija Krishnamurthy, Bristol-Myers Squibb 3:50 iCE3: a Powerful Analytical Tool for Antibody Drug Conjugate, Jiaqi Wu, ProteinSimple As of July 21, 2014 2014 EAS Preliminary Technical Oral Program    Wednesday Afternoon Continued Innovative Directions in Sample Preparation for Chromatography, sponsored by the Chromatography Forum of Delaware Valley Chairs: Xiaoli Wang and Bruce Richter, Agilent Technologies Application of SPME in High-Throughput and In-Vivo Drug Quantification, Janusz Pawliszyn, University 2:00 of Waterloo Investigations into Analytical Extractions using Green Solvents, Douglas Raynie, South Dakota State 2:30 University 3:00 Break Selective Extraction of DNA Using Magnetic Ionic Liquids, Jared L Anderson, Kevin D Clark, 3:20 Omprakash Nacham, Honglian Yu, University of Toledo Advances in Sample Preparation for Dietary Supplements and Other Complex Matrices, Derick Lucas, 3:50 Jerry Zweigenbaum, Bruce Richter, Irina Dioumaeva, Agilent Technologies Advances in HPLC and Dissolution Chair: Judy Lin, Bristol-Myers Squibb HPLC Method Development Strategies for Molecules with Multiple Chiral Centers, Michael W Dong, 2:00 Kelly Zhang, Meenakshi Goel, Nik P Chetwyn, Genentech Strategies of Advanced LC/MS/MS Screening and Development for Regulated Bioanalysis, Jian Wang, 2:20 Ryan Gu, Eliza Fung, Ang Liu, John Lute, Mark Arnold, Anne Aubry, Bristol-Myers Squibb Selected Ion Flow Tube Mass Spectrometry (SIFT-MS): Real-time, Sensitive Detection of Residual 2:40 Solvents in Pharmaceuticals, Barry J Prince, Daniel B Milligan, Vaughan S Langford, Syft Technologies, Chuck Renner, Quantum Analytics 3:00 Break USP Analysis of DMSO Soluble Drug Substances and Excipients Using NexION ICP/MS, 3:20 Jonathan L Sims, Fadi Abou-Shakra, PerkinElmer Real-Time Dissolution Behavior of Indomethacin in Spray Dried Dispersion (SDD) in Biorelevant Media 3:40 Using UV Surface Imaging Technology, Steven Ponce, Xujin Lu, Christopher Zordan, Bristol-Myers Squibb Understanding the Dynamic Process of Dissolution and Hydrolysis of Aspirin by ATR/FTIR, Vrushali M 4:00 Bhawtankar, Seton Hall University Recent Compendial Activity for Dissolution Testing When Gelatin Crosslinking is an Issue, Gregory P 4:20 Martin, Complectors Consulting, Vivian A Gray, VAG Consulting Sample Preparation Techniques Chair: Christina Robb, CT Agricultural Experiment Station Extraction of Volatile Organics Using Carbonnanotubes Immobilized Composite Membranes, Smruti 2:00 Ragunath, Somenath Mitra, New Jersey Institute of Technology The Introduction of PDMS-Overcoated Adsorbent Based Fiber Coatings, Len Sidisky, Robert Shirey, 2:20 Yong Chen, Supelco/Sigma-Aldrich Comparison of Green Solvents during Chemical Extraction by Diffusion Studies, Shanmugapriya 2:40 Dharmarajan, Douglas E Raynie, South Dakota State Univeristy 3:00 Break 3:20 Expanding Method Capabilities through Dynamic Sample Preparation, Keith Griswold, Pepsico Extraction of Steroids from Water and Herbal Medicines using QuEChERS Sample Preparation, Michelle 3:40 L Schmidt, Nicholas H Snow, Seton Hall University Single Reaction Chamber Microwave Digestion: Sample Prep for Better Trace Analysis, David Gunn, 4:00 Njies Pedjie, Milestone Inc Molecular Spectroscopy of Composites and Related Materials Chair: Alan J Rein, Agilent Technologies Improved Bonding of Composites, Polymers and Coatings by Monitoring Surface Preparation with 2:00 Handheld FTIR Spectroscopy, John Seelenbinder, Alan J Rein, Agilent Technologies Non-Contact Material Characterization Using Mid-Infrared Quantum Cascade Laser Spectroscopy, Mark 2:30 Norman, Anish Goyal, Block Engineering 3:00 Break Portable Raman Spectroscopy Opens the Door for Site Analysis, Katherine Bakeev, Dawn Yang, Philip 3:20 Zhou, B&W Tek Repair of CFRP Composite with Localized Incipient Thermal Damage Guided by Handheld FTIR 3:50 Inspection, Tucker Howie, Ashley Tracey, Brian Flinn, University of Washington, Paul Vahey, Paul Shelley Boeing As of July 21, 2014 2014 EAS Preliminary Technical Oral Program    Wednesday Afternoon Continued NMR Spectroscopy of Pharmaceuticals and Materials Chair: Gary Martin, Merck What’s in your “Natural” Supplement? Application of NMR Spectroscopy to Natural Products, Jimmy 2:00 Yuk, Mark Garvey, Christian Fischer, Kim Colson, Bruker BioSpin 2:30 Enabling Strategies and Platforms for NMR Metabolite Characterizations, Janet Caceres Cortes 3:00 Break New Methods for the Simultaneous Measurement of Homo- and Heteronuclear Coupling Constants, 3:20 Josep Sauri, Merck, Teodor Parella, Universitat Autònoma de Barcelona Experiment Approaches to Probe Long-Range H-X Correlations in 2-D NMR Spectroscopy, Ronald 3:50 Crouch, Agilent Technologies, Craig Butts, Bristol University PLENARY LECTURE We are excited to announce our award winner of the EAS Award for Outstanding Achievement in the Fields of Analytical Chemistry, Dr Joseph Caruso, from the University of Cincinnati, will present a plenary lecture for all of EAS registrants, on Monday, Nov 17th at 4:30pm in the Double Tree Hotel This presentation will be followed by a time of networking and refreshments with all registrants of EAS encouraged to attend This is not an event to miss.  As of July 21, 2014