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combinatorial synthesis of derivatives of bioactive compounds via a sulfone scaffold

combinatorial synthesis of derivatives of bioactive compounds via a sulfone scaffold

combinatorial synthesis of derivatives of bioactive compounds via a sulfone scaffold

... A1 B5 A B1 A2 B2 A2 B A2 B A2 B5 A3 B1 Split and react A3 B2 A3 B3 A3 B4 A3 B5 A B1 A2 B3 A3 B A B3 A 1B A3 B A 2B A 2B C1 A 2B A 3B Split and react A1 B3 A B1 Pool A 1B A1 B 15 Products A 3B C2 Reactions ... A1 B4C1 A1 B C A1 B C A1 B3C3 A B4 C A B3 C A 1B 4C A2 B C A2 B4C1 A2 B C A2 B C A2 B3C3 A B4 C A B3 C A 2B 4C A3 B C A3 B C A3 B C A3 B4 C A3 B3C3 A B4 C A B3 C A B4 C A1 B C A3 B C A1 B C A3 B C A1 B5C3 ... C3 A1 B1 C A1 B C A B1 C A 1B 2C A 1B 1C A1 B2C3 A B1 C A B2 C A2 B1 C A2 B C A B1 C A 2B 2C A 2B 1C A2 B2C3 A B1 C A B2 C A B1 C A 3B 2C A3 B1C2 A3 B2C2 A 3B 1C A 3B 2C A 3B 1C A 3B 2C A1 B C A1 B4C1...
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synthesis of wo3tio2 nanocomposites via sol–gel method

synthesis of wo3tio2 nanocomposites via sol–gel method

... patterns of 40 wt% WO3 /TiO2 nanocomposites after calcination at 400 ◦ C for (a) h, (b) h and (c) 12 h, respectively As shown in Fig 3, the WO3 /TiO2 nanocomposites prepared by the sol–gel method ... Longer Fig DTA curves of the precursor with different amount of WO3 (a) 10 wt%, (b) 20 wt% and (c) 40 wt% Fig XRD patterns of the WO3 /TiO2 nanocomposites with different amounts of WO3 (a) 10 wt% ... respectively Fig TEM image of the 40 wt% WO3 /TiO2 nanocomposites 202 H Yang et al / Journal of Alloys and Compounds 398 (2005) 200–202 Table The lattice parameters of TiO2 in WO3 /TiO2 nanocompositesa...
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Báo cáo hóa học:

Báo cáo hóa học: " An alternative route for the synthesis of silicon nanowires via porous anodic alumina masks" potx

... dimensions These nanoparticles necessarily have a size smaller than the pores of the AAO mask and will be responsible for the constant dimensions of the synthesized nanowires Figure shows the surface of ... structure of the membrane and before the treatment conditions allow the nanowires growth As can be seen there, the catalyst can be observed as small particles inside the porous structure of the mask ... the melting of Si into the alloy [33] The diameter of the nanowires ranged from ca 30-50 nm, with an average size of ca 40 nm and was related to the pore size of the AAO mask HRTEM revealed the...
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Báo cáo y học:

Báo cáo y học: "Isolation and identification of bioactive compounds in Andrographis paniculata (Chuanxinlian)" potx

... expression of E-selectin, chitinases, mucin Muc5ac and iNOS in lung tissues and airway hyperresponsiveness [71] Andrographolide inhibits OVA-induced increases TNF-α and GM-CSF in BALF of OVA-sensitized ... namely andrographolide, bis-andrographolide 14-deoxy-11,12-didehydroandrographolide, andrograpanin, 14-deoxyandrographolide, (±)-5hydroxy-7,8-dimethoxyflavanone and 5-hydroxy-7,8dimethoxyflavone Andrographolide ... tract infections and relieving the inflammatory symptoms of sinusitis [85] The migratory response of leukocytes to chemokines forms the first line of defence to the invading microbial A paniculata...
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Organocatalytic strategies towards chiral fluorinated molecules as precursors of bioactive compounds

Organocatalytic strategies towards chiral fluorinated molecules as precursors of bioactive compounds

... Introduction: chiral organofluorine compounds I.1.Importance of organofluorine in medicinal chemistry I.2 Synthesis of chiral fluorinated molecules I.3 Summary I Introduction: chiral organofluorine compounds ... methods towards chiral organofluorine molecules as precursors for bioactive compounds 133 List of Schemes Scheme Enantioselective fluorination of 20-deoxycamptothecin 15 Scheme Fluorination of N-phthaloylphenylglycine ... development of organocatalytic methods for the synthesis of chiral organofluorine molecules with focus on nitrogen-containing species as potentially bioactive compounds or synthons towards bioactive...
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Part 1 combinatorial synthesis of n heterocycles part 2  development of polymer supported hantzsch ester

Part 1 combinatorial synthesis of n heterocycles part 2 development of polymer supported hantzsch ester

... A1B1 A1B3 A2B1 A2B2 A2B3 A3B1 A3B2 A3B3 A1B4 A3B4 A2B5 A2B4 C1 A1B2 A1B5 A3B5 C2 C4 C3 Split and react A1B1C1 A1B2C1 A1B1C2 A1B2C2 A1B1C3 A1B2C3 A1B1C4 A1B2C4 A2B1C1 A2B2C1 A2B1C2 A2B2C2 A2B1C3 ... xanthines 31 2. 2 .2 .1 Solution-phase synthesis of substituted xanthines 31 2. 2 .2 .1. 1 Synthesis of benzyl N- butyl glycinate (2- 2 -10 ) 31 2. 2 .2 .1. 2 Synthesis of benzyl 2- (N- butyl -N' -cyanoformamidino) ... aldehydes and aniline and reduction of benzoquinones xiv List of Tables Table 2 -1 Synthesis of 2 -1- 8 24 Table 2- 2 Synthesis of 2 -1- 13 26 Table 2- 3 Synthesis of 2 -1- 7b 26 Table 2- 4 Synthesis of 2- 2 -11 a...
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controllable synthesis of zno architectures by a surfactant-free hydrothermal process

controllable synthesis of zno architectures by a surfactant-free hydrothermal process

... best of knowledge, large-scale fabrication of ZnO tubular radial bunches with changed diameter in each tube has been rarely reported in a surfactant-free hydrothermal process When HMTA was employed, ... concentration of oxygen vacancies and high optical quality of single-crystal ZnO [8,12] Conclusions In summary, various ZnO architectures, especially novel radialized flowerlike structures assembled by ... [0001] um c um d Fig ZnO architectures obtained from ammonia (a) , HMTA (b), EA (c), ED (d) at 90 °C for 20 h The insets of Fig 2b are the SAED pattern and the HRTEM image of a nanotower, respectively...
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Báo cáo hóa học:

Báo cáo hóa học: " Preparation and thermal conductivity of CuO nanofluid via a wet chemical method" potx

... fraction at 25°C The thermal conductivity of the base fluid (H2O) was measured, and it had an average value of 0.580 W·m -1 ·K -1 It can be seen that the thermal conductivity ratio increases as ... al.’s data, Das et al.’s data, and Liu et al.’s data [30-32], suggesting the potential application as heat transfer fluids 12 13 14 Conclusion A wet chemical method to synthesize stable CuO nanofluids ... thermal conductivity ratio of the typical sample, defined as k/k0, where k and k0 are the thermal conductivities of the nanofluids and the base media (H2O) respectively, as a function of the particle...
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Báo cáo hóa học:

Báo cáo hóa học: " The Periodic Instability of Diameter of ZnO Nanowires via a Self-oscillatory Mechanism" pptx

... structure only appears when the diameter of wire is small For nanowires with large diameter, the periodic instability diminishes (Fig 2c) The occurrence of periodic instability of diameter of nanowires ... denotes the atomic volume of O From this equation, we know that diameter of droplet increase and the supersaturation will increase and approach to the value of Dl0/kT In a word, the larger the diameter ... into the droplet lead to the saturation and one-dimensional crystal growth of ZnO This Fig SEM images of periodic bead-like ZnO nanowires on sapphire: (a) low-magnification image of periodic bead-like...
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Báo cáo hóa học:

Báo cáo hóa học: " Sound Synthesis of the Harpsichord Using a Computationally Efficient Physical Model" potx

... partial In practice, the offset ranges from practically Hz to a few Hertz The gain of the resonator, that is, the amplitude of the beating partial, is set to be the same as that of the partial ... further in Section of this paper The idea is to include in these samples the sound of the quill scraping the string plus the beginning of the attack of the sound so that a natural attack is obtained ... supported by several ribs installed in patterns that leave trapezoidal areas of the soundboard vibrating freely The main function of the soundboard is to amplify the weak sound of the vibrating strings,...
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sol–gel synthesis and morphological control of nanocrystalline tio2 via urea treatment

sol–gel synthesis and morphological control of nanocrystalline tio2 via urea treatment

... template-assisted sol–gel approach via urea treatment and under hydrothermal condition for synthesizing the nanocrystalline TiO2 rods and hollow tubes, consisting of aggregates of nanorods of ∼10 nm ... and 5d Conclusions A novel approach adopting the anionic template-assisted sol–gel synthesis via urea treatment and under hydrothermal processing to synthesize the nanocrystalline TiO2 rods and ... complete urea reaction encourages a basic sol–gel reaction system; this allows the surface of TiO2 to be negatively charged because the pH of the sol–gel system is now above the IEP of TiO2 Therefore,...
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synthesis of one-dimensional sno2 nanorods via a hydrothermal technique

synthesis of one-dimensional sno2 nanorods via a hydrothermal technique

... the SnO2 nanorods Fig The XRD pattern of the SnO2 nanorods grown via the hydrothermal method room temperature on a Horiba Jobin Yvon LabRam IR system at a spatial resolution of mm Raman scattering ... consist of nanorods as well as nanoparticles The diameters of SnO2 nanorods are in the range of 100–150 nm with lengths of the order of 1–2 mm The end planes of the nanorods are tetragonal (see ... duration leads to an increase of the surface-to-volume ratio of nanorods The concentration of tin ions in solution also influences to the size of nanorods The formation of SnO2 nanorods was obtained...
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synthesis of single-crystalline hollow b-feooh nanorods via a controlled

synthesis of single-crystalline hollow b-feooh nanorods via a controlled

... before ethanolthermal reaction, (b) hollow b-FeOOH nanorods after ethanol-thermal reaction Figure Thermo-gravimetric analysis (TGA) of the b-FeOOH nanorods: (a) b-FeOOH nanorods gained by maintained ... prepared as above experiment: (a) SEM image of b-FeOOH hollow nanorods, (b) TEM image of b-FeOOH hollow nanorods, (c) HRTEM image and its related Fourier transform electron diffraction pattern of ... the hollow interiors of the nanorods in Figure 2b It can be seen that b-FeOOH hollow nanorods have an average diameter of 20$30 nm and an aspect ratio above 3$4 Almost there is only one big cavity...
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