... Spellman’s Standard Handbook for Wastewater Operators, Vol.1, Technomic Publ., Lancaster, PA, 1999.)© 2003 by CRC Press LLC 392 Handbook of Water and Wastewater Treatment Plant Operations ... Spellman’s Standard Handbook for Wastewater Operators, Vol. 1, Technomic Publ., Lancaster, PA, 1999.)© 2003 by CRC Press LLC 386 Handbook of Water and Wastewater Treatment Plant Operations ... Handbook of Water and Wastewater Treatment Plant Operations 1. Wash each sample bottle or piece of glasswarewith a brush and phosphate-free detergent.2. Rinse three times with cold tap water. 3....