Introduction to Modern Liquid Chromatography, Third Edition part 37 docx

... solutes 1 to 5 increases in proceeding from the Inertsil to the Symmetry to the Discovery column (note the retention ranges for peaks 1–5 in Fig. 7.9b, indicated at the top of each chromatogram ... C 18 column (5-μm particles); mobile phase, 13% acetonitrile-buffer (buffer is citrate plus phosphate); 2.0 mL/min; 35 ◦ C. Peaks for basic compounds 5 to 7 are shaded. Chromatograms based...

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... 5.22b), the ligands are further apart, so as to allow access of both narrow and wide molecules (i and j) to the stationary phase. When a molecule has access to the stationary phase, steric exclusion ... surface area of the particle. 5.4.1.2 Shape Selectivity The following, minor digression examines two distinct forms of steric exclusion; for now, the reader may prefer to skip to Sec...

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... CONSIDERATIONS, 715 14.7.1 Thermodynamics of Solute-Selector Association, 715 Introduction to Modern Liquid Chromatography, Third Edition, by Lloyd R. Snyder, Joseph J. Kirkland, and John W. Dolan Copyright ... Reversed-Phase High Performance Liquid Chromatography,Aca- demic Press, New York, 1984. 169. A. M Striegel, W. W Yau, J. J Kirkland, and D. D Bly, Modern Size-Exclusio...

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... Development for Gradient Prep-LC, 753 15.6 PRODUCTION-SCALE SEPARATION, 754 Introduction to Modern Liquid Chromatography, Third Edition, by Lloyd R. Snyder, Joseph J. Kirkland, and John W. Dolan Copyright ... Chromatogr. A, 906 (2001) 379 . 62. P. Franco, A. Senso, L. Oliveros, and C. Minguill ´ on, J. Chromatogr. A, 906 (2001) 155. 63. T. Ikai, C. Yamamoto, M. Kamigaito, and Y....

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... rules, 583–584 structure vs. chromatography, 583–584 Proteomics, multidimensional liquid chromatography, 616–618 Protocol; see Validation, protocol Pseudocritical chromatography, 654 Pump(s), 104–113 active ... U-HPLC High-pressure liquid chromatography, 8 High-priced liquid chromatography; see U-HPLC High-speed liquid chromatography, 8 HILIC, see Hydrophilic interaction chr...

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... Hybrid Systems, 111 INTRODUCTION TO MODERN LIQUID CHROMATOGRAPHY Third Edition LLOYD R. SNYDER LC Resources, Inc. Orinda, CA JOSEPH J. KIRKLAND Advanced Materials Technology Wilmington, DE JOHN W. ... Lloyd R. Introduction to modern liquid chromatography / Lloyd R. Snyder, Joseph J. Kirkland. – 3rd ed. / John W. Dolan. p. cm. Includes index. ISBN 978-0-470-16754-0 (cloth)...

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... 158 4.3 Introduction to Individual Detectors, 160 4.4 UV-Visible Detectors, 160 4.4.1 Fixed-Wavelength Detectors, 163 4.4.2 Variable-Wavelength Detectors, 164 4.4.3 Diode-Array Detectors, 165 4.4.4 ... 113 3.6 Autosamplers, 113 3.6.1 Six-Port Injection Valves, 114 3.6.1.1 Filled-Loop Injection, 114 3.6.1.2 Partial-Loop Injection, 115 3.6.2 Autosampler Designs, 116 3.6.2.1 Pull -to- Fill A...

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... 651 13.10.3 Liquid- Chromatography Modes for Polymer Analysis, 653 13.10.3.1 Size-Exclusion Chromatography, 653 13.10.3.2 Interactive Liquid Chromatography, 653 13.10.3.3 Liquid Chromatography under Critical ... RPC- 5 Chromatography, 623 13.5.3 Hydrophobic Interaction Chromatography, 624 13.6 Separation of Carbohydrates, 625 13.6.1 Hydrophilic Interaction Chromatography, 625 1...

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... interaction chromatography HILIC hydrophilic interaction chromatography i.d. column or tubing inner diameter (mm) IEC ion-exchange chromatography IPC ion-pair chromatography k retention factor (same ... retention factor (same as capacity factor k  ); equal to (t R /t 0 ) − 1 k ∗ gradient retention factor; Equation (9.5) L column length (mm) LC-MS liquid chromatography–mass spectrometry L...

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... most laboratories that deal with a need for analyzing chemical mixtures are equipped for HPLC; it is often the first choice of technique Introduction to Modern Liquid Chromatography, Third Edition, ... Do?, 4 1.2 A SHORT HISTORY OF HPLC, 6 1.3 SOME ALTERNATIVES TO HPLC, 8 1.3.1 Gas Chromatography (GC), 8 1.3.2 Thin-Layer Chromatography (TLC), 9 1.3.3 Supercritical Fluid Chromato...

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