TRUONG DAI HOC SU PHAM

Một phần của tài liệu Khóa luận tốt nghiệp Hóa học: Nghiên cứu sự tạo phức giữa Zn(II) và thuốc thử Canmagit trong môi trường nước và ứng dụng trong chuẩn độ Complexon (Trang 77 - 94)

Spectrophotometer Biochrom 4060

Title Duong cong bao hoa Zn(II) _canmagit Filename PBH23.QE2

Operator My Phu

Comments Cannagit=10^-4 Date 16 April 2003 Number of replicates 1

Wavelength $20.9 nm Temperature OFF

Standard Slope Method Linear Interpolation

Conc, Mean{Abs)

0.500 0.058 1.000 0.091

2.000 0.199 ẹ

3.000 0.289 ?

4.000 0.365 4.500 0.380 4.800 0.380 5.000 0.392 5.500 0.389 6.000 0.390

7.000 0.396

10 May 2003 +

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Spectrophotometer Biochrom 4060

Title duong cong bao hoa Zn(iI) Canmagit Filename PBH24.QE2

Operator My Phu

Comments Canmagit=10^~=4

Date 17 April 2003 Number of replicates 1

@avelength 520.0 nom

Temperature OFF

Standard Slope Method Linear Interpolation

Conc, Mean(Abs)

0.500 0.058

1.000 0.103

2.000 0.190 `.

3.000 0.272 4.000 0.360

4.500 0.377 5.000 0.381

5.500 0.391

6.000 0.393

10 May 2003 +®

Spectrophotometer Biochrom 4060

Title duong cong bao hoa Zn(II) Canmagit

Filename PBH25 .QE2

Operator My Phu.

Comments Canmagit+10°-4 Date 18 April 2003 Number of replicates 1

Wavelength 520.0 nm Temperature OFF

Standard Slope Method Linear Interpolation

Conc. Mean(Abs)

0.500 0.053 1.000 0.112

2.000 0.194 %e 3.000 0.277

4.000 0.359 4.500 0.374 5.000 0.393 5.500 0.403 6.000 0.403 7.000 0.401

8.000 0.398

0.050

3,000 4000

Concentration (mi)

1000 2.000

10 May 2003 +%

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Spectrophotometer Biochrom 4060

Title duong cong bao hoa Zn(II) Canmagit Filename PBH21.QE2

Operator My Phu

Comments Canmagit=10^~4 Date 15 April 2003 Number of replicates ‡

Wavelength $42.0 nm

Temperature OFF

Standard Slope Method Linear Interpolation

Conc. Meae(Abs)

1,000 0,069 2,000 0.138

3,000 0.204

4.000 0.267 ‘e 4.500 0.268

4.800 0.273 5,000 0.262 6.000 0.272

7,000 0,287

Abs

0.200

0.150

0.100

error

10 May 2003 T

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Spectrophotometer Biochrom 4060

Title Duong cong bao hoa Zn(II) Calmagite

Filename PBH8 .QE2 F i

Operator My Phu Cat - 4p

Comments Calmagite=2°10(-4) ,pH=9,5 : ie Date 12 April 2003 an fil?

Number of replicates 1 - ứ. me â

Wavelength 542.0 nm “ Avr

Temperature OFF - u

Standard Slope Method Linear Interpolation lô

Conc, Mean(Abs)

1.000 0.054 2.000 0.154 4.000 0.310

6.000 0.454 M 9.000 0.561

10.00 0.564 11.00 0.597 12.00 0.577 14.00 0.571

10 May 2003 , k¿

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Spectrophotometer Biochrom 4060 Title Untitled

Filename PBH11.QE2

Operator Comments

Date 12 April 2003 Number of replicates 1

Wavelength $20.0 nm

Temperature OFF

Standard Slope Method Linear Interpolation

Conc, Mean(Abs)

1.000 0.065 2.000 0.185

4.000 0.370 c

6.000 0.544 ˆ”

9.000 0.712 9.000 0.74e 10.00 0.782

11.00 0.776

10 May 2003 % +

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Spect rophotometer Biochrom 4060

Title Duong cong bao hoa Zn(II) Calmagite

Filename PBH14.QE2

Operator My Phu

Comments ph^9, 5;Calmagite=5*10(-5) Date 14 April 2003

Number of replicates 1

Wavelencth 520.0 nm

Temperature OFF

Standard Slope Method Linear Interpolation

Conc. Mean{Abs)

0.500 0.054 1.000 0.083

1.500 0.119 s

1.800 0.148 v

2.200 0.181 2.500 0.186 2.800 0.197 3.500 0.185

Abs Duong cong bao hoa Zn(11)_Calmaglte "ơ — off

BH 14.QE2 — = - 0.200 : . — .

` |

0150. KP. san

: ||

| PI

FT Se eee ÔNH:00N Go

| “

"4

0050 | <S——__________ ————

0.500 1.000 1.500 2.000 2.500 3.000

J9 April 2905

——— —-- seu ^ ~ .~~ aR

$ == BES SP ees

= <

io ceằ thi cua t& Ca:magice

Rod aaa a a

r..4-3::ie fe to da

lệằ: Lai La sy Pt

Tse 5 So, == Z a5

— a ° le œ - ST 3

_-. Meee & 46

iuasac :f - $e 2

Weveler it a te feaca as :.= SIF

Se ees TS: ì -Ýt6€ÀtC OS Tarsocstion

V.” + *e P

`“.

ĐÓ 2 TES = cavesPA

ra

...^.

wae

meat —

seers 188%

~363

-Ắ.e*~Ýce

2432

ee239

ahaa nd

`

10 May 2003 : 3L

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Spectrophotometer Biochrom 4060

Title Do thi phuc Zn_tt theo pp dg cg bao hoa Filename P_PBH3.QE2

Operator My Phu

Comments Zn#2°10(-4)

Date 09 April 2003 Number of replicates 1

Wavelength 520.0 nm Temperature OFF

Standard Slope Method Linear Interpolation

Conc. Mean{Abs)

0.500 0.056 1.000 0.092

2.000 0.172

3.000 0.261 `

4.000 0.359 5.000 0.432 6.000 0.519

7.009 0.613

8.000 0.696 9.000 0.785 10.00 0.984 12.00 1.034 15.00 1.196

21 May 2003 ' 3L

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Spectrophotometer Biochrom 4060 Title MDQ tt theo pH

Filename P_PHT1.QE2

Operator My Phu

Comments Cal=l0^-4; Zn=S*10*-5 Date 27 April 2003

Number of replicates 1

Wavelength 520.0 nm

Temperature OFF

Standard Slope Method Linear Interpolation

Conc, Mean/ Abs)

2.300 0.886 3.000 0.875 3.500 0.988

4.000 0.885 v„

4.500 0.903 5,000 0.882 5.500 0.879 6.000 0.857 6.500 0.846

7.000 0.785 7.500 0.727

8.000 0.626

8.500 0.554

9.000 0.527

9.500 0.509 10.00 9.513

10.50 0.496 11.00 0.485 11.50 0.488 12.00 0.404

21 May 2003 $4

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Spectrophotometer Biochrom 4060

Title MDQ phuc theo pH Filename P_PHP1.QE2

Operator My Phu

Comments Cal=1l0^-4; Zn*5*10^-Š Date 27 April 2003

Number of replicates 1

Wavelength 520.0 nm Temperature OFF

Standard Slope Method Linear Interpolation

Conc, Mean(Abs)

2.300 0.876 3.000 0.889 3.500 0.883 4.000 0.877

4.500 0.898

5.000 0.884

5.500 0.866 6.000 0.876

6.$00 0.872 7.000 0.873 7.500 0.888 8.000 0.918

8.500 0.892 9.000 0.894 9.$00 0.888 10.00 0.848

10.50 0.827 11.00 0.814 11.50 0.626 12.00 0.429

TRUONG DAI HỌC SU PHAM

ctrophotometer Biochrom 4060

le Pho cua phuc o cac gia tri pH ename P4.Ws5

rator ments

e 11 April 2003

,

Fllenarme Tite

- PP-01-WwS2 Scan phuc(8,5 11)

PP-02.WS2 Scan phuc(8,5 11)

PP-05.WS2 Scan phuc(8,5 11)

PP-06.WS2 Đoan _phuc(8,5_ 11)

PH 3C~01,W$2 Scan phí4-5~=6) PH Sc-02.WS2 Scan phi4-5-6) PH SC-03.WS2 Scan phi4-5-6)

se me |

350.0 400.0 450.0 500.0 550.0 600.0 650.0 700.0 750.0 8000 Wavelength

May 2003 %

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Spectrophotometer Biochrom 4060 Title MDQ tt theo pH

Filename PPH3.QE2 Operator My Phu

Comments Calmagite=10*-4;Zn#5°10*-5 Date 25 April 2003

Number of replicates 1

Wavelength 520.0 nm

Temperature OFF

Standard Slope Method Linear Interpolation

Cons, Mean(Abs)

6.000 0.872 6.500 0.850

7.000 0.818

7.500 0.7141 Ủ*

8.000 0.642

‘aay 2003 %

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Spectrophotometer Biochrom 4060

Title MDQ cua phuc theo pH

Filename PPH22.QE2 Operator My Phu

Comments Calmagite=Zn(II)=10(-4)

Date 22 April 2003 Number of replicates 1

Wavelength $20.0 nm Temperature Orr

Standard Slope Method Linear Interpolation

Conc, Mean( Abs)

€.000 0.875 6.500 0.897

7.000 0.898

7.500 0.907 ,,

8.000 0.903 8.500 0.905

“TỔ Hay 2003 Lần

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Spectrophotometer Biochrom 4060

Title MDQ CUA TT THEO pH

Filename PPHSA.QE2 Operator My Phu

Comments Cal#10°-4; Zn=5*10%-S(dl) Date 28 April 2003

Number of replicates 1

Wavelength 520.0 nm

Temperature OFF

Standard Slope Method Linear Interpolation

Conc. Mean(Abs)

6.000 0.874 6.500 0.842 7.000 0.792

7.500 0.708 *+

8.000 0.625 8.500 0.568

3 May 2003

Spectrophotometer

Title

Filename

Operator Comments

Date

Number of replicates

Wavelength Temperature

Standard Slope Method

Conc,

„000 .500 .000

.500 ,000

œ Œ ~ ~1 Ơa ƠŒ:.500

Mean{Abs)

0.879

0.892 0.8802

0.887 0.911 0.894

3

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Biochrom 4060

MDQ CUA PHUC THEO pH PPH2€.QE2

My Phu

Cal=10%-4; Zn=5*10^=5 28 April 2003

1

520.0 nm OFF

Linear Interpolation

9

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"19 May 2003

Spectrophotometer

Title

Filename

Operator

Comments Date

Number of replicates

Wavelength Temperature

Standard Slope Method

Conc, Mean(Abs)

6.000 0.872 6.500 0.859

7.000 0.812

7.500 0.738 |

9.000 0.633 °°

8.500 0.597

. ——

| ——

0.850 |

|

0.800

0.750 |

0.700 =

0.650 | ——

0.600 —

——

6.000 6.500

Biochrom 4060

MDQ tt theo pH PPH4.QE2

My Phu

Cal=i0^-4;5*10^-5, (lan 2)

25 April 2003 1

520.0 nm OFF

Linear Interpolation

„9 May 2003

Spectrophotometer Title

Filename

Operator Comments

Date

Number of replicates Wavelength

Temperature

Standard Slope Method

Cone,

-000 -500 -900 .500

„900

eer oy„500

Mean(Abs)

0.878 0.879

0.880 0.903

0.912 *

0.908

yO

Một phần của tài liệu Khóa luận tốt nghiệp Hóa học: Nghiên cứu sự tạo phức giữa Zn(II) và thuốc thử Canmagit trong môi trường nước và ứng dụng trong chuẩn độ Complexon (Trang 77 - 94)

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