DTA MẪU BÙN ĐỎ (NHÀ MÁY HỐ CHẤT TÂN BÌNH) DTA MẪU DIATOMIT LÂM ĐỒNG DTA MẪU 0% NaOH (50% BÙN ĐỎ+50% DIATOMIT) – 150 oC DTA MẪU 5% NaOH (50% BÙN ĐỎ+50% DIATOMIT) – 150 oC DTA MẪU 10% NaOH (50% BÙN ĐỎ+50% DIATOMIT)- 150 oC DTA MẪU 15% NaOH (50% BÙN ĐỎ+50% DIATOMIT) – 150 oC 3800 3500 3200 2900 2600 2300 Sample: DIATOMITE Resolution: Technique: KBr Nr of Scans: Measured by: Nguyen Quoc Viet Source: MIR 2000 1800 1600 Wavenumber cm-1 1400 Aperture: 6mm 32 Scanner Velocity: 10 KHz 1200 1000 900 800 700 600 Intruments: TENSOR37 466 535 696 797 755 913 1037 1641 3441 3698 3622 10 20 Transmittance [%] 30 40 50 60 IR MẪU DIATOMIT NGUYÊN LIỆU 500 400 3800 3500 3200 2900 2600 2300 Sample: BUN DO Resolution: Technique: KBr Nr of Scans: Measured by: Nguyen Quoc Viet Source: MIR 2000 1800 1600 Wavenumber cm-1 1400 Aperture: 6mm 32 Scanner Velocity: 10 KHz 1200 1000 900 800 455 802 1002 1410 1477 1639 3434 3620 20 Transmittance [%] 30 40 50 60 IR MẪU BÙN ĐỎ NGUYÊN LIỆU 700 600 Intruments: TENSOR37 500 400 3800 3500 3200 2900 2600 2300 2000 Nr of Scans: Measured by: Nguyen Quoc Viet Source: MIR 1400 Aperture: 6mm Sample: GEO-POLYMER 0%XUT-120 C Resolution: Technique: KBr 1800 1600 Wavenumber cm-1 32 Scanner Velocity: 10 KHz 1200 413 472 535 694 799 914 1032 1635 3697 3621 3525 3459 10 20 30 Transmittance [%] 40 50 60 IR MẪU 0% NaOH Ở 120oC (50% BÙN ĐỎ+50% DIATOMIT) 1000 900 800 700 600 500 400 Intruments: TENSOR37 3800 3500 3200 2900 2600 2300 2000 Sample: GEO-POLYMER 5%XUT-120 C Resolution: Technique: KBr Nr of Scans: Measured by: Nguyen Quoc Viet Source: MIR 1800 1600 Wavenumber cm-1 1400 Aperture: 6mm 32 Scanner Velocity: 10 KHz 1200 465 428 535 694 797 914 1031 1443 1641 3438 3697 3621 10 20 Transmittance [%] 30 40 50 60 IR MẪU 5% NaOH Ở 120oC (50% BÙN ĐỎ+50% DIATOMIT) 1000 900 800 700 600 500 400 Intruments: TENSOR37 XUTBÙN 120 ĐỎ+50%DIATOMIT) XRD MẪUMAU_GEO 5%NaOHPOLYMER Ở 120 oC (50% 200 190 180 170 160 150 140 130 110 100 90 d=3.33285 80 d=4.82841 Lin (Counts) 120 70 60 50 40 30 20 10 15 20 30 40 50 2-Theta - Scale MAU_GEO POLYMER XUT 120 - File: MAU_GEO POLYMER XUT 120.raw - Type: 2Th/Th locked - Start: 15.000 ° - End: 60.000 ° - Step: 0.030 ° - Step time: s - Temp.: 25 °C (Room) - Ti XRD MẪU 10%NaOH Ở 120 oC10(50% MAU_GEO POLYMER XUT BÙN 120 ĐỎ+50%DIATOMIT) 200 190 180 170 160 150 140 130 110 100 d=4.82540 90 80 70 40 30 d=1.81643 50 d=3.33341 60 d=4.11897 Lin (Counts) 120 20 10 15 20 30 40 50 60 2-Theta - Scale MAU_GEO POLYMER 10 XUT 120 - File: MAU_GEO POLYMER 10 XUT 120.raw - Type: 2Th/Th locked - Start: 15.000 ° - End: 65.010 ° - Step: 0.030 ° - Step time: s - Temp.: 25 °C (Room) - 15 XUT 120 ĐỎ+50%DIATOMIT) XRD MẪU MAU_GEO 15%NaOHPOLYMER Ở 120 oC (50% BÙN 200 190 180 170 160 150 140 130 110 100 90 60 50 40 30 d=3.33378 d=4.08131 70 d=2.68631 d=2.67236 d=3.16327 80 d=4.97880 Lin (Counts) 120 20 10 15 20 30 40 50 60 2-Theta - Scale MAU_GEO POLYMER 15 XUT 120 - File: MAU_GEO POLYMER 15 XUT 120.raw - Type: 2Th/Th locked - Start: 15.000 ° - End: 65.010 ° - Step: 0.030 ° - Step time: s - Temp.: 25 °C (Room) - MAU_GEO POLYMER XUT 120 XRD MẪU 0%NaOH Ở 120 oC0(50% BÙN ĐỎ+50%DIATOMIT) 200 190 180 170 160 150 140 130 110 100 90 80 50 d=3.34229 60 d=4.37582 70 d=4.84176 Lin (Counts) 120 40 30 20 10 15 20 30 40 50 60 2-Theta - Scale MAU_GEO POLYMER XUT 120 - File: MAU_GEO POLYMER XUT 120.raw - Type: 2Th/Th locked - Start: 15.000 ° - End: 65.010 ° - Step: 0.030 ° - Step time: s - Temp.: 25 °C (Room) - Ti MAU_POLYMER XUTBÙN ĐỎ+50%DIATOMIT) XRD MẪU 0%NaOH Ở 150 oC_0 (50% 350 340 330 320 310 300 290 280 270 260 250 240 230 220 210 190 180 170 160 150 140 130 120 110 100 90 70 d=3.33100 80 d=4.82634 Lin (Counts) 200 60 50 40 30 20 10 15 20 30 40 50 60 70 2-Theta - Scale MAU_POLYMER _0 XUT - File: MAU_POLYMER _0 XUT.raw - Type: 2Th/Th locked - Start: 15.000 ° - End: 75.000 ° - Step: 0.030 ° - Step time: s - Temp.: 25 °C (Room) - Time Started: 24 s - MAU_POLYMER _5 XUT XRD MẪU 5%NaOH Ở 150 oC (50% BÙN ĐỎ+50%DIATOMIT) 350 340 330 320 310 300 290 280 270 260 250 240 230 220 210 190 180 170 160 150 140 130 120 110 100 90 80 70 60 d=3.33477 d=4.83403 Lin (Counts) 200 50 40 30 20 10 15 20 30 40 50 60 70 2-Theta - Scale MAU_POLYMER _5 XUT - File: MAU_POLYMER _5 XUT.raw - Type: 2Th/Th locked - Start: 15.000 ° - End: 75.000 ° - Step: 0.030 ° - Step time: s - Temp.: 25 °C (Room) - Time Started: 19 s - MAU_GEO POLYMER _10 XUT XRD MẪU 10%NaOH Ở 150 oC (50% BÙN ĐỎ+50%DIATOMIT) 350 340 330 320 310 300 290 280 270 260 250 240 230 220 210 190 180 170 160 150 140 130 120 110 100 d=3.33973 Lin (Counts) 200 90 80 70 60 50 40 30 20 10 15 20 30 40 50 60 70 2-Theta - Scale MAU_GEO POLYMER _10 XUT - File: MAU_GEO POLYMER _10 XUT.raw - Type: 2Th/Th locked - Start: 15.000 ° - End: 75.000 ° - Step: 0.030 ° - Step time: s - Temp.: 25 °C (Room) - Time o XRD MẪU 15%NaOH Ở 150 C (50%_15 BÙN ĐỎ+50%DIATOMIT) MAU_GEO POLYMER XUT 350 340 330 320 310 300 290 280 270 260 250 240 230 220 210 d=3.43128 190 180 170 160 150 100 90 30 d=1.68940 d=1.90658 d=2.22598 d=2.51030 40 d=2.69322 50 d=3.17106 60 d=3.65959 70 d=4.11019 d=4.84831 80 20 10 15 20 30 40 50 60 2-Theta - Scale MAU_GEO POLYMER _15 XUT - File: MAU_GEO POLYMER _15 XUT.raw - Type: 2Th/Th locked - Start: 15.000 ° - End: 69.780 ° - Step: 0.030 ° - Step time: s - Temp.: 25 °C (Room) - Time 01-083-1735 (C) - Analcime - Na15.92Al15.84Si32.16O96(H2O)16 - WL: 1.5406 - Body-centered - Tetragonal - a 13.72100 - b 13.72100 - c 13.73500 - alpha 90.000 - beta 90.000 - gamma 90.00 d=1.34991 110 d=1.37648 120 d=2.92451 130 d=1.54189 140 d=5.59894 Lin (Counts) 200 o XRD MẪU 0%NaOHMAU_0 Ở 200 DIATOMETE C (50% BÙN ĐỎ+50%DIATOMIT) 150 140 130 120 110 90 80 70 60 40 d=3.33039 50 d=4.82652 Lin (Counts) 100 30 20 10 10 20 30 40 50 60 2-Theta - Scale MAU_0 DIATOMETE - File: MAU_0 DIATOMETE.raw - Type: 2Th/Th locked - Start: 10.000 ° - End: 70.000 ° - Step: 0.030 ° - Step time: s - Temp.: 25 °C (Room) - Time Started: 16 s - 2-Th 01-085-0335 (C) - Quartz low - SiO2 - WL: 1.5406 - Hexagonal - a 4.91340 - b 4.91340 - c 5.40520 - alpha 90.000 - beta 90.000 - gamma 120.000 - Primitive - P3221 (154) - - 113.007 - I/Ic MAU_5 DIATOMETE XRD MẪU 5%NaOH Ở 200 oC (50% BÙN ĐỎ+50%DIATOMIT) 150 140 130 120 110 d=3.34214 Lin (Counts) 100 90 80 70 60 50 40 30 20 10 10 20 30 40 50 60 2-Theta - Scale MAU_5 DIATOMETE - File: MAU_5 DIATOMETE.raw - Type: 2Th/Th locked - Start: 10.000 ° - End: 70.000 ° - Step: 0.030 ° - Step time: s - Temp.: 25 °C (Room) - Time Started: 18 s - 2-Th 01-085-0335 (C) - Quartz low - SiO2 - WL: 1.5406 - Hexagonal - a 4.91340 - b 4.91340 - c 5.40520 - alpha 90.000 - beta 90.000 - gamma 120.000 - Primitive - P3221 (154) - - 113.007 - I/Ic XRD MẪU 10%NaOHMAU_10 Ở 200 oDIATOMETE C (50% BÙN ĐỎ+50%DIATOMIT) 150 140 130 120 110 90 80 70 d=1.35290 d=1.37361 d=1.51671 d=1.67236 30 d=1.87634 40 d=2.50652 d=2.92343 50 d=2.68737 60 d=3.42510 d=5.59206 Lin (Counts) 100 20 10 10 20 30 40 50 60 2-Theta - Scale MAU_10 DIATOMETE - File: MAU_10 DIATOMETE.raw - Type: 2Th/Th locked - Start: 10.000 ° - End: 70.000 ° - Step: 0.030 ° - Step time: s - Temp.: 25 °C (Room) - Time Started: 18 s - 201-074-2219 (C) - Analcime - Na(AlSi2O6)H2O - WL: 1.5406 - Cubic - a 13.72000 - b 13.72000 - c 13.72000 - alpha 90.000 - beta 90.000 - gamma 90.000 - Body-centered - Ia-3d (230) - 16 01-085-0335 (C) - Quartz low - SiO2 - WL: 1.5406 - Hexagonal - a 4.91340 - b 4.91340 - c 5.40520 - alpha 90.000 - beta 90.000 - gamma 120.000 - Primitive - P3221 (154) - - 113.007 - I/Ic XRD MẪU 15%NaOH 200 oC (50% BÙN200 ĐỎ+50%DIATOMIT) MAU_GEO Ở POLYMER _15 XUT 350 340 330 320 310 300 d=3.43348 290 280 270 260 250 240 230 d=5.60865 210 200 190 180 170 d=2.92729 160 150 140 130 120 110 d=1.34581 d=1.37537 d=1.43910 d=1.90592 d=1.56132 30 d=1.74401 d=1.71629 40 d=1.98950 50 d=2.42710 60 d=3.66344 70 d=2.69442 80 d=2.80362 90 d=2.50693 100 d=4.85295 Lin (Counts) 220 20 10 10 20 30 40 50 60 70 2-Theta - Scale MAU_GEO POLYMER _15 XUT 200 - File: MAU_GEO POLYMER _15 XUT 200.raw - Type: 2Th/Th locked - Start: 10.000 ° - End: 75.010 ° - Step: 0.030 ° - Step time: s - Temp.: 25 °C (Room) - Time Started Operations: Smooth 0.100 | Strip kAlpha2 0.500 | Background 1.000,0.100 | Import 01-083-1735 (C) - Analcime - Na15.92Al15.84Si32.16O96(H2O)16 - WL: 1.5406 - Body-centered - Tetragonal - a 13.72100 - b 13.72100 - c 13.73500 - alpha 90.000 - beta 90.000 - gamma 90.000 - I41/acd (14 ... MẪU 0% NaOH (50% BÙN ĐỎ+50% DIATOMIT) – 150 oC DTA MẪU 5% NaOH (50% BÙN ĐỎ+50% DIATOMIT) – 150 oC DTA MẪU 10% NaOH (50% BÙN ĐỎ+50% DIATOMIT)- 150 oC DTA MẪU 15% NaOH (50% BÙN ĐỎ+50% DIATOMIT)... (50% BÙN ĐỎ+50% DIATOMIT) 500 400 PHÂN TÍCH HIỂN VI NHIỆT MẪU BÙN ĐỎ NGUYÊN LIỆU PHÂN TÍCH HIỂN VI NHIỆT MẪU 0% NaOH (50% BÙN ĐỎ + 50% DIATOMIT)-150 oC PHÂN TÍCH HIỂN VI NHIỆT MẪU 5% NaOH (50% BÙN... NHIỆT MẪU 5% NaOH (50% BÙN ĐỎ + 50% DIATOMIT)-150 oC PHÂN TÍCH HIỂN VI NHIỆT MẪU 10% NaOH (50% BÙN ĐỎ + 50% DIATOMIT)-150 oC PHÂN TÍCH HIỂN VI NHIỆT MẪU 15% NaOH (50% BÙN ĐỎ + 50% DIATOMIT)-150 oC