Bsi bs en 12697 17 2017

BS EN 12697-17:2017 BSI Standards Publication Bituminous mixtures — Test methods Part 17: Particle loss of porous asphalt specimens BS EN 12697-17:2017 BRITISH STANDARD National foreword This British Standard is the UK implementation of EN 12697-17:2017 It supersedes BS EN 12697-17:2004 which is withdrawn The UK participation in its preparation was entrusted to Technical Committee B/510/1, Asphalt products A list of organizations represented on this committee can be obtained on request to its secretary This publication does not purport to include all the necessary provisions of a contract Users are responsible for its correct application © The British Standards Institution 2017 Published by BSI Standards Limited 2017 ISBN 978 580 91781 ICS 93.080.20 Compliance with a British Standard cannot confer immunity from legal obligations This British Standard was published under the authority of the Standards Policy and Strategy Committee on 28 February 2017 Amendments/corrigenda issued since publication Date Text affected BS EN 12697-17:2017 EN 12697-17 EUROPEAN STANDARD NORME EUROPÉENNE EUROPÄISCHE NORM February 2017 ICS 93.080.20 Supersedes EN 12697-17:2004+A1:2007 English Version Bituminous mixtures - Test methods - Part 17: Particle loss of porous asphalt specimens Mélanges bitumineux - Méthodes d'essai - Partie 17 : Perte de matériau des éprouvettes d'enrobé drainant Asphalt - Prüfverfahren - Teil 17: Kornverlust von Probekörpern aus offenporigem Asphalt This European Standard was approved by CEN on 25 December 2016 CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN member This European Standard exists in three official versions (English, French, German) A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management Centre has the same status as the official versions CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and United Kingdom EUROPEAN COMMITTEE FOR STANDARDIZATION COMITÉ EUROPÉEN DE NORMALISATION EUROPÄISCHES KOMITEE FÜR NORMUNG CEN-CENELEC Management Centre: Avenue Marnix 17, B-1000 Brussels © 2017 CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Members Ref No EN 12697-17:2017 E BS EN 12697-17:2017 EN 12697-17:2017 (E) Contents Page European foreword Scope Normative references Apparatus Preparation of test specimens Procedure Calculation Test report Precision 10 BS EN 12697-17:2017 EN 12697-17:2017 (E) European foreword This document (EN 12697-17:2017) has been prepared by Technical Committee CEN/TC 227 “Road materials”, the secretariat of which is held by DIN This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by August 2017, and conflicting national standards shall be withdrawn at the latest by August 2017 Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights CEN shall not be held responsible for identifying any or all such patent rights This document supersedes EN 12697-17:2004+A1:2007 Compared with EN 12697-17:2004+A1:2007 the following changes have been made: a) change from size (diameter/height of specimen) to mass for the suitability of specimen (4.2); b) Clause 4.3, changed to description of manufacturing and coring when using asphalt with aggregate size larger than 16 mm Text from (4.3) transferred to (4.4) with addition of reference to EN 126975 for determination of maximum density; c) New clause 4.5; detailed definition of the storage time with addition of explaining NOTE; d) age of specimen and storage conditions added to the test report (Clause 7); e) Clause 6.3, including NOTE, deleted The void content and density shall always be reported (NOTE transferred to 4.4); f) Clause Bullet point e) “if required” deleted To be in line with the deletion of clause 6.3 This document has been prepared under a mandate given to CEN by the European Commission and the European Free Trade Association This European Standard is one of a series of standards as listed below: — EN 12697-1, Bituminous mixtures — Test methods — Part 1: Soluble binder content — EN 12697-2, Bituminous mixtures — Test methods — Part 2: Determination of particle size distribution — EN 12697-3, Bituminous mixtures — Test methods — Part 3: Bitumen recovery: Rotary evaporator — EN 12697-4, Bituminous mixtures — Test methods — Part 4: Bitumen recovery: Fractionating column — EN 12697-5, Bituminous mixtures — Test methods — Part 5: Determination of the maximum density — EN 12697-6, Bituminous mixtures — Test methods — Part 6: Determination of bulk density of bituminous specimens — EN 12697-7, Bituminous mixtures — Test methods — Part 7: Determination of bulk density of bituminous specimens by gamma rays BS EN 12697-17:2017 EN 12697-17:2017 (E) — EN 12697-8, Bituminous mixtures — Test methods — Part 8: Determination of void characteristics of bituminous specimens — EN 12697-10, Bituminous mixtures — Test methods — Part 10: Compactability — EN 12697-11, Bituminous mixtures — Test methods — Part 11: Determination of the affinity between aggregate and bitumen — EN 12697-12, Bituminous mixtures — Test methods — Part 12: Determination of the water sensitivity of bituminous specimens — EN 12697-13, Bituminous mixtures — Test methods — Part 13: Temperature measurement — EN 12697-14, Bituminous mixtures — Test methods — Part 14: Water content — EN 12697-15, Bituminous mixtures — Test methods — Part 15: Determination of the segregation sensitivity — EN 12697-16, Bituminous mixtures — Test methods — Part 16: Abrasion by studded tyres — EN 12697-17, Bituminous mixtures — Test methods — Part 17: Particle loss of porous asphalt specimen — EN 12697-18, Bituminous mixtures — Test methods — Part 18: Binder drainage — EN 12697-19, Bituminous mixtures — Test methods — Part 19: Permeability of specimen — EN 12697-20, Bituminous mixtures — Test methods — Part 20: Indentation using cube or cylindrical specimens (CY) — EN 12697-21, Bituminous mixtures — Test methods — Part 21: Indentation using plate specimens — EN 12697-22, Bituminous mixtures — Test methods — Part 22: Wheel tracking — EN 12697-23, Bituminous mixtures — Test methods — Part 23: Determination of the indirect tensile strength of bituminous specimens — EN 12697-24, Bituminous mixtures — Test methods — Part 24: Resistance to fatigue — EN 12697-25, Bituminous mixtures — Test methods — Part 25: Cyclic compression test — EN 12697-26, Bituminous mixtures — Test methods — Part 26: Stiffness — EN 12697-27, Bituminous mixtures — Test methods — Part 27: Sampling — EN 12697-28, Bituminous mixtures — Test methods — Part 28: Preparation of samples for determining binder content, water content and grading — EN 12697-29, Bituminous mixtures — Test methods — Part 29: Determination of the dimensions of a bituminous specimen — EN 12697-30, Bituminous mixtures — Test methods — Part 30: Specimen preparation by impact compactor BS EN 12697-17:2017 EN 12697-17:2017 (E) — EN 12697-31, Bituminous mixtures — Test methods — Part 31: Specimen preparation by gyratory compactor — EN 12697-32, Bituminous mixtures — Test methods — Part 32: Laboratory compaction of bituminous specimens by vibratory compactor — EN 12697-33, Bituminous mixtures — Test methods — Part 33: Specimen prepared by roller compactor — EN 12697-34, Bituminous mixtures — Test methods — Part 34: Marshall test — EN 12697-35, Bituminous mixtures — Test methods — Part 35: Laboratory mixing — EN 12697-36, Bituminous mixtures — Test methods — Part 36: Determination of the thickness of a bituminous pavement — EN 12697-37, Bituminous mixtures — Test methods — Part 37: Hot sand test for the adhesivity of binder on precoated chippings for HRA — EN 12697-38, Bituminous mixtures — Test methods — Part 38: Common equipment and calibration — EN 12697-39, Bituminous mixtures — Test methods — Part 39: Binder content by ignition — EN 12697-40, Bituminous mixtures — Test methods — Part 40: In situ drainability — EN 12697-41, Bituminous mixtures — Test methods — Part 41: Resistance to de-icing fluids — EN 12697-42, Bituminous mixtures — Test methods — Part 42: Amount of foreign matters in reclaimed asphalt — EN 12697-43, Bituminous mixtures — Test methods — Part 43: Resistance to fuel — EN 12697-44, Bituminous mixtures — Test methods — Part 44: Crack propagation by semi-circular bending test — EN 12697-45, Bituminous mixtures — Test methods — Part 45: Saturation ageing tensile stiffness (SATS) conditioning test — EN 12697-46, Bituminous mixtures — Test methods — Part 46: Low temperature cracking and properties by uniaxial tension tests — EN 12697-47, Bituminous mixtures — Test methods — Part 47: Determination of the ash content of natural asphalts — prEN 12697-48, Bituminous mixtures — Test methods for hot mix asphalt — Part 48: Interlayer Bonding — EN 12697-49, Bituminous mixtures — Test methods — Part 49: Determination of friction after polishing — CEN/TS 12697-50, Bituminous mixtures — Test methods — Part 50: Resistance to scuffing BS EN 12697-17:2017 EN 12697-17:2017 (E) — FprCEN/TS 12697-51, Bituminous mixtures — Test methods — Part 51: Surface shear strength test 1) — FprCEN/TS 12697-52, Bituminous mixtures — Test methods — Part 52: Conditioning to address oxidative ageing — prEN 12697-53, Bituminous mixtures — Test methods — Part 53: Cohesion increase by spreadabilitymeter method According to the CEN-CENELEC Internal Regulations, the national standards organisations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and the United Kingdom In preparation BS EN 12697-17:2017 EN 12697-17:2017 (E) Scope This European Standard specifies a test method for determining the particle loss of porous asphalt mixtures Particle loss is assessed by the loss of mass of porous asphalt samples after turns in the Los Angeles machine This test enables the estimation of the abrasion resistance of porous asphalt The test applies to laboratory compacted cylindrical specimens of porous asphalt mixtures, the upper sieve size of which does not exceed 22,4 mm It does not reflect the abrasive effect by studded tyres Normative references The following documents, in whole or in part, are normatively referenced in this document and are indispensable for its application For dated references, only the edition cited applies For undated references, the latest edition of the referenced document (including any amendments) applies EN 1097-2, Tests for mechanical and physical properties of aggregates - Part 2: Methods for the determination of resistance to fragmentation EN 12697-5, Bituminous mixtures - Test methods for hot mix asphalt - Part 5: Determination of the maximum density EN 12697-6, Bituminous mixtures - Test methods for hot mix asphalt - Part 6: Determination of bulk density of bituminous specimens EN 12697-8, Bituminous mixtures - Test methods for hot mix asphalt - Part 8: Determination of void characteristics of bituminous specimens EN 12697-30, Bituminous mixtures - Test methods for hot mix asphalt - Part 30: Specimen preparation by impact compactor EN 12697-31, Bituminous mixtures - Test methods for hot mix asphalt - Part 31: Specimen preparation by gyratory compactor EN 12697-35, Bituminous mixtures - Test methods - Part 35: Laboratory mixing Apparatus 3.1 3.2 Los-Angeles-machine, as specified in EN 1097-2 Thermometer, capable of covering the test temperature range with an accuracy of ± 0,5 °C 3.3 Chamber, room or enclosure, large enough for the Los-Angeles-machine During the test, the air temperature in the chamber shall remain constant to the test temperature ± °C The air temperature shall be measured near the Los-Angeles-machine 3.4 Oven, equipped with a closed ventilation system or a chamber fitted with a thermostatic control to maintain the test temperature constant in the vicinity of the samples, stored prior to the test, to ± °C 3.5 Balances, of suitable capacity for the mass to be weighed with an accuracy of ± 0,1 % and a resolution of 0,1 g BS EN 12697-17:2017 EN 12697-17:2017 (E) Preparation of test specimens 4.1 At least five specimens shall be prepared for each sample tested 4.2 The cylindrical specimens shall have a mass of (1,0 ± 0,2) kg The asphalt shall be mixed in accordance with EN 12697–35 and specimens compacted as specified in EN 12697–30, compacted by × 50 blows, or EN 12697–31, compacted by 40 gyrations NOTE The compaction method has an influence on the result NOTE For mixtures with a bulk density of approximately 2,0 Mg/m3, specimens with a diameter of (100 ± 3) mm and a height of (63,5 ± 2,5) mm should comply 4.3 When using asphalt with an aggregate size greater than 16 mm, larger samples shall be manufactured and cored to achieve the correct size 4.4 After the specimens have been compacted and removed from the mould, their bulk density and void content, shall be determined in accordance with EN 12697-6 (Procedure D: bulk density by dimensions) and EN 12697-8, respectively Maximum density is determined in accordance with EN 12697-5 NOTE The density of the specimens can affect the result because the mass of a specimen will influence the impact force imparted on contact during the test, particularly when asphalt with aggregates of high or low density is tested 4.5 Prior to the start of testing, the specimens shall be stored on a flat surface at a temperature of not more than 25 °C for between 48 h and 42 days from the time of their manufacture NOTE The storage time influences the mechanical properties of the specimen For test purposes other than for Type testing, different storage times may be applied Procedure 5.1 The test temperature shall be defined and maintained in the chamber during the test with an uncertainty of ± °C Before testing, specimens shall be kept at the test temperature for at least h NOTE Test temperature has a very large influence on the test result Temperatures between 15 °C and 25 °C are usually used for design purposes For porous asphalt in cold climate zones, temperatures representing the low temperature local conditions can also be used The test is not suitable for temperatures above 35 °C 5.2 The mass of specimen shall be determined and W1 (see Clause 6) shall be recorded One specimen shall then be placed inside the Los-Angeles-machine drum and, with the metal balls removed, the drum shall be turned at 3,1 rad/s to 3,5 rad/s (30 rpm to 33 rpm) for 300 turns 5.3 When the test is completed, the specimen shall be removed from the machine, slightly cleaned by means of a cloth eliminating particles that are clearly loose, and weighed again The reading W2 (see Clause 6) shall be recorded 5.4 The test shall be repeated in the same way for each of the specimens prepared according to Clause BS EN 12697-17:2017 EN 12697-17:2017 (E) NOTE Observation as to whether the fractures occur within the stone particles, in the binder film or at the boundaries between the stone particles and the binder can indicate the type of failure which can be used to redesign the mixture in order to improve this property These observations can be included in the test report Calculation 6.1 The particle loss PL shall be calculated for each specimen test using the following formula: = PL 100 × where PL (W1 − W2 ) W1 (1) is the value of particle loss, in per cent (%); W1 is the initial specimen mass, in grams (g); W2 is the final specimen mass, in grams (g) 6.2 The result shall be given as average value of five single values The result shall be rounded to the nearest % Test report The test report shall include the following information: a) identification of samples; b) date of preparation and testing; c) test temperature; d) the average particle loss; e) bulk density and voids of samples; f) the type of failure, if required; g) name of person performing the test; h) number and date of this European Standard; i) j) age of test specimen at test and storage conditions under which it was kept; comments of any anomalies, if any, which might have affected the results BS EN 12697-17:2017 EN 12697-17:2017 (E) Precision 8.1 The following uncertainties shall apply: — For particle loss below 40 %: Uncertainties for repeatability r = % and for reproducibility R = %; — for particle loss equal to or higher than 40 %: Uncertainties for repeatability r = % and for reproducibility R = % 8.2 The study of repeatability and reproducibility was carried out by laboratories in accordance with ISO 5725 under the following conditions: — test temperature: 25 °C; — two porous asphalts for each level of particle loss; — mixture compacted according to EN 12697-30 (2 × 50 blows); — number of replicates: five 10 This page deliberately left blank NO COPYING WITHOUT BSI PERMISSION EXCEPT AS PERMITTED BY COPYRIGHT LAW British Standards Institution (BSI) BSI is the national body responsible for preparing British Standards and other standards-related 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