Determination of Microstructure and Phase Composition of Sand Lime Brick after Autoclaving Process Procedia Engineering 161 ( 2016 ) 747 – 753 Available online at www sciencedirect com 1877 7058 © 201[.]
Available online at www.sciencedirect.com ScienceDirect Procedia Engineering 161 (2016) 747 – 753 :RUOG0XOWLGLVFLSOLQDU\&LYLO(QJLQHHULQJ$UFKLWHFWXUH8UEDQ3ODQQLQJ6\PSRVLXP :0&$86 'HWHUPLQDWLRQRI0LFURVWUXFWXUHDQG3KDVH&RPSRVLWLRQRI6DQG /LPH%ULFNDIWHU$XWRFODYLQJ3URFHVV 5\V]DUG'DFKRZVNLD.DWDU]\QD.RPLVDUF]\ND a Kielce Univercity of Technology, Faculty of Civil Enginneering and Architecture, Al 1000-lecia P.P.7,25-314 Kielce, Poland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±0HUFXU\,QWUXVLRQ3RURVLPHWU\$QDGGLWLRQDOFRPSRQHQWWRWKHVWDQGDUGLQJUHGLHQWVRIWUDGLWLRQDOVDQG OLPHSURGXFWVOLWKLXPZDWHUJODVVZDVXVHG7KUHHVHULHVRIVDPSOHVLQWKHUHFWDQJXODUVKDSHZLWKGLPHQVLRQV[[>PP@ ZHUHSUHSDUHG7KHVWXG\RIVWDQGDUGVDPSOHVZLWKWKHFRQWHQWRIDQGDGGLWLYHVZDVSHUIRUPHGLQD.LHOFH8QLYHUVLW\ RI7HFKQRORJ\ODERUDWRULHV © 2016 The Authors Published by Elsevier Ltd This is an open access article under the CC BY-NC-ND license 7KH$XWKRUV3XEOLVKHGE\(OVHYLHU/WG (http://creativecommons.org/licenses/by-nc-nd/4.0/) 3HHUUHYLHZXQGHUUHVSRQVLELOLW\RIWKHRUJDQL]LQJFRPPLWWHHRI:0&$86 Peer-review under responsibility of the organizing committee of WMCAUS 2016 Keywords:VLOLFDWHSURGXFWVPLFURVUXFWXUHWREHUPRULWHFDOFLXPVLOLFDWHK\GUDWHV;UD\GLIIUDFWRPHWU\;5'6(0 1RPHQFODWXUH 6(0 ;5' 6FDQQLQJHOHFWURQPLFURVFRSH ;UD\GLIIUDFWRPHWU\ &RUUHVSRQGLQJDXWKRU7HO E-mail address:NDWHB#RSSO 1877-7058 © 2016 The Authors Published by Elsevier Ltd This is an open access article under the CC BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/) Peer-review under responsibility of the organizing committee of WMCAUS 2016 doi:10.1016/j.proeng.2016.08.762 748 Ryszard Dachowski and Katarzyna Komisarczyk / Procedia Engineering 161 (2016) 747 –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yszard Dachowski and Katarzyna Komisarczyk / Procedia Engineering 161 (2016) 747 –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yszard Dachowski and Katarzyna Komisarczyk / Procedia Engineering 161 (2016) 747 –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¶V DQGWKHOHQJWKRIWKH6L2FKDLQV,QRUGHUWRFRUUHFWGHWHUPLQDWLRQRIWKHSKDVHYDULHW\WKHDQDO\VLVRI&DWR6L FRQWHQW&6VKRXOGEHSHUIRUPHG>@('6VSHFWUXPFRQILUPVWKHSUHVHQFHRIWREHUPRULWHLQWKHVDPSOH)LJ Ryszard Dachowski and Katarzyna Komisarczyk / Procedia Engineering 161 (2016) 747 –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he Chemistry of CementV/RQGRQ >@.XURZVNL:The Chemistry of Buildings Materials$*+8F]HOQLDQH:\GDZQLFWZD1DXNRZR'\GDNW\F]QH.UDNyZ >@+LGH\XNL.6DWRVKL.DWDOORemoval of organic polyelectrolytes and their metal complexes by adsorption onto xonotlite,(OVHYLHU 6FLHQFHLQ3ROLVK >@(LOHUV/1HOVRQ((ULN%DWDOOHigh temperature cement compositions pectolite, scawitte, truscottite or xonotlite which you want?$PHULFDQ,QVWLWXWHRI0LQLQJ0HWDOOXUJLFDODQG3HWUROHXP(QJLQHHUV'DOODV >@:ROINH6Technology of sand-lime products$UDG\:DUV]DZDLQ3ROLVK >@'DFKRZVNL56WĊSLHĔ$The impact of various additives on the microstructure of silicate products,QWHUQDWLRQDO&RQIHUHQFHRQ*UHHQ %XLOGLQJVDQG6XVWDLQDEOH&LWLHV3URFHGLD(QJLQHHULQJ9ROS >@'DFKRZVNL5-DVLĔVND,Effect of glass foam on porosity of silicates$UFKLYHVRIWKH,QVWLWXWHRI&LYLO(QJLQHHULQJ ... >@:ROINH6Technology of sand- lime products$UDG\:DUV]DZDLQ3ROLVK >@''DFKRZVNL56WĊSLHĔ$The impact of various additives on the microstructure of silicate products,QWHUQDWLRQDO&RQIHUHQFHRQ*UHHQ... responsibility of the organizing committee of WMCAUS 2016 doi:10.1016/j.proeng.2016.08.762 748 Ryszard Dachowski and Katarzyna Komisarczyk / Procedia Engineering 161 (2016) 747 – 753 &6+ &DOFLXP6LOLFDWH+\GUDWHV... 3HHUUHYLHZXQGHUUHVSRQVLELOLW\RIWKHRUJDQL]LQJFRPPLWWHHRI:0&$86 Peer-review under responsibility of the organizing committee of WMCAUS 2016 Keywords:VLOLFDWHSURGXFWVPLFURVUXFWXUHWREHUPRULWHFDOFLXPVLOLFDWHK\GUDWHV;UD\GLIIUDFWRPHWU\;5''6(0