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1
INTRODUCTION TO
BREWING AT
FULLERS
2
CONTENTS
BREWHOUSE 5
• Brewing Liquor 6
• Raw Materials 7
• Milling 8
• Mashing 9
• Extract 12
• Starch Degradation 13
• Wort separation 15
•Hops 16
• Wort Boiling 18
• Wort Clarification
& Cooling 19
• Wort Analysis
Examples 20
FERMENTATION 21
• Carbohydrate
Metabolism 23
• Nitrogen
Metabolism 24
• Fermentation
Profiles 25
• END PROCESSING 27
• Beer Conditioning 28
• Cask Beer 30
• Conditioning / Racking
• Tank 32
• Filtration Aids 33
•Filtration 34
• Bright Beer Tank 36
• Small Pack Quality
Control 39
• Bottling 40
• Canning 42
• Pasteurisation 44
• Kegging 47
• End Processing Food
Safety 48
C. I .P 49
RECOMMENDED
READING 51
3
MALT
SILO
FLASH PASTEURISER
BOTTLES / CANS
OR
KEGS
FERMENTATION
THE BREWING PROCESS
BREWING
LIQUOR
MASH TUN
COPPER
/ WHIRL
POOL
MILL
SWEET WORT
CONDITIONING
TANKS
MATURATION
TANKS
CASKS
RACKING
TANKS
PARAFLOW
BRIGHT BEER
TANKS
4
The Brewing Process
• MILLING - malted barley is crushed to form a coarse
flour called grist
• MASHING - grist is added to liquor to form a porridge-like
mash. This activates the enzymes, thus enabling them to
solubilise the protein and starch fractions of the
endosperm
• WORT SEPARATION-the aqueous extract, called wort,
is separated from the spent solids using a mash tun
• WORT BOILING - the wort is boiled in the presence of
hops which impart bitterness and aroma. Boiling sterilises
the wort, coagulates some proteins and causes formation
of colour compounds. The spent hop material along with
some protein, known as trub, is removed by whirlpool
action.
• FERMENTATION - the wort is then cooled to 17°C and
transported to the fermentation vessel. The wort is
aerated & pitched with yeast. Fermentation proceeds
until much of the carbohydrate is converted to alcohol
and carbon dioxide. Higher alcohols and other yeast
metabolites (for example esters) contribute to beer
flavour and aroma.
• END PROCESSING - beer is then conditioned to modify
the flavour and aroma before clarifying. All beer
characteristics are checked and adjusted to within
specification. The beer is packaged into cask or filtered
and pasteurising before being packaged into keg, bottle
or can.
5
BREWHOUSE
6
Brewing Liquor
• Water Treatment - removal of hardness by heating & acid
addition
• Direct Flavour Effects - Na
+
sweet (salty in excess) / Mg
2+
bitter, sour / Fe
3+
metallic / Cl
-
fullness / S0
4
2-
astringency /
K+ salty
• Indirect flavour effects - yeast requirements / pH / enzymes
during mashing Keep calcium >150ppm. Four times more
calcium than malt oxalate required
pH CONTROL
• Bicarbonate more influential at raising pH than calcium at
lowering
• Carbonate : bicarbonate buffer system
Ca
2+
H
2
0 + CO
2
HCO3- CO
3
2-
CaCO
3
• Calcium : malt buffering system
3 Ca
2+
+ 2 HPO
4
2-
2H
+
+ Ca
3
(PO
4
)2
Polypeptide H + Ca
2+
Polypeptide Ca + 2 H+
• High bicarbonate high wort pH due to removal of H+
• Calcium reacts with malt protein to reduce wort pH /
increased run-off rate / increased extract recovery / increased
TSN & FAN / precipitation of oxalate
7
Raw Materials
Pale Ale Malt
• Malted barley
• Concentrated source of starch
• Starch consists of unbranched helical amylose [200-
400 D-glucose units linked via α−1,4-positions] AND
branched amylopectin [D-glucose units linked via α-
1,6 and α -1,4 links. Up to 6000 glucose units]
molecules.
• Barley starch granules : large granules supply most of
the brewers extract (20 - 25µ) and small starch
granules (1 - 5µ)
• Barley protein : 30% glutelin (dissolves in weak
alkali)+ 37% hordein (dissolves in 80% alcohol)+ 11%
albumin (dissolves in water)
• High molecular weight proteins : improve head
retention
• Low molecular weight proteins : amino acids and small
peptones for fermentation are haze precursors
• Fats : husk and aleurone layer e.g. stearic acid, oleic
acid, linoleic acids = long chain fatty acids. Detrimental
to beer foam, but required for membrane synthesis.
8
Raw Materials
Coloured Malts & Adjuncts
• Crystal Malt - contributes colour (150° EBC colour
units)and malty / nutty / toffee / fruity notes to
London Pride, Chiswick Bitter & ESB
• Chocolate Malt - contributes colour & flavour to
London Porter
• Amber Malt - contirbutes colour (45°EBC colour
units) and sweetness and dryness to 1845
• Malted Wheat - contributes fullness and fruity notes
to Summer Ale along with more protein for head
formation
9
Milling
Mechanical breakdown of dry goods to produce grist.
Preparation of grist for the mash tun
Keep husk material in-tact to act as filter bed during
wort recovery
• Endosperm material into small particles, grits,
which readily hydrate during mashing to reactivate
the malt enzymes giving us maximum extract.
• Dry milling - 4 roller mills with 2 pairs of contra-
rotating rollers.
• Proportions of coarse grits (0.3mm-0.6mm
diameter):fine grits (0.15mm - 0.3mm): flour
(<0.15mm) ratios vary from 27:35:38 to 24:35:41
• Gypsum (calcium sulphate) is added to the grist as
it is produced (see liquor treatment page)
• Grist transferred via conveyor to grist hoppers
above mash tuns
10
Mashing
Hydrate grist and activate enzymes to form
soluble substances for fermentation
• Hot liquor (69°-71°C) comes into contact with
the grist in the ‘Steels Masher’ to achieve a
mash temperature of 65°C in the mash tun
• A porridge-like mash is formed with a bed
depth of 1.5-2.0m in the mash tun
• The mash tun has a false / slotted floor 5mm
from the base of the vessel and the mash sits
on this for 55mins. The false floor is flooded
with hot liquor before mashing starts to
remove the air
• During this period starch is degraded by
amyloytic enzymes forming sugars (primarily
maltose) and protein is further degraded by
proteases. The cell wall material is also further
degraded by glucanases
• Important flavour developments occur during
mashing as a result of the starch degradation
[...]... ALCOHOLS FATTY ACIDS ESTERS LIPIDS MALTOSE GLUCOSE SUCROSE invertase invertase MALTOTRIOSE maltase hexokinase, glucokinase GLUCOSE-6PHOSPHATE glucose-phosphate isomerase FRUCTOSE FRUCTOSE-6PHOSPHATE phospho fructokinase FRUCTOSE-1,6DIPHOSPHATE PHOSPHOENOL PYRUVATE pyruvate kinase Anaerobic Metabolism PYRUVATE pyruvate decarboxylase ACETALDEHYDE alcohol dehydrogenase ETHANOL 26 Beer Maturation / Conditioning... vessel to an external calandria (called the EWB=external wort boiler) for heating & returned to the vessel tangenitially (at 90°) Chemisty • Formation of bitter compounds • Wort sterilisation • Precipitation of calcium phosphate & proteins causing the pH to drop from 5.4 to pH 5.2 • Evaporation and hence concentrate the wort • Inactivation of enzymes • Formation of flavour active compounds • Formation... is a heat exchanger made up of 100 plates with chilled liquor ( . 1
INTRODUCTION TO
BREWING AT
FULLERS
2
CONTENTS
BREWHOUSE 5
• Brewing Liquor 6
• Raw Materials 7
• Milling 8
• Mashing 9
• Extract 12
• Starch Degradation. Wort sterilisation
• Precipitation of calcium phosphate & proteins
causing the pH to drop from 5.4 to pH 5.2
• Evaporation and hence concentrate the wort
•