Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 40) pdf
Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 40) pdf
... blocks. Anesth Analg 55:763–768
27) Hollmen H, Korhonen M, Ojala A (1969) Bupivacaine in paracervical block-plasma levels and changes in mater-
nal and foetal acid-base balance. Br J Anaesth 41:603–608
... chromatography in two fatal cases of intoxication due to
lidocaine and mepivacaine. N Engl J Med 271:487–490
23) Watanabe T, Namera A, Yashiki M et al. (1998) Simple...
Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 36) pdf
... HPLC analysis of ASA and its metabolites in plasma,
tissues and urine [9]
Reagents and its preparation
ASA (Sigma) is dissolved in methanol; for calibration curves, solutions of ASA and its metabo-
lites ... presented.
Structure of acetylsalicylic acid (ASA).
⊡ Figure 4.1
HPLC analysis of ASA and its metabolites in plasma [16]
Reagents and their preparation
• A...
Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 45) pdf
... N-phe-
nyl-p-phenylenediamine, o-aminophenol, m-aminophenol, toluene-3,4-diamine (3,4-di-
aminotoluene) and toluene-2,4-diamine (2,4-diaminotoluene), from Aldrich (Milwaukee,
WI, USA). A 10-mg aliquot each of the above ... a 60-year-old male attempted suicide by ingesting p-phenylen-
ediamine, provoked severe edema of the pharynx and rhabdomyolysis and died of cardiac
attac...
Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 8) pdf
... accuracy. In the Japan-shaking poisoning incidents taking
place in 1998, such as curry (arsenous acid) poisoning in Wakayama, sodium azide poisoning
in Niigata and cyanide poisoning in Nagano, ... Department of Legal Medicine and the Advanced Critical
Care Medical Center have been cooperating for practical analysis and studies on new analytical
methodologies of dru...
Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 10) pdf
... mixture
and mixed well.
v. A er standing for 5 min, the absorbances at 532 and 558 nm (A
532
and A
558
) are read against
distilled water in another cuvette as a blank.
vi. e percentage of HbCO ... production of Met-Hb and no chang-
es in COHb and total Hb can be achieved; the storage with shading at –80 is most desirable.
GC analysis
See [4].
Reagents and the...
Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 13) pdf
... poisoning from con-
traband vodka. Forensic Sci 6:1–3
13) Fraser AD, MacNeil W (1989) Gas chromatographic analysis of methyl formate and application in methanol
poisoning cases. J Anal Toxicol ... stirring with a small Te on-
coated magnetic bar
b
. A er 15 min of heating, about 0.6 mL volume of the headspace va-
por is drawn into a gas-tight syringe
c
. Just a er the v...
Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 14) pdf
... an ultra-sensi-
tive analysis of breath ethanol is also given.
Determination of ethanol in blood and urine
Reagents and their preparation
• 10 µL of ethanol is dissolved in 10 mL distilled water ... edn.
Nanzando, Tokyo, pp 108–116 (in Japanese)
3) Hara K, Kageura M, Hieda Y et al. (1991) Quantitative analysis of ethanol in postmortem specimens using wide-
bore capill...
Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 58) pdf
... = (calibrator concentration) × (peak area
obtained from a specimen ÷ peak area of IS added to a specimen) × (peak area of IS added
to the calibrator solution ÷ peak area of the calibrator).
b) ... organochlorine, carbamate and triazine pesticides, and a method for simul-
taneous analysis of many pesticides by GC/MS is presented. For alkylpyridinium and amino
acid typ...
Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 63) pdf
... and fatal concentrations
584 Cresol
GC/MS analysis
Reagents and their preparation
o-, m- and p-Cresols and IS are prepared according to the section of reagents and preparation
of the HPLC analysis.
GC/MS ... HPLC and GC/MS analysis of
cresol isomers and their conjugates are presented.
HPLC analysis
Reagents and their preparation
• A 10-mg aliquot each of o...
Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 27) ppt
... MO, USA). Pure powder of perazine and clospi-
razine was donated by Mitsubishi Welpharma, Osaka, Japan; that of upentixol by Takeda
Chem. Ind. Ltd., Osaka, Japan; that of thioproperazine by ... Yoshinao Katsumata
Introduction
Phenothiazine drugs, including chlorpromazine and levomepromazine, have been being
widely used as neuroleptics ( major tranquilizers), antiparkinsonian...