Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 37) pptx

... phenytoin and carbamazepine- epoxide can be purchased from Sigma. Lamotrigine, carbamazepine-diol and 9-hydroxy- methyl-10-carbamyl acridan were reported to be obtainable from Chiba-Geigy (Basel, ... preparation • Carbamazepine, ethosuximide, phenytoin, primidone, phenobarbital, diazepam, oxaze- pam, nitrazepam and 5-( 4-methylphenyl )-5 -phenylhydantoin (internal standard, IS) can...

Ngày tải lên: 15/12/2013, 12:15

... timiperone and spiperone with relatively high molecular weights, LC/MS may be most suitable. Poisoning cases, and toxic and fatal concentrations A 2-year plus 5 month-old female and an 11-month-old male ... dyskinesia of the face, appeared.  us, diphenhydramine was injected into her intravenously; she recov- ered 4 days a er admission. For the male baby, similar treatments, suc...

Ngày tải lên: 15/12/2013, 12:15

... uoroacetic acid can be added to a mobile phase as an ion-pairing reagent for analysis of the quaternary amino muscle relaxants [6]. e) For solid-phase extraction of the drugs, weak cation-exchanger ... Dragendorff reagent; ➄ : iodoplatinate reagent TLC analysis 362 Muscle relaxants Direct inlet MS analysis [4] Reagents and their preparation • A 1-g aliquot of iodine and...

Ngày tải lên: 24/12/2013, 18:15

... for bleaching and other purposes. Sodium hypochlorite ( NaClO) aqueous solu- tion is usually used as a disinfectant, bleaching agent, fungicide and ink eraser, and is thus usually included in detergents ... solutions are analyzed by the above CE to construct a calibration curve (concentration of a hypochlorite ion in a specimen vs. peak area). A peak area obtained fro...

Ngày tải lên: 24/12/2013, 18:15

... the author et al. [1] experienced an actual case of ingestion of a large amount of permethrin-containing emulsion (Adio ® , Agros, Tokyo, Japan) and measured the concentrations of its cis and ... pretreatments and rapidness of analysis; it seems more useful than GC in clinical analysis. HPLC chromatograms for extracts of sera obtained from a permethrin-poisoned p...

Ngày tải lên: 24/12/2013, 18:15

... glands are located in the axillary, mammary, genital and perianal regions.  e glands are under the control of sympa- thetic nerves; but a majority of the glands is cholinergic and a small part ... analysis of drugs and poisons for living subjects. A blood concentration of a toxin can be an indicator for estimation of intoxication degree. Urine sometimes conta...

Ngày tải lên: 22/01/2014, 00:20

... of analysis of drugs and poisons Actual training of analysis is essential rather than collecting informations on analytical methods to make accurate identi cation and quantitation of a causative ... to a private clinical laboratory company with a charge. In Japan, many experts are available for analysis of toxic compounds; their results of analysis and...

Ngày tải lên: 22/01/2014, 00:20

... symptoms upon arrival at a hospital. His skin was immediately washed, and various treatments, such as gastrolavage, administration of activated charcoal and a purgative (magnesium citrate) and enforced ... column at 50 °C. It should be kept in mind that naphthalene is contained in gasoline, kerosene and heavy oil [1] and also in tobacco smoke [2]. 439Naphthalene Mass...

Ngày tải lên: 22/01/2014, 00:20

... in a small amount of methanol containing 0.5 % acetic acid and transferred to a small glass vial with a Te on cap, and again evaporated to dryness under reduced pressure i . viii. A 1 0- L aliquot ... victim was found dead in an automobile in a public park.  e cases Nos. 3 and 4 were treated as unnatural death. In other cases, all patients recovered a er bein...

Ngày tải lên: 22/01/2014, 00:20

... wide-bore capillary gas chromatography of organoposphate pesticides. Forensic Sci Int 41:67–72 2) Hayasaka M, Kawabata S, Haba A et al. (1994) Analysis of malathion metabolites in biological samples. ... malathion and its metabolites obtained by capillary GC/MS and packed-column GC-FPD, respectively. 1: malaoxon diacid*; 2: malaxon β-monoacid*; 3: malaoxon α-monoacid*; 4: mal...

Ngày tải lên: 26/01/2014, 18:20