handbook of stochastic analysis with applications - d kannan , v lakshmikantham

... provided by the Ehrenfest model for heat exchange, with S = { d, — d + 1, • • • , 0, 1, 2, • • • , d} , with p^ = 1 - 4jt» anc j ^ = £h» for — d < i < d, ... Technion, Haifa, Israel Bo Zhang People's University of China, Beijing, China Q. Zhang University of Georgia, Athens, Georgia xvu HANDBOOK OF...

Ngày tải lên: 08/04/2014, 12:24

Ngày tải lên: 31/03/2014, 15:23

... glass vial with a Te on-septum screw cap, which has been cooled with ice, and vortex-mixed for 5 s; a 3- L aliquot of the organic layer is injected into GC. At least 5 vials with di erent volume ... cooled with ice, capped airtightly and stored in a refrigerator. ii. A 0.4-mL volume of the blood specimen is rapidly mixed with 0.4 mL of the IS-containing pentane solutio...

Ngày tải lên: 18/10/2013, 00:15

... observed at m/z 175. n) In EI mass spectra for t-BDMS derivatives, intense peaks due to [M–57] + are usually ob- served. However, in the case of the t-BDMS derivative of EMPA, a fragment ion, having ... curve is constructed with a similar proce- dure to that described in the above commentary f . However, ions at m/z 153 and 168 for t-BDMS derivative of EMPA and diphenylmethane (IS...

Ngày tải lên: 18/10/2013, 00:15

... solution. IR, γ CHCl 3 1,7 10 cm –1 ; NMR (CDCl 3 ) δ: 1.1 0, 1.38 (s, 3H × 2, gem-CH 3 ), 1.70 (s, 3H, C 9 -CH 3 ), 3.22 (dd, 1H C 10a -H ), 5.42 (m, 1H, C 8 -H ), 6.0 7, 6.24 (s, 1H × 2, aromatic-H); ... was made ⊡ Table 2.1 Diagnostic ions in mass spectra of  9 -THC-11-ioc acid, 5α-cholestane and 5’-nor- 8 -THC-4’-ioc acid with different derivatizati...

Ngày tải lên: 24/10/2013, 19:15

... unconjugated (free) forms of morphine, codeine and 6-acetylmorphine, the extrac- tion is made as follows. A 2-mL volume of urine is diluted 2-fold with puri ed water and mixed with 0.1 mL of the ... methods, the liquid-liquid extraction and the solid-phase extraction, are avail- able; the latter gives cleaner extracts for GC and GC/MS analysis. i. Liquid-liquid extraction i. A 2...

Ngày tải lên: 24/10/2013, 19:15

... cap, followed by the addi- tion of 20 mg of anhydrous sodium carbonate and vortex-mixed for 1 min. v. A er centrifugation at 3,0 00 rpm for 2 min, 1- or 4- L of the upper layer is injected into ... 20 µL of IS solution and 0.2 mL of the saturated silver acetate solution e are added to the above solution, vortex-mixed and centrifuged at 3,0 00 rpm for 5 min. iii. A 0.2-...

Ngày tải lên: 24/10/2013, 19:15

... 26 1, 30 3, 31 6, 38 4, 53 7, 56 3, 59 3, 62 0, 650 DB-5 7 8, 17 4, 19 0, 28 3, 38 4, 45 6, 48 3, 53 7, 563 DB-17 16 0, 16 7, 22 0, 23 1, 31 6, 38 5, 48 9, 49 2, 49 4, 593 DB-210 537 DB-5MS 17 4, 50 0, 54 6, 56 3, 600 DB-624 ... Analysis 584 HP-Wax 154 HPLC 3 8, 17 4, 17 5, 17 9, 20 1,...

Ngày tải lên: 24/10/2013, 19:15

... standards [2] • Cocaine hydrochloride (Shionogi & Co ., Ltd ., Osaka, Japan; Takeda Chem. Ind. Ltd ., Osaka, Japan; or Sigma, St. Louis, MO, USA) is dissolved in 0.2 M hydrochloric acid aqueous ... TFAA with TFET can also give good results for derivatizations. f) For body  uid specimens, such as blood, urine, stomach content  uid and bile, sodium  uoride is added to each...

Ngày tải lên: 29/10/2013, 01:15

... transferred to a small glass centrifuge tube with a ground-in stopper, followed by addition of several mg of solid K 2 CO 3 and 3 mL of chloroform.  e tube is vortex-mixed well and centri- fuged at ... accelerating voltage: 1.5 kV. Procedure i. To 1-mL of whole blood or urine, containing pentazocine, are added 50 ng dextromethor- phan (IS, methanolic solution) and 6 mL distilled...

Ngày tải lên: 29/10/2013, 02:15