Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 63) pdf
Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 63) pdf
... In this chapter, procedures for HPLC and GC/MS analysis of
cresol isomers and their conjugates are presented.
HPLC analysis
Reagents and their preparation
• A 10-mg aliquot each of o-, m- and ... analysis
Reagents and their preparation
o-, m- and p-Cresols and IS are prepared according to the section of reagents and preparation
of the HPLC analysis.
GC/MS...
Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 36) pdf
... in human plasma, tissues and urine
can be analyzed. Quantitation limit of ASA and salicylic acid was about 500 ng/mL; the recov-
eries were 89–101 %.
GC analysis of ASA and its metabolite in ... HPLC analysis of ASA and its metabolites in plasma [16]
Reagents and their preparation
• ASA, salicylic acid, gentisic acid and salicyluric acid can be purchased from Sig...
Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 40) pdf
... paracervical block-plasma levels and changes in mater-
nal and foetal acid-base balance. Br J Anaesth 41:603–608
28) Matouskova A, Hanson B (1979) Continuous mini-infusion of bupivacaine into ... al. experienced, is described
as follows.
A 61-year-old female received an intra-gingival injection of Xylocaine™ solution (contain-
ing 2 % lidocaine and a small amount of epine...
Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 45) pdf
... p-aminophenol, catechol,
resorcinol and hydroquinone can be purchased from Sigma (St. Louis, MO, USA); N-phe-
nyl-p-phenylenediamine, o-aminophenol, m-aminophenol, toluene-3,4-diamine (3,4-di-
aminotoluene) ... edema of the pharynx and rhabdomyolysis and died of cardiac
attack 4 h a er admission; the concentration of p-phenylenediamine in his blood was 1.47 µg/
mL, and 6-a...
Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 8) pdf
... analysts is also important to maintain a high quality of their ana-
lytical skill; the establishment of educational institutions special to toxin analysis is awaited.
Only a er solving all of ... tests are being made at bedside, viz. inside the Ad-
vanced Critical Care Medical Center and complicated analysis for identi cation and quantita-
tion is being made at laboratories...
Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 10) pdf
... storage with shading at –80 is most desirable.
GC analysis
See [4].
Reagents and their preparation
• Solution of saponin and potassium ferricyanide: 500 mg of saponin (obtainable from many
manufacturers) ... with air.
A 20 0- L volume of each CO standard gas is drawn into a gas-tight syringe and injected
into GC to make an external calibration curve (
> Figure 1.3)....
Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 13) pdf
... poisoning from con-
traband vodka. Forensic Sci 6:1–3
13) Fraser AD, MacNeil W (1989) Gas chromatographic analysis of methyl formate and application in methanol
poisoning cases. J Anal Toxicol ... are presented.
Analysis of methanol
Reagents and their preparation (in common with both wide-bore
capillary GC and headspace SPME-GC)
• Methanol standard solution: a 0.127 mL v...
Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 14) pdf
... an ultra-sensi-
tive analysis of breath ethanol is also given.
Determination of ethanol in blood and urine
Reagents and their preparation
• 10 µL of ethanol is dissolved in 10 mL distilled water ... GC. e peak areas obtained at 4 concentrations of ethanol are
plotted against the amount of ethanol to make a calibration curve; the nal amounts of
ethanol injected ar...
Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 58) pdf
... = (calibrator concentration) × (peak area
obtained from a specimen ÷ peak area of IS added to a specimen) × (peak area of IS added
to the calibrator solution ÷ peak area of the calibrator).
b) ... Chemical Industries, Ltd., Osaka, Japan. As internal standard (IS), fenitrothion-
d
6
was obtained from (Hayashi Pure Chemical Ind., Ltd, Osaka, Japan). Other common
chemicals used we...
Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 27) ppt
... MO, USA). Pure powder of perazine and clospi-
razine was donated by Mitsubishi Welpharma, Osaka, Japan; that of upentixol by Takeda
Chem. Ind. Ltd., Osaka, Japan; that of thioproperazine by ... Springer-Verlag Berlin Heidelberg 2005
II.3.1 Phenothiazines
by Akira Ishii and Yoshinao Katsumata
Introduction
Phenothiazine drugs, including chlorpromazine and levomepromazine, have...
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