Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 59) pptx
Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 59) pptx
... wide-bore capillary gas chromatography of organoposphate pesticides. Forensic Sci Int 41:67–72 2) Hayasaka M, Kawabata S, Haba A et al. (1994) Analysis of malathion metabolites in biological samples. ... malathion and its metabolites obtained by capillary GC/MS and packed-column GC-FPD, respectively. 1: malaoxon diacid*; 2: malaxon β-monoacid*; 3: malaoxon α-monoacid*; 4: malathion diacid*; 5: malaoxon; ... Table 2.2Distribution of malathion and its metabolites in blood, bile and some organs of a human victim in fatal malathion poisoning [8]Concentration (µg/g)Sample Malathion Malaoxon Monoacid...
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Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 28) pptx
... timiperone and spiperone with relatively high molecular weights, LC/MS may be most suitable.Poisoning cases, and toxic and fatal concentrations A 2-year plus 5 month-old female and an 11-month-old male ... dyskinesia of the face, appeared. us, diphenhydramine was injected into her intravenously; she recov-ered 4 days a er admission. For the male baby, similar treatments, such as intravenous injec-tion ... bromperidol was used as IS for analysis of haloperidol and vice versa. is is because both drugs are not simultaneously administered in most cases.d) All glasswares, including glass centrifuge...
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Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 37) pptx
... phenytoin and carbamazepine-epoxide can be purchased from Sigma. Lamotrigine, carbamazepine-diol and 9-hydroxy-methyl-10-carbamyl acridan were reported to be obtainable from Chiba-Geigy (Basel, ... preparation• Carbamazepine, ethosuximide, phenytoin, primidone, phenobarbital, diazepam, oxaze-pam, nitrazepam and 5-( 4-methylphenyl )-5 -phenylhydantoin (internal standard, IS) can be all purchased from ... carbamazepine) and two carbamazepine metabolites ( carbamazepine-diol and carbamazepine- epoxide) can be detected from human plasma (> Figure 5.3). e detec-tion limits of each drug was about...
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Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 38) pptx
... uoroacetic acid can be added to a mobile phase as an ion-pairing reagent for analysis of the quaternary amino muscle relaxants [6].e) For solid-phase extraction of the drugs, weak cation-exchanger ... Dragendorff reagent; ➄: iodoplatinate reagentTLC analysis 362 Muscle relaxants Direct inlet MS analysis [4]Reagents and their preparation• A 1-g aliquot of iodine and 2 g potassium iodide are dissolved ... peripheral-acting muscle relaxants are intentional and/ or homicidal. In this chapter, therefore, analytical methods only for the peripheral-acting muscle relaxants (> Table 6.2) are dealt with....
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Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 43) pptx
... for bleaching and other purposes. Sodium hypochlorite ( NaClO) aqueous solu-tion is usually used as a disinfectant, bleaching agent, fungicide and ink eraser, and is thus usually included in detergents ... solutions are analyzed by the above CE to construct a calibration curve (concentration of a hypochlorite ion in a specimen vs. peak area). A peak area obtained from a specimen is applied to the calibration ... detergents for laundry. Calcium hypochlorite [ Ca(ClO)2, bleaching pow-der] is also used as a bleaching agent and disinfectant. e kinds of household utensils contain-ing hypochlorite are numerous;...
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Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 46) pptx
... the author et al. [1] experienced an actual case of ingestion of a large amount of permethrin-containing emulsion (Adio®, Agros, Tokyo, Japan) and measured the concentrations of its cis and ... pretreatments and rapidness of analysis; it seems more useful than GC in clinical analysis. HPLC chromatograms for extracts of sera obtained from a permethrin-poisoned patient 3 h and 3 months after ... metabolic acidosis and renal dysfunction. By treatments, such as endotra-cheal intubation, gastrolavage, administrations of activated charcoal and magnesium citrate and transfusion, his conditions...
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Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 2) pptx
... glands are located in the axillary, mammary, genital and perianal regions. e glands are under the control of sympa-thetic nerves; but a majority of the glands is cholinergic and a small part ... analysis of drugs and poisons for living subjects. A blood concentration of a toxin can be an indicator for estimation of intoxication degree. Urine sometimes contains large amounts of metabolites ... erent according to indi-viduals, types of the gland and various stresses (emotional, physical and thermal) [19]. e sweat analysis started in about 1970, and showed that various drugs can be...
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Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 7) pptx
... of analysis of drugs and poisons Actual training of analysis is essential rather than collecting informations on analytical methods to make accurate identi cation and quantitation of a causative ... to a private clinical laboratory company with a charge. In Japan, many experts are available for analysis of toxic compounds; their results of analysis and maintenance of their analytical instruments ... for analysis of a causative toxin, trials of toxin analysis and hosting a short course of training for preliminary spot tests of drugs and poisons. Poisoning mailing list (ml-poison) e ml-poison...
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Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 48) pptx
... symptoms upon arrival at a hospital. His skin was immediately washed, and various treatments, such as gastrolavage, administration of activated charcoal and a purgative (magnesium citrate) and enforced ... column at 50 °C.It should be kept in mind that naphthalene is contained in gasoline, kerosene and heavy oil [1] and also in tobacco smoke [2].439NaphthaleneMass spectra of naphthalene and naphthalene-d8 ... 6.2440 NaphthalenePoisoning case and fatal concentrations A 6-month-old male [3] opened two packages of naphthalene (commercial name: Neopas®) and seemed to ingest a part of the total amount...
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Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 53) pptx
... in a small amount of methanol containing 0.5 % acetic acid and transferred to a small glass vial with a Te on cap, and again evaporated to dryness under reduced pressurei.viii. A 1 0- L aliquot ... victim was found dead in an automobile in a public park. e cases Nos. 3 and 4 were treated as unnatural death. In other cases, all patients recovered a er being admitted in hospitals. In Cases ... niphobles in a large amount, was poisoned by eating its liver and died just a er arrival at a hospital. In Case No. 3, the victim was found dead in a ship on ocean navigation. In Case No. 4,...
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