Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 8) pdf
Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 8) pdf
... analysts is also important to maintain a high quality of their ana-lytical skill; the establishment of educational institutions special to toxin analysis is awaited.Only a er solving all of ... tests are being made at bedside, viz. inside the Ad-vanced Critical Care Medical Center and complicated analysis for identi cation and quantita-tion is being made at laboratories of the Department ... in emergency medi-cine; it requires both rapidness and accuracy. In the Japan-shaking poisoning incidents taking place in 1998, such as curry (arsenous acid) poisoning in Wakayama, sodium azide...
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Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 36) pdf
... in human plasma, tissues and urine can be analyzed. Quantitation limit of ASA and salicylic acid was about 500 ng/mL; the recov-eries were 89–101 %. GC analysis of ASA and its metabolite in ... HPLC analysis of ASA and its metabolites in plasma [16]Reagents and their preparation• ASA, salicylic acid, gentisic acid and salicyluric acid can be purchased from Sigma (St. Louis, MO, USA).• ... administered intravenously 15 min before sampling HPLC analysis of ASA and its metabolites in plasma, tissues and urine346 Acetylsalicylic acid of its blood. By this method, ASA and its two metabolites...
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Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 40) pdf
... paracervical block-plasma levels and changes in mater-nal and foetal acid-base balance. Br J Anaesth 41:603–608 28) Matouskova A, Hanson B (1979) Continuous mini-infusion of bupivacaine into ... al. experienced, is described as follows. A 61-year-old female received an intra-gingival injection of Xylocaine™ solution (contain-ing 2 % lidocaine and a small amount of epinephrine) at a ... C.Epidural, conduction, infiltration, topical and spinal anaesthesias, ventricular arrhythmia378379Local anaestheticsReagents and their preparation• Cacaine hydrochloride and other local anaesthetics...
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Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 45) pdf
... p-aminophenol, catechol, resorcinol and hydroquinone can be purchased from Sigma (St. Louis, MO, USA); N-phe-nyl-p-phenylenediamine, o-aminophenol, m-aminophenol, toluene-3,4-diamine (3,4-di-aminotoluene) ... edema of the pharynx and rhabdomyolysis and died of cardiac attack 4 h a er admission; the concentration of p-phenylenediamine in his blood was 1.47 µg/mL, and 6-aminobenzothiazole, the metabolic ... concentrationsChugh et al. [6] reported a case of a 20-year-old female, who had ingested 40 mL of 4 % p-phe-nylenediamine (1.6 g), had provoked the swelling of the face and neck, upper-abdominal pain,...
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Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 10) pdf
... storage with shading at –80 is most desirable. GC analysis See [4].Reagents and their preparation• Solution of saponin and potassium ferricyanide: 500 mg of saponin (obtainable from many manufacturers) ... with air. A 20 0- L volume of each CO standard gas is drawn into a gas-tight syringe and injected into GC to make an external calibration curve ( > Figure 1.3).ix. Measurement of a total ... is shaken well and le at room tem-perature for 30 min.vi. A needle of a gas-tight syringe is inserted into the disposable syringe, and 200 µL of the headspace gas is drawn into the gas-tight...
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Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 13) pdf
... poisoning from con-traband vodka. Forensic Sci 6:1–3 13) Fraser AD, MacNeil W (1989) Gas chromatographic analysis of methyl formate and application in methanol poisoning cases. J Anal Toxicol ... are presented. Analysis of methanolReagents and their preparation (in common with both wide-bore capillary GC and headspace SPME-GC)• Methanol standard solution: a 0.127 mL volume of methanol ... stirring with a small Te on-coated magnetic bar b. A er 15 min of heating, about 0.6 mL volume of the headspace va-por is drawn into a gas-tight syringe c. Just a er the vapor volume in...
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Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 14) pdf
... an ultra-sensi-tive analysis of breath ethanol is also given.Determination of ethanol in blood and urineReagents and their preparation• 10 µL of ethanol is dissolved in 10 mL distilled water ... GC. e peak areas obtained at 4 concentrations of ethanol are plotted against the amount of ethanol to make a calibration curve; the nal amounts of ethanol injected are 25, 50, 75 and 100 ... 239–260 (in Japanese) 2) Phemacentical Society of Japan (ed) (1992) Standard Methods of Chemical Analysis in Poisoning, 4th edn. Nanzando, Tokyo, pp 108–116 (in Japanese) 3) Hara K, Kageura M,...
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Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 58) pdf
... = (calibrator concentration) × (peak area obtained from a specimen ÷ peak area of IS added to a specimen) × (peak area of IS added to the calibrator solution ÷ peak area of the calibrator).b) ... Chemical Industries, Ltd., Osaka, Japan. As internal standard (IS), fenitrothion-d6 was obtained from (Hayashi Pure Chemical Ind., Ltd, Osaka, Japan). Other common chemicals used were of the ... impurities of urine. e simultaneous analysis is aimed at screening of compounds in a wide range; the condi-tions should be set according to an average property of many analytes. erefore, satisfactory...
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Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 63) pdf
... In this chapter, procedures for HPLC and GC/MS analysis of cresol isomers and their conjugates are presented. HPLC analysis Reagents and their preparation• A 10-mg aliquot each of o-, m- and ... biological fluids of a non-fatal case of cresol intoxication. Forensic Sci Int 47:21–29 5) Fuke C, Sakai Y, Yagita K et al. (19 98) The quantitative analysis of cresols in a case of cresol poisoning ... percutaneous absorption: a male child was playing on a slide in a park, and slid into a puddle with his buttocks getting wet with water probably containing a large amount of cresol. A er 30 min,...
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Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 27) ppt
... MO, USA). Pure powder of perazine and clospi-razine was donated by Mitsubishi Welpharma, Osaka, Japan; that of upentixol by Takeda Chem. Ind. Ltd., Osaka, Japan; that of thioproperazine by ... Springer-Verlag Berlin Heidelberg 2005II.3.1 Phenothiazines by Akira Ishii and Yoshinao KatsumataIntroductionPhenothiazine drugs, including chlorpromazine and levomepromazine, have been being ... available. In this chapter, the methods of qualitative and quantitative analysis of phenothiazines in human body uids using useful GC/MS and LC/MS are presented.GC/MS analysis Reagents and...
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