n. 1-2 Phàn thuc nghiêm.
FHA: T.TlCH(m3)
T.TlCH(m3) î . THONG (K^^/m i'D C'H-CO 11.50 Z ( M / m 3 . VZ(M/Pa) HE SO F C P a ) N.D0(M/m3) N.D0(g/Di3) N . D 0 ( u g / g ) S.L Mol S.L Z K.KHl 6E+09 3)1. 1.8541325 0 ra)4.03417902E .2420507.41 2.4B0i8794E- 1.00055221E- 2.63345343E- 2.22i548a4E- 60.0331328 BO.0331328 NUOC 7000000 1000 0 -04.176305898 1234141.28 05 2.48018794E-05 08 4.37271761E-06 06 1.15089928E-03 03 1.15089928E-03 30.6090233 30.6090233 DAT 45000 1500 .02 4.33682555 195157.15 2.48018794E-05 1.07561424E-04 .0283101669 .018873444^ 4.84026409 ' 4.84026409 T.TICH 21000 1500 .04 8.6736511 182146.673 2.48018794E 2.15122848K .0566203337 .0377468891 4 . 5 1 7 5 7 9 8 2 4 . 5 1 7 5 7 9 8 2
TÀI LIEU THAM KHÀO
1. Nguyên Trpng Bièu, Tû Vàn Mac, Thuôc Ûiû hûu ca, Nxb. KHKT, Hà npi, 1978.
2. Cor sô b^ thuyét sàc ki khi, chuong uînh hpp tâc khoa hpc kî thuât
Viêt nam-Hà lan, Hà npi, 1988.
3. Danh mue thuôc BVTV dupx: phép su dung, han ché su dung, câm su dung Uong nông nghiêp ô Viêt nam, QD sô 476 NN-BVTV/QD cùa Bô Nông nghiêp va công nghiêp thuc phàm, ngày 11/5/1994. 4. Danh mue thuôc BVTV câm va han ché su dung do UNEP de xuât,
Tap chi bào vê thuc vât, SÔ 6, U.26, 1991.
5. Nguyên Vàn Dat, Nguyên Quôc Tuàn, ..., Dé tài 66A-01-01, 1990. 6. Dé tài SKV 01-914-02-87, Chûng nhân thiét bi phông kièm nghiêm. 7. Tràn Quang Hùng, Thuéc bào ve thuc vât, nxb. Nông nghiêp, 1992. 8. Tràn Vân Nhàn, Nguyên Thac Sun, Giâo uînh Hda d, nxb. DH &
THCN, Hà npi, 1986.
9. Pham Thi Phong, Nghién cûu su ton luu va khà nâng on quang cho Fenvalerate, Luan an phd tien sî, Hà npi, 1993.
10. Tài Lieu huc^g dln phân uch thô nhuOng nông hda, Viên nông hda thô nhuông, Hà npi, 1976.
11. Nguyên Quoc Tuàn, Bùi Sî Doanh, Tràn Quang Hùng, Phân Uch du
lupng Metyl Parathion Uong dât, nuôc bàng sàc \î long cao âp, Thông
bâo khoa hpc cùa câc truông Dai hpc, chuyên dé tài nguyên va moi truông, Hà npi, 1988.
12. Nguyên Quoc Tuân, Tràn Quang Hùng, Nguyên Xuân DQng, Xâc dinh Rotenon chiét tû rê cây Derris ô câc dia phuong khâc nhau cùa Viêt
13. Nguyên Quoc Tuân, Pham BÎnh Quyèn, Ành huông cùa vi sinh vât dât dén su phân hùy 2,4-D Uong dât, Thông bâo khoa hpc cùa câc truông Dai hpc , chuyén dé khoa hpc moi truông, Hà nôi, 1993. 14. Xâc dinh du lupng BHC Uong gao va dau tuong, TCVN 4718-89. 15. Xâc dinh du lupng Metyl Parathion Uong didc va dau tuong, TCVN
4719-89.
16. Xâc dinh du lupng Dimethoat Uong chè, TCVN 5161-90.
17. Xâc dinh du lupng Metyl Paradiion Uong chè, TCVN 1591-90. 18. Xâc dinh du lupng Lindan Uong chè, TCVN 5160-90.
19. AgnihoUi N.P., The dégradation of Pesticides in soil (see: Pesticide Residues in the Environment in India, Bangalor, 343-353, 1978).
20. Ahronson N., Pure Applied ChemisUy, 59, 1419-1430, 1987.
21. AJlebone J.E., Haminton R.J., Détermination of 2,4-D in Plant Tissue, J. Chromatogr., 108, 188-193, 1975.
22. AOAC Officiai Methods of Analysis, 99-100, Arlington, Virginia, 1984.
23. Argauer R.J., Fluoresence and UV Absorbance of Pesticides and Naturally Occuring Chemicals in Agricultural Products after HPLC Séparation on a bonded-CN polar base, ACS Symp. Serv., 136, 103- 126, 1980.
24. Asharf S., Bartle K.D., CLifford N., Organophosphorous Pesticides in River and Drinking Water, Tentative Methods, HM Stationary Office, London, 1983.
25. Baker P.G., Bottomley P., Détermination of Residues of Synthetic Pyrethoids in Fruis Vegetables by Gas-Liquid and High-Performance Liquid Chromatography, The Analysis, 107(2), 206-212, 1982.
26. Bcelo D., Occurence, Handling and Chromatographic Détermination of Pesticides in the Aquatic Environment, The Analysis, 116(7), 684- 689, 1991.
27. Bergtedt L., Widmark G., Répétitive Scaning in Gas Chromatography- Mass Specuometry, Chromatographia, 3, 59-63, 1970.
28. Bollag J.M., Brigs G.G., Dawson J.E., Alexander M., Hydroxyladon of Chlorinatd Phénols, J. Agr. Food Chem., 16(5), 826-828, 1968. 29. Bollag J.M., Brigs G.G., Dawson J.E., Alexander M., 2.4-D
MettaboLism. Enzymatic Dégradation of Chlorocatechol, J. Agr. Food Chem., 16(5), 829-835, 1968.
30. Bowman M.C., Beroza M., J. Ass. Offi. Agr. Chem., 48, 943-948, 1965.
31. Bozyk R., Qualitate KonUolle von Labormittaln Mach Mathematizohen Statistichen Methodan, Wasava, 1980.
32. Cat-up Opération on Old Pesticides: an Intégration Reports N® 678801(X)2, National InsUtute of Public Health and Enviromental Protection, 1991.
33. Changes in Methods: J. Ass. Off. Anal. Chem., 69(2), 253-254, 1986. 34. Chau Alfred S.Y., Thomson K., Investigation of the Intergrity of
Seven Herbicidal Acidin Water Sampels, J. Assoc. Off. Anal. Chem., 61(6), 1481-1484, 1978.
35. Clau A.S.Y., Afghan B.K., Analysis of Pesticides in Water, CRC Press, 1982.
36. Daceghton C.G., Hsieh D.P.H., Parathion Utilization by Bacterial Symbionts in a Chemostate, Appl. Environ. Microbiol. 34, 175-184, 1977.
37. Denis W.H., Chemical Dégradation of Pesticides, CIPAC Procceding, 1979.
38. Devine J.M., Zweig G., J. Ass. Off. Anal. ChemisUy, 52, 187-192, 1969.
39. Eichelberger J.W., Lichtenberg J.J., Persistence of Pesticides in River Water, Envir. Sci. and Technol., 5(6), 541-544, 1971.
40. Eme K., Acta Chem. Scand., 7, 1663-1666, 1963.
41. Evans W.C., Smith B.S.W., Frenley H.N., Dvies J.I., Bacterial Metabolism of 2.4-Dichlorophenoxyacetate, Biochem. J.,122, 543-551,
1971.
42. Farm Chemicals Handbook, Académie Press, p. El, 1992. 43. Farm Chemicals Handbook, Académie Press, p.E8, 1990.
44. Frei R.W., long G.J., Brinkman U.A.Th., The hunt for Traces by Liquid Chromatography, Analusis, 15(2), 59-68, 1987.
45. Goelitz D.F., Larma W.L., US Geological Survey, Water Supply Paper, 1817-C, 1967.
46. Goewie C E . , Pwakman P.K., Frei R.W., Brinkman U.A.Th., Pre- column Technology in High-Performance Liquid Chromatography for the Determinationof Phenylurea Herbicides in Water in the Preesenf of their Anilines, J. Chromatogr., 284, 73-86, 1984.
47. Guan H. Tan, Comparision of Solvent ExUaction and Solid Phase ExUaction for Deteminadon of Organochlorine Psticide Residues in Water, The Analysis, 117(6), 1129-1132, 1992.
48. Guidelines on Producing Pesticide Residues Data from Supervised Trials, PAO, Rome, 1990.
49. Gunther F.A., Residue Reviews, 60, Spriger-Verlag, New York, Heidelberg, Berlin, 1976.
50. Herman D., Kaushik N.K., Solomon K.R., Impact of AlUazin on Perifîtor in Freshwater Enclousers and some Ecological Consquences, Can. J. Aquat. Sci., 93, 1917-1925, 1986.
51. Hoogendom E.A., Suategies in Method Development for the Détermination of Polar Pesticides with Coupled-Column Liquid Chromatography, Drukkerij EUnkwijk BV, UUecht, 1993.
52. Imanaka M., Hino S., Matsunaga K., Ishida T., Oxadiazon Residues in Surface Water and Curian Carps (Carassius Cuvieri) of Lake Kojima, J. Pesticide Science, 10(1), 125-134, 1985.
53. lUPAC Reports on Pesticides: Potential Contaminaion of Ground Water by Pesticides, lUPAC, 1987(see: Pure and Appl., 10, 1419-
1446, 1987.
54. Janda V., Steebeke K.D., Sandra P., Predicdon on the Condition for Fluid ExUaction of AUazin in Soil, The Analysis, 117(9), 1697-1700, 1992.
55. Jonhson J.A., Farmer W.J., Bath Versus Column Method for Determining DisUibudon of Organic betwen Soil and Water Phase, Soil Sci., 155(2), 92-99, 1993.
56. Junk G.A., Richard J.J., SoUd Phase ExUacion, GC Seperation and EC Deetecdon of Tributyltin Chloride, Chemosphere, 16(1), 61-68, 1987.
57. Junk G.A., Richard J.J., Organic in Water: Solid Phase Extraction on a smal Scale, Anal. Chem., 60(5), 451-454, 1988.
58. Junk G.A., Avery M.J., Richard J.J., Interférences in Solid Phase ExUacdon using C-18 Bond Porous Silica Caridges, Anal. Chem., 60(13), 1347-1350, 1988.
59. Kajkkannu K., Ramula U.S.S., Degredation and Persistence of Carbofuran in Soil, (see: Pesdeide Residues in Ûie Environment in India, Procceding of a Symposium held in November, Bangalor,
1978.
60. Kaufman D.D. et al., Movement of Cypermethrin, Permethrin, Decamethrin and thei dégradation products in soil, J. Agr. Food Chem., 29(2), 239-295, 1981.
61. Kautner T.R., Mumma R.O., Application of Mass SpecUoscopy to Pesticide Residue Analysis, Residue Analysis, Residue Review, 16,
138-151, 1966.
62. Lagana A., Mario A., Fago G., Martinez B.P., Multiresidue Analysis of Phenylurea Herbicides in Crops by HPLC with Diod Array Detector, Analusis, 22(3), 63-69, 1994.
63. Laveglia J., Dahm P.A., Dégradation of Organophosphorous and Carbamat Insecticides in the Soil and by Soil Microorganisms, Annu. Rev. Entomol., 22, 483-511, 1977.
64. Lawrence J.F., Fluometric Derivatizationin High-Performance Liquid Chromatography, J. Chromatogr. Sci., 17, 147-150, 1979.
65. Leichtenstein E. P., Schulz K.R., The Effects of Moisture and Microorganisms on the Persistence Insecticides in Soil with Spécial Emphasis on Parathion, J. Envir. Enomology, 57, 618-627, 1964.
66. Li-Tse Ou, Shamrma A., Dégradation of Metyl Parathion by a mixed Bacterial Culture and a Bacillus sp. isoluted from Différent Soils, J. Agric. Food Chem. 37(6), 1514-1518, 1989.
67. Li-Tse Ou, Metyl Parathion Dégradation and MetaboUsm in Soil: Influence of High Soil-Water Contents, Soil Boil. Biochem., 17 (2), 241-243, 1985.
68. Li-Tse Ou, Rao P.S.C., Davison J.M., Metyl Parathion Dégradation in Soil : Influence of Soil-Water Tension, Soil Biol. Biochem., 15(2), 211-215, 1983.
69. Louise M. N., Biological-included Hydrolysis of Paratthion in soil: Isolation of Hydrolyzing Bacteria, Soil Bio. Biochem. 14, 219-222,
1982.
70. Mackay D., Paerson S., Canculating Fugacity, Environ. Sci. Technol., 15(9), 1006-1014, 1981.
71. Mackay D., Paterson S., Application of Fugacity Model to the Estimate of Chemical DisUibution and Persistence in the Environment (see: Fate of Chemicals in the Environment), ACS Symposium Séries, 225, 175-196, 1983b.
72. Maybury N., Laboratory Manual of Pesticide Residue Analysis in Agricultural Products, Agr. Canada, 1985.
73. Mierzma S., Witek S., Gas- Liquid Chromatographic Method with EleUodetection for the Détermination of Residues of Some Phenoxyacetic acid Herbicides in Water as their 2,2,2- uichloroethyl esters, J. Chromatogr., 136, 105-111, 1977.
74. Mikami N., Photodegradattion of Feniuothion in Water and Soil Surface and its Hidrolysis in Water, J. of Pesticide Science, 10(2), 273-270, 1985.
75. Mikami N., Dégradation of Pyrethoids Insection in the Environment, J. of Pesticide Science, 12, 539-548, 1987.
76. Mikami N.,Takahashi N., Hayashi K., Miyamoto J., Photodegradation of Fenvalerate (Sumicidin) in Water and Soil Surface, J. Pesticide Science, 5, 225-230, 1980.
77. Miyamoto J., Saferty Assessment of Fenvalerate, Esfenvalerat and Fenpropathrin in their use of Agriculture, Sumitomo Chemical Co. Ltd., Japan, 1988.
78. Miyamoto L, Environmental Fate and Effect of Fenvalerate, Esfenvalerate and Fenpropathrin. Saferty Assessment in their use for Agriculture.( See: Heath Aspects of Pesticide use, IPCS, Moscow, 166-192, 1991.)
79. Modeste F., Caude M., Couplage en Ligne de la Chromatographic en Phase Liquide avec la Chromatographic en Phase Gazense. Principes, Delopments et Applications, Analusis, 22(3), 89-107, 1994.
80. Moreale A., Van Bladel R., Behavior of 2.4-D in Belgian Soil, J. Envir. Quai., 9(4), 627-633, 1980.
81. Neilen M.W.F., Koomen G., Freei R.W., Brinkman U.A.Th., Electrochmical Détection of Phenylurea Herbicides in Liquid Chromatography, J. of Liquid Chromatogr., 8, 315-332, 1985.
82. Nelson L.M., Biological Included Hydrolysis of Parathion in Soil: Isolation of Hydrolysing Bacteria, Soil Biol. Biochem. 14, 219-222, 1982.
83. Nesbit H. J., Watson J. R., Dégradation of the Herbicide 2.4-D in River Water, I. Discrition of Study Area and Survey of Rate Determining Factor, Water Research, 14, 1683-1688, 1980.
84. Nesbit H.J., Watson J.R., Dégradation of 2,4-D in the Water, IL The Rôle of Suspended Sedimeent Nuuients and Water Température, Water Research, 14, 1689-1694, 1980.
85. Neey W.B., Blaud G.E., Environmental Exposure from Chemicals, CRC Press, Boca Raton, Florida, 1985.
86. Nose K., A multi-site Decay Model of Pesticides in soil, J. of Pesticide Science, 12(3), 505-508, 1987.
87. Noy Th., Weiss E., Herps T., Van Cruchen H., Rijks L, One-Line Combination of Liquid Chromatography and Capillary Gas Chromaography. PreconcenUation and Analysis of Organic Compounds in Aqueous Samples, J. of High Res. Chromatogr. and Chromatogr. Comunications, 11(2), 181-186, 1988.
88. OECD Guidline for Testing of Chemicals, Adopted by the Council on 30th March, 1989.
89. Pandey S.Y., Jain H.K., Agnihotri N.P., Pesistence of Disulfoton in Soil and its Residues in Moong (Phaseolus Aureus) and Cowpea (Vigna Sinensis), Indian J. Ag. Chem., 9, 61-66, 1976.
90. Pandey S.Y. and Agnihotri N.P., Effect of Fertilization on the Dégradation of Dicrotophos, Disulfoton, and Phorate in Soil, FertiUzer News, 20, 32-33, 1975.
91. Pesticide Residue Analysis (Procceding of joint FAO/WHO Course, 13-26 April 1983), PAO, Rome, Italy, 1983.
92. Procédures for Soil Analysis, ISRI, the Netherlands, 1980.
93. Ramsteiner K., HPLC Colunm Switching, a Step Toward die Automation of Sample Cleanup, Intem. J. Envir. Anal. Chem., 25, 49-65, 1986.
94. Robinson J.B., Chapman R.A., Détermination of Carbofuran Residues in Potato, Onion and Tumip: Comparative Analysing Using Gas Chromatography Selected Ion Monitoring or High-Performance Liquid Chromattography, J. Chromatogr., 193, 213-224, 1980.
96. Saltzman S., Mingelgrin U. Yaron B., Rôle of Water in the Hydrolysis of Parathion and Metyl Parathion on Kaolinite, J. Agr. Food Chem-, 24(4), 739-743, 1976.
97. Saxena A.N. and Peswani K.M., Influence of Soil Moisture on the Disspation of Phorate and Disulfoton in Soil and Mustard Crops, Indian J. Ent., 37, 68-71, 1975.
98. Serda C M . , Gibson D.T., Munnecke D.M., Lancaster J.H., Plasmid Invovement in Parathion Hydrolysis by Pseudomonas Diminuta, Appl. Environ. Microbiol. 44, 246-249, 1982.
99. Sethunathan N., Siddaramappa R., Rajaramk P., Barik S. and Wahid P.A. , Parathion: Residues in Soil and Water (see: Residue Reviews, 68, 91-122, 1977.
100. Shimadzu Application Data Book, Japan, 1994.
101. Siddrampra R., Rajaram K.P. and Sethimathan N., Dégradation of Parathion by Bacteria Isolated from Flood Soil, Applied Microbiology, 26, 846-849, 1973.
102. Sing R.P., Chiba M., Solubility of Benomyl in Water at Diffrent pHs and its Conversion to MBC, STB, BBU, J. Agr. Food Chem., 33(1-2), 63-67, 1985.
103. Slobonik J., Coroenewegen M.G.M., Brower E.R., Lignan H., Brinkman U.A.Th., Fully Automatic Multi-Residue Mediods for Trace Level Monitoring of Polar Pesticides by Liquid Chromatography, J. Chromatogr. 642(1-2), 359-370, 1993.
104. Solomon K.R., Bowheey C.S., Liber K., Stephenson G.R., Persistence of Hexazinone (Velpar), Trichlopyr (Galon) and 2.4-D in a Norûiem Otario Aquatic Environmnt, J. Agric. Food Chem., 38(6), 1314-1318,
105. Solomon K.R., Yoo J.Y., Lean D., Kaushik N.K., Day K.E., Stepphenson G.I., Methoxychlor Distribution Disspitation and Effecs in Freshwater Linnocorrah, Envi. Toxicol. Chem., 5, 577-586,, 1986. 106. Sphon J.A., Dmico J.N., The Mass SpecUa of Some Chlorinated
Automatic Pesicidal Copounds, Org. Mass Specu., 3, 51-62, 1970. 107. 107.Steinheiner T.R., HPLC Détermination of AlUazine and Physical
Dégradation in Agricultural Soil and Associated Surface and Grownd Water, J. Agr. Food Chem., 41(4), 250-255, 1993.
108. Suffet I.H., The p-value Approach to Quatitative Liquid ExUaction of Pesticides Herbicides from Water, 3-Liquid-Liquid ExUaction of Phenoxy Acid Herbicides from Water, J. Agr. Food Chem., 21(4), 591-598, 1973.
109. Suffet I.H., The p-Value Approach to Quatitative Liquid-Liquid ExUaction of Pesticides and Herbicides from Water. 2. Seleection of Solvent Ratio and Number of ExUactions, J. Agr. Food Chem. 21(2), 288-294, 1973.
110. Takahashi N., Mikami N., Photodegraation of die Herbicide Bromobuside in Water, J. Pesticide Science, 10(2), 247-256, 1985.