X Mつe"8 ej<"xem xét 違pj"j逢荏ng x穎 lý Argon-rncuoc"n‒p"8員e"8k吋m hình thái c栄a tinh b瓜t s逸n, b逸p.
X Bぐ trí thí nghiうm: m厩i lo衣i tinh b瓜t ch丑n ra m瓜t m磯u có m泳e" 8瓜 liên k院t ngang cao nh医t cùng v噂i m磯w"8嘘i ch泳pi"8go"8k"rj¤p"v ej.
X Cách tiｘn hành: m磯u tinh b瓜v"8逢嬰c s医y 荏 nhi羽v"8瓜 40oC trong m瓜v"pi {"8吋 8違m b違q"mj»"vt逢噂c khi ch映r0"Ucw"8„"o磯w"8逢嬰c phân b嘘8隠u trên khay ch泳a m磯u và ti院n hành ch映p trên thi院t b鵜 SEM-1400, JEOL, Nh壱t B違n.
3.5.5. Kh違o sát 違pj"j逢荏ng c栄a x穎 lý Argon-plasma lên màu s逸c c栄a tinh b瓜t s逸n, b逸p
X Mつe"8 ej<"xem xét 違pj"j逢荏ng x穎 lý Argon-plasma lên màu s逸c c栄a tinh b瓜t s逸n, b逸p.
X Bぐ trí thí nghiうm: m厩i lo衣i tinh b瓜t ch丑n ra m瓜t m磯u có m泳e" 8瓜 liên k院t ngang cao nh医t cùng v噂i m磯w"8嘘i ch泳pi"8go"8k"rj¤p"v ej.
X Cách tiｘn hành: M磯u tinh b瓜v" 8逢嬰c cho vào bich ni lông và ti院p" j pj" 8q"
b茨ng máy Minolta-CR400-Nh壱t B違n. K院t qu違 vjw"8逢嬰c là trung bình c栄a ba l亥p"8q"
l員p l衣ị Gía tr鵜 L, a, b bi吋u th鵜 l亥p"n逢嬰t màu tr逸pị"8臼 và vàng c栄a tinh b瓜t [51].
3.5.60"Zƒe"8鵜pj"mj違"p<pi"vk‒w"j„c in vitro e栄c"o磯w"vkpj"d瓜v"ucw"z穎"n#"rncuoc"d茨ng enzyme pancreatin và amyloglucosidase d茨ng enzyme pancreatin và amyloglucosidase
X Mつe"8 ej<"8ƒpj"ik違 違pj"j逢荏ng c栄a liên k院v"picpi"8院n kh違p<pi"vk‒w"j„c"e栄a tinh b瓜t s逸n, b逸p.
X Bぐ trí thí nghiうm: m厩i nguyên li羽u ch丑n ra 5 m磯u theo m泳e"8瓜 liên k院t ngang
mjƒe"pjcw"8go"8k"rj違n 泳ng.
X Cách tiｘn hành: L医y 2 g pancreatin j”c"vcp"vtqpi"46"on"p逢噂c c医t và khu医y
vtqpi"32"rj¿v0"Ucw"8„."n{"v¤o"荏 1500 vòng trong 10 phút. L医y 20 ml d鵜ch n鰻i sau ly tâm pha v噂i h厩n h嬰p g欝o"5.8"on"p逢噂c c医t, và 0,4 ml amyloglucosidasẹ Dung d鵜ch
gp¦{og""p {"8逢嬰e"8員t trong b吋8k隠u nhi羽t 荏 37 oC trong 10 phút.
Vkpj"d瓜v"52"oi""8逢嬰e"ejq"x q"嘘pi"grrgpfqth"vj吋"v ej"4"on"x噂k"o瓜v""j衣v"dk" vj栄{"vkpj0"O厩k"o磯w"n員r"n衣k"5"n亥p0"Ejq"2.97"on"fwpi"f鵜ej"8羽o"pcvtk"czgvcv"*rJ"704+" x q"ucw"8„"ejw{吋p"嘘pi"p {"x q"v栄"医o"pjk羽v"8»"59"oC trong 10 phút. Cho thêm vào
嘘pi"2.97"on fwpi"f鵜ej"gp¦{o"8«"ejw育p"d鵜"荏"vt‒p."o厩k"grrgpfqth"eƒej"pjcw"ej pj" zƒe"27"ik¤{0"Rj違p"泳pi"8逢嬰e"f瑛pi"n衣k"ucw"32"x "462"rj¿v"d茨pi"eƒej"8wp"u»k"vtqpi"32" rj¿v0"Inwequg"e„"8逢嬰e"v瑛"rj違p"泳pi"p {"8逢嬰e"vjw"n衣k"vtqpi"rj亥p"f鵜ej"p鰻k"d茨pi"eƒej" ly tâm (5000×g, 5 phút) và j o"n逢嬰pi"8逢運pi"zƒe"8鵜pj"d茨pi"rj逢挨pi"rjƒr"FPU0" Rj¤p"8q衣p"vkpj"d瓜v"8逢嬰e"rj¤p"nq衣k"f詠c"vt‒p"v嘘e"8瓜"e栄c"swƒ"vt·pj"vj栄{"rj¤p0" Vkpj"d瓜v"vk‒w"j„c"pjcpj"*TFƯ"x "vkpj"d瓜v"vk‒w"j„c"ej壱o"*UFƯ"8逢嬰e"zƒe"8鵜pj"d茨pi"
p欝pi"8瓜"inwequg"ucw"mjk"rj違p"泳pi"gp¦{og"vtqpi"32"x 462"rj¿v0"Rj亥p"vkpj"d瓜v"vt挨"
(Resistant starch-TƯ"n "rj亥p"e”p"n衣k không tiêu hóa sau 240 phút [52].
3.5.7. Kh違o sát 違pj"j逢荏ng c栄c"gp¦{og"vk‒w"j„c"n‒p"8員e"8k吋m hình thái c栄a tinh b瓜t s逸n, b逸p
X Mつe"8 ej<"zƒe"8鵜nh m泳e"8瓜 t医n công c栄a enzyme lên b隠 m員t tinh b瓜t
X Bぐ trí thí nghiうm: m厩i lo衣i nguyên li羽u l医y m磯u có m泳c liên k院t ngang cao nh医t cùng v噂i m磯w"8嘘i ch泳pi"8go"ej映p kính hi吋p"xk"8k羽n t穎 quét.
X Cách tiｘn hành: M磯w" 8逢嬰c r穎a hai l亥n b茨pi"p逢噂c c医v." ucw"8„"j衣t tinh b瓜t
8逢嬰c kh穎 p逢噂c b茨ng ethanol và thêm tert-butanol vào cu嘘i cùng s医y khô m磯u 荏
EJ姶愛PI"6<"M蔭V"SW謂"XÉ"DÉP"NW一P
6030"Dk院p"v pj"vkpj"d瓜v"u逸p"x "d逸r"d茨pi"rj逢挨pi"rjƒr"Ctiqp-pncuoc"荏"ƒr"uw医v" vj逢運pi
603030"O»"v違"8員e"8k吋o"e栄c"vkpj"d瓜v"d茨pi"rj鰻"HVKT"
Rj鰻"HVKT"8逢嬰e"u穎"f映pi"pj逢"o瓜v"e»pi"e映"8吋"8鵜pj"n逢嬰pi"x "o»"v違"u詠"vjc{"8鰻k"
trong e医w"vt¿e"e栄c"vkpj"d瓜v0"J·pj"6044 ejq"vj医{"rj鰻"HVKT"e栄c"vkpj"d瓜v"u逸p"ucw"mjk" z穎 n#"荏"eƒe"o泳e"vj運k"ikcp"x "8k羽p"ƒr"mjƒe"pjcw"vj·"eƒe"8雨pj"mj»pi"vjc{"8鰻k"uq"x噂k" o磯w"8嘘k"ej泳pị"mj»pi"zw医v"jk羽p"tj‒o"8雨pj"o噂k0"Vtqpi"x́pi"3722 - 800 cm-1e„"u詠" ej欝pi"ejfiq"rj鰻"rj泳e"v衣r"vtqpi"8„"ejk院o"逢w"vj院"n "u詠"fcq"8瓜pi"e栄c"mjwpi"r{tcpqug" vtqpi"rj¤p"v穎"inwequg"e栄c"vkpj"d瓜v"]7.47̲0"A雨pj";4;"eo-1n "fq"u詠"ikcq"8瓜pi"e栄c"nk‒p" m院v"g-1,4 glycosidic. A雨pj"p {"vtqpi"pijk‒p e泳w"e栄c"Fgg{ck"x "e瓜pi"u詠"*4234+"n "
924 cm-1 và 930 cm-1 vtqpi"pijk‒p"e泳w"e栄c"Tcoc¦cp"x "e瓜pi"u詠"*4224+0"Piw{‒p" pj¤p"f磯p"8院p"u詠"vjc{"8鰻k"x鵜"vt "p {"n "fq"e„"o員v"nk‒p"m院v"g-1,6 glycosidic trong phân
v穎"co{nqrgevkp."n o"f鵜ej"ejw{吋p"8雨pj"x隠"d逢噂e"u„pi"ecq"j挨p ]47̲0"Fcq"8瓜pi"e栄c
C-O-J" v衣k" 8雨pj"1016 cm-10" A雨pj" p {" vtqpi" pijk‒p" e泳w" e栄c" Tcoc¦cp" x " e瓜pi" u詠"
(2002) là 1094 cm-1 x " vtqpi" pijk‒p" e泳w" e栄c" Fgg{ck" x " e瓜pi" u詠" *4234+" n " v衣k
993 cm-1 ]7.47̲0"A雨pj"3464"eo-1 n "fq"u詠"ikcq"8瓜pi"e栄c"EJ2QJ"]47̲0"Rj¤p"v穎""p逢噂e" j医r"vjw"vtqpi"x́pi"x»"8鵜pj"j·pj"e栄c"vkpj"d瓜v"8逢嬰e"zƒe"8鵜pj"v衣k"8雨pj"3869"eo-1
và
8雨pj"3859"eo-1 p院w"j医r"vjw"vtqpi"x́pi"mj»pi"m院v"vkpj"e栄c"vkpj"d瓜v0"Vtqpi"pijk‒p" e泳w"e栄c"Fgg{ck"x "e瓜pi"u詠"*4234+"8雨pj"j医r"vjw"rj¤p"v穎"p逢噂e"vtqpi"x́pi"x»"8鵜pj" j·pj"e栄c"vkpj"d瓜v"u逸p là 1630 cm-10"U詠"mjƒe"dk羽v"vtqpi"m院v"sw違"p {"8逢嬰e"ik違k"vj ej"n " fq"mjƒe"pjcw"x隠"nq衣k"vkpj"vj吋 vtqpi"vkpj"d瓜v"]47̲0"X́pi"5822 - 3000 cm-1 là giao
8瓜pi"mfiq"e<pi"e栄c"pj„o"QJ0"X́pi"5222 - 2800 cm-1 n "ikcq"8瓜pi"dk院p"f衣pi"EJ2 ]47̲0"D違pi"607"v„o"v逸v"rj鰻"HVKT"e栄c"vkpj"d瓜v"u逸p0
Pj逢" x壱{" m院v" sw違" pijk‒p" e泳w" e栄c" ej¿pi" v»k" rj́" j嬰r" x噂k" eƒe" pijk‒p" e泳w" 8«" 8逢嬰e"e»pi"d嘘"vt逢噂e"8¤{0
Hình 4.220"Swcpi"rj鰻"HVKT"e栄c"vkpj"d瓜v"u逸p Ej¿"vj ej<"Vkpj"dじv"uｈp"vj»"*AE1+."zぬ"n#"32"rj¿v-6 kV (T-10P-8M+."zぬ"n#"32"rj¿v-8 kV (T-10P-:M+."zぬ"lý 20 phút-6 kV (T-20P-8M+."zぬ"n#"42"rj¿v-8 kV (T-20P-8K). D違pi"6070"A雨pj"j医r"vjw"eƒe"pj„o"ej栄"{院w"e栄c"vkpj"d瓜v"u逸p U嘘"u„pi"*eo-1 ) Nhóm 3282 Fcq"8瓜pi"mfiq"e<pi"Q-H 3000 - 2800 Fcq"8瓜pi"dk院p"f衣pi"EJ2 1647 J医r"vj映"rj¤p"v穎"p逢噂e"x q"x́pi"x»"8鵜pj"j·pj"e栄c"vkpj"d瓜v 1344 C-O-H, CH2 1242 CH2OH 1080 C-O, C-C, O-H 1047 C-O, C-C, C-O-H 1016 C-O-H
M院v"sw違"rj¤p"v ej"rj鰻"HVKT"vt‒p"vkpj"d瓜v"d逸r"v逢挨pi"v詠"pj逢"vkpj"d瓜v"u逸p."mj»pi" e„"u詠"mjƒe"dk羽v"8ƒpi"m吋"x隠"u嘘"n逢嬰pi"x "x鵜"vt "8雨pj"j医r"vjw"e栄c"o磯w"vkpj"d瓜v"dk院p"v pj" uq"x噂k"8嘘k"ej泳pi0"Vw{"pjk‒p"e„"vjc{"8鰻k"vtqpi"ikcq"8瓜pi"mfiq"e<pi"e栄c"pj„o"Q-J"v瑛"
3282 cm-1 荏"vkpj"d瓜v"u逸p"n‒p"5464"eo-1 荏"vkpj"d瓜v"d逸r0"U詠"vjc{"8鰻k"p {"n "fq"j o" n逢嬰pi"co{nqug"x "co{nqrgevkp"mjƒe"pjcw 荏"o厩k"nq衣k"vkpj"d瓜v"]47̲"*"j·pj"6043+0"D違pi" 608"v„o"v逸v"rj鰻"HVKT"e栄c"vkpj"d瓜v"d逸r0
Hình 4.230"Swcpi"rj鰻"HVKT"e栄c"vkpj"d瓜v"d逸r
Ej¿"vj ej<"Vkpj"dじv"dｈr"vj»"*AE2+."zぬ"n#"32"rj¿v-5 kV (M-10P-7M+."zぬ"n#"32"rj¿v-6 kV (M-10P-8M+."zぬ"n#"42"rj¿v-5 kV (M-20P-5K)."zぬ"n#"42"rj¿v-6 kV (M-20P-6K).
D違pi"6080"A雨pj"j医r"vjw"eƒe"pj„o"ej栄"{院w"e栄c"vkpj"d瓜v"d逸r J医r"vjw (cm-1) Nhóm 3242 Fcq"8瓜pi"mfiq"e<pi"Q-H 3000 - 2800 Fcq"8瓜pi"dk院p"f衣pi"EJ2 1647 J医r"vj映"rj¤p"v穎"p逢噂e"x q"x́pi"x»"8鵜pj"j·pj"e栄c"vkpj"d瓜v 1344 C-O-H, CH2 1242 CH2OH 1080 C-O, C-C, O-H 1047 C-O, C-C, C-O-H 1016 C-O-H
929 C-O-E"*"ikcq"8瓜pi"e栄c"nk‒p"m院v"g-1,4 glycosidic)
603040"O泳e"8瓜"nk‒p"m院v"picpi"
Rj鰻"HVKT"ejq"dk院v"rj¤p"v穎"p逢噂e"8逢嬰e"ik英"n衣k"vtqpi"e医w"vt¿e"e栄c"vkpj"d瓜v"pj運" nk‒p" m院v" ej員v" x " nk‒p" m院v" {院w" x噂k" rj¤p" v穎" p逢噂e0" Ej¿pi" 8逢嬰e" vj吋" jk羽p" 荏" jck" 8雨pj"
(1647; 3282 cm-1+"vtqpi"vkpj"d瓜v"u逸p"jc{"jck"8雨pj"*3869="5464"eo-1+"vtqpi"vkpj"d瓜v" d逸r0"Swc"8„"e„"vj吋"zƒe"8鵜pj"8逢嬰e"o泳e"8瓜"nk‒p"m院v"picpi"v瑛"jk羽w"e逢運pi"8瓜"v逢挨pi" 8嘘k"e栄c"8雨pj"E-O-J"x噂k"jck"8雨pj"p {"]7]. 60304030"O泳e"8瓜"nk‒p"m院v"picpi"vtqpi"vkpj"d瓜v"u逸p Swc"rj¤p"v ej"e医w"vt¿e"e栄c"vkpj"d瓜v"u逸p"d茨pi"rj鰻"HVKT"vc"dk院v"8逢嬰e"vkpj"d瓜v" u逸p"e„"8雨pj"j医r"vjw"nk‒p"m院v"ej員v"x噂k"p逢噂e"v衣k"3869"eo-1 x "8雨pj"nk‒p"m院v"{院w"x噂k" p逢噂e" v衣k" 54:4" eo-10" O泳e" 8瓜" nk‒p" m院v" picpi" vtqpi" vkpj" d瓜v" 8逢嬰e" v pj" d茨pi" jck" rj逢挨pi"rjƒr<"*C+"3238"- 1647 (cm-1) và (B) 1016 - 3282 (cm-1+0"M院v"sw違"x隠"o泳e"8瓜" nk‒p"m院v"picpi"ik英c"eƒe"o磯w"z穎"n#"e栄c"vkpj"d瓜v"u逸p"8逢嬰e"vj吋"jk羽p"vtqpi"d違pi"6090"
M院v"sw違"v瑛"d違pi"609"ejq"vc"vj医{<"vjgq"rj逢挨pi"rjƒr"*C+."x噂k"épi"vj運k"ikcp"z穎" n#."o泳e"8瓜"nk‒p"m院v"picpi"e栄c"o磯w"vkpj"d瓜v"u逸p"dk院p"v pj"v<pi"vw{院p"v pj"v瑛"6"mX"8院p" :"mX"x "ucw"8„"ik違o"zw嘘pi0"雲"épi"8k羽p"áp z穎"n#."o泳e"8瓜"nk‒p"m院v"picpi"e栄c"o磯w" vkpj"d瓜v"u逸p"dk院p"v pj"v<pi"vw{院p"v pj"v瑛"7"rj¿v"8院p"32"rj¿v"t欝k"ucw"8„"ik違o"zw嘘pi0" O磯w"vkpj"d瓜v"u逸p"z穎"n#"荏"7"rj¿v."6"mX"8衣v"o泳e"8瓜"nk‒p"m院v"picpi"n "2.:6:"x "i医r"
3.9;"n亥p"uq"x噂k"o磯w"8嘘k"ej泳pi0"O磯w"vkpj"d瓜v"u逸p"8逢嬰e"z穎"n#"荏"32"rj¿v.":"mX"8衣v" o泳e"8瓜"nk‒p"m院v"picpi"e詠e"8衣k"x "i医r"4.69"n亥p"uq"x噂k"o磯w"8嘘k"ej泳pi0"O泳e"8瓜"nk‒p" m院v"picpi"v pj"vjgq"rj逢挨pi"rjƒr"D"ejq"vj医{"u詠"rj́"j嬰r"x噂k"o泳e"8瓜"nk‒p"m院v"picpi" v pj"vjgq"rj逢挨pi"rjƒr"C."o員e"f́"ikƒ"vt鵜"8衣v"8逢嬰e"vj医r"j挨p0 M院v"sw違"p {"nk‒p"swcp"vt詠e"vk院r"8院p"e逢運pi"8瓜"8雨pj"QJ0"Vj運k"ikcp"8亥w"z穎"n#" v医v"e違"eƒe"rj¤p"v穎"vkpj"d瓜v"vt‒p"d隠"o員v"8逢嬰e"m ej"jq衣v"f磯p"8院p"j·pj"vj pj"nk‒p"m院v" picpi"x "rj¤p"v穎"p逢噂e0"Pj運"8瓜"育o"dcp"8亥w"e栄c"vkpj"d瓜v"vj医r"p‒p"p逢噂e"v衣q"tc"8逢嬰e" j医r"vjw"x q"x́pi"x»"8鵜pj"j·pj"e栄c"vkpj"d瓜v"x "v<pi"v益"n羽"pj鵜"vt́pi"j嬰r"]5;̲0"Vj運k" ikcp"z穎"n#"e pi"f k."8k羽p"áp z穎"n#"e pi"ecq"n o"ik違o"eƒe"rj¤p"v穎"v詠"fq"vt‒p"d隠"o員v" x "u胤"8衣v"8院p"vt衣pi"vjƒk"d«q"j”c"ucw"o瓜v"vj運k"ikcp"z穎"n#"]5;̲0"Dk吋w"8欝"603"vj吋"jk羽p" e逢運pi"8瓜"8雨pj"e栄c"o瓜v"u嘘"pj„o"ej泳e"vtqpi"vkpj"d瓜v"u逸p0"Vtqpi"8„"vc"e„"vj吋"pj·p" vj医{"t茨pi"eƒe"8雨pj"nk‒p"swcp"8院p"pj„o"QJ"i欝o"54:4="3869="3466="3238"eo-1vw{院p" v pj"vjgq"o泳e"8瓜"nk‒p"m院v"picpi0"Vtqpi"8„"8雨pj"3238"eo-1 v<pi"vw{院p"v pj"x噂k"o泳e" 8瓜"nk‒p"m院v"picpi"vjgq"rj逢挨pi"vt·pj"{"?"3.32;z"-"2.567"*T2 ?"2.;4+0"A雨pj"54:4"eo-1 vw{院p" v pj" vjgq" o泳e" 8瓜" nk‒p" m院v" picpi" vjgq" rj逢挨pi" vt·pj" {" ?" 2.863z" Î 0,027 (R2 = 0,929).
D違pi"6090"謂pj"j逢荏pi"e栄c"8k羽n áp x "vj運k"ikcp"z穎"n#"Ctiqp-rncuoc"8院p"o泳e"8瓜"j·pj"vj pj"nk‒p"m院v"ngang vtqpi"u違p"rj育o" vkpj"d瓜v"u逸p"dk院p"v pj1 Nk‒p"m院v" ngang Vj運k"ikcp" ( phút) Ak羽p"áp (kV) 4 5 6 7 8 9 1016-1647 (A) AE 0,47 ± 0,06aA 0,47 ± 0,06aA 0,47 ± 0,06aA 0,47 ± 0,06aA 0,47 ± 0,06aA 0,47 ± 0,06aA 5 0,85 ± 0,03bD 0,88 ± 0,01bcD 0,93 ± 0,08 bcdC 0,97 ± 0,06cdD 0,99 ± 0,025dB 0,61 ± 0,06aB 10 0,70 ± 0,08aBC 0,94 ± 0,06bD 0,96 ± 0,06bC 0,99 ± 0,02bD 1,17 ± 0,06cC 0,75 ± 0,08aC 20 0,72 ± 0,03aBC 0,80 ± 0,01bC 0,88 ± 0,04cC 0,88 ± 0,02cC 0,95 ± 0,04dB 0,72 ± 0,06aC 30 0,74 ± 0,06aC 0,72 ± 0,06aB 0,72 ± 0,06aB 0,8 ± 0,02aB 1,05 ± 0,08bB 1,00 ± 0,03bD 40 0,63 ± 0,02aB 0,68 ± 0,01abB 0,69 ± 0,06abcB 0,77 ± 0,02cB 1,04 ± 0,07dB 0,75 ± 0,06bcC 1016-3282 (B) AE 0,59 ± 0,01aA 0,59 ± 0,01aA 0,59 ± 0,01aA 0,59 ± 0,01aA 0,59 ± 0,01aA 0,59 ± 0,01aA 5 0,59 ± 0,01aA 0,60 ± 0,01aA 0,82 ± 0,01cD 0,87 ± 0,01dC 0,88 ± 0,01dC 0,74 ± 0,03bC 10 0,77 ± 0,01aD 0,84 ± 0,01bD 0,91 ± 0,01cE 1,00 ± 0,04dD 1,00 ± 0,05dD 0,80 ± 0,01abD 20 0,72 ± 0,03abCD 0,78 ± 0,01bcC 0,79 ± 0,01bcC 0,85 ± 0,06cC 0,74 ± 0,06bB 0,66 ± 0,04aB 30 0,69 ± 0,02aBC 0,68 ± 0,03aB 0,70 ± 0,01aB 0,69 ± 0,02aB 0,88 ± 0,03cC 0,78 ± 0,03bD 40 0,65 ± 0,05aB 0,67 ± 0,03abB 0,72 ± 0,03bB 0,72 ± 0,03bB 0,86 ± 0,05cC 0,70 ± 0,01abC 1Eƒe"ikƒ"vtお"vtqpi"dＶpi"dkあw"vjお"ikƒ"vtお"vtwpi"d·pj"ł"8じ"nうej"ejwｂp"*p?5+ Eƒe"ikƒ"vtお"e„"m#"jkうw"kp"jqc"vtqpi"épi"oじv"eじv"jc{"m#"jkうw"kp"vj⇔ぜpi"vtqpi"épi"oじv"j pi"mjƒe"pjcw"ぞ"oざk"rj⇔￢pi"rjƒr"v pj" oとe"8じ"nk‒p"mｘv"picpi"dkあw"vjお"uば"mjƒe"dkうv"*r>2027+ A: Tínj"vjgq"rj⇔￢pi"rjƒr"C; D<"V pj"vjgq"rj⇔￢pi"rjƒr"D
Dk吋w"8欝6030"E逢運pi"8瓜"8雨pj"e栄c"o磯w"vkpj"d瓜v"u逸p"vjgq"o泳e"8瓜"nk‒p"m院v"picpi
Ej¿"vj ej<"Vkpj"dじv"uｈp"vj»"*AE1+."zぬ"n#"32"rj¿v-6 kV (T-10P-8M+."zぬ"n#"32"rj¿v-8 kV (T-10P-:M+."zぬ"n#"42"rj¿v-6 kV (T-20P-8M+."zぬ"n#"42"rj¿v-8 kV (T-20P-8K).
4.1.2.2. O泳e"8瓜"nk‒p"m院v"picpi"vtqpi"vkpj"d瓜v"d逸r"
Vkpj"d瓜v"d逸r"e„"8雨pj"j医r"vjw"nk‒p"m院v"ej員v"x噂k"p逢噂e"v衣k"3869"eo-1 x "8雨pj"j医r" vjw"nk‒p"m院v"{院w"x噂k"p逢噂e"v衣k"8雨pj"5464"eo-10"V瑛"m院v"sw違"p {"vc"e„"vj吋"v pj"8逢嬰e"o泳e" 8瓜"nk‒p"m院v"picpi"vtqpi"vkpj"d瓜v"d逸r"d茨pi"jck"rj逢挨pi"rjƒr<"*E+"3238"Î 1647 (cm-1) và (D) 1016 Î 3242 (cm-1+0"M院v"sw違"x隠"o泳e"8瓜"nk‒p"m院v"picpi"ik英c"eƒe"o磯w"z穎"n#" e栄c"vkpj"d瓜v"d逸r"8逢嬰e"vj吋"jk羽p"vtqpi"d違pi"60:0
Pj·p"x q"d違pi"60:"vc"pj壱p"vj医{<"vjgq"rj逢挨pi"rjƒr"*E+."x噂k"épi"vj運k"ikcp"z穎" n#."o泳e"8瓜"nk‒p"m院v"picpi"vtqpi"o磯w"vkpj"d瓜v"d逸r"dk院p"v pj"v<pi"vw{院p"v pj"v瑛"6"mX" 8院p"8"mX"x "ucw8„"ik違o"zw嘘pi0"雲"épi"o瓜v"8k羽p"ƒr z穎"n#."o泳e"8瓜"nk‒p"m院v"picpi" e栄c"o磯w"vkpj"d瓜v"d逸r"dk院p"v pj"v<pi"vw{院p"v pj"v瑛"7"rj¿v"8院p"42"rj¿v"x "ucw"8„"ik違o" zw嘘pi0"O磯w"vkpj"d瓜v"d逸r"8逢嬰e"z穎"n#"荏"7"rj¿v."6"mX"o泳e"nk‒p"m院v"picpi"n "2.:93"x " i医r"3.57"n亥p"uq"x噂k"o磯w"8嘘k"ej泳pi0"O磯w"vkpj"d瓜v"d逸r"8逢嬰e"z穎"n#"荏"32"rj¿v"8"mX"8衣v" o泳e"8瓜"nk‒p"m院v"picpi"e詠e"8衣k"x "i医r"4"n亥p"uq"x噂k"o磯w"8嘘k"ej泳pi0"O泳e"8瓜"nk‒p"m院v" picpi"v pj"vjgq"rj逢挨pi"rjƒr"F"e pi"ejq"m院v"sw違"v逢挨pi"v詠"pj逢"v pj"vjgq"rj逢挨pi" rjƒr"E"pj逢pi"ikƒ"vt鵜"8衣v"8逢嬰e"vj医r"j挨p0" 3282 cm-1 1647 cm-1 1244 cm-1 1016 cm-1 929 cm-1 a b c d e
V逢挨pi"v詠"pj逢"vkpj"d瓜v"u逸p0"M院v"sw違"x隠"o泳e"8瓜"nk‒p"m院v"picpi"vtqpi"vkpj"d瓜v" d逸r"e pi"nk‒p"swcp"vt詠e"vk院r"8院p"e逢運pi"8瓜"8雨pj"QJ0"V瑛"dk吋w"8欝"604"pj壱p"vj医{"t茨pi" 8雨pj" 3238" eo-1 v<pi" vw{院p" v pj" x噂k" o泳e" 8瓜" nk‒p" m院v" picpi" vjgq" rj逢挨pi" vt·pj"
y = 1,237x + 0,148 (R2 ?"2.;5:+"x "8雨pj"5464 cm-1 v<pi"vw{院p"v pj"x噂k"o泳e"8瓜"nk‒p" m院v"picpi"vjgq"rj逢挨pi"vt·pj"{"?"2.::7z"Î 0,263 (R2 = 0,837). Mjk"uq"uƒpj"8k隠w"mk羽p"z穎"n#"8吋"v衣q"o泳e"8瓜"nk‒p"m院v"picpi"ecq"pj医v"ik英c"vkpj" d瓜v"d逸r"x "u逸p."ej¿pi"v»k"pj壱p"vj医{"vkpj"d瓜v"d逸r"pj衣{"e違o"j挨p"x噂k"8k羽p"ƒrz穎"n#0"A吋" 8衣v"8逢嬰e"o泳e"8瓜"nk‒p"m院v"picpi"ecq"pj医v"vtqpi"épi"o瓜v"8k隠w"mk羽p"mj違q"uƒv"vj·"vkpj" d瓜v"d逸r"ej雨"e亥p"o瓜v"8k羽p áp 8"mX"vjc{"x·":"mX"pj逢"vkpj"d瓜v"u逸p0"Pj逢pi"n衣k"e亥p"vj運k" ikcp"z穎"n#"f k"j挨p0"U詠"mjƒe"dk羽v"p {"e„"vj吋"fq"piw欝p"i嘘e"x "v pj"ej医v"mjƒe"dk羽v"e栄c" jck"nq衣k"vkpj"d瓜v0"
D違pi"60:0"謂pj"j逢荏pi"e栄c"8k羽n áp x "vj運k"ikcp"z穎"n#"Argon-plasma 8院p"o泳e"8瓜"j·pjvj pj"nk‒p"m院v"picpi"vtqpi"u違p"rj育o" vkpj"d瓜v"d逸r"dk院p"v pj1 Nk‒p"m院v" ngang Vj運k"ikcp" ( phút) Ak羽p"ƒr (kV) 4 5 6 7 8 9 1016-1647 (C) AE 0,64 ± 0,07aA 0,64 ± 0,07aA 0,64 ± 0,07aA 0,64 ± 0,07aA 0,64 ± 0,07aA 0,64 ± 0,07aA 5 0,87 ± 0,05bBC 0,93 ± 0,07bcB 0,99 ± 0,04cB 0,90 ± 0,01bC 0,79 ± 0,02aB 0,75 ± 0,01aB 10 0,89 ± 0,09abBC 0,91 ± 0,04bcB 1,03 ± 0,03cB 0,79 ± 0,09aB 0,80 ± 0,05aB 0,88 ± 0,03 abC 20 0,80 ± 0,03aB 1,19 ± 0,05cC 1,26 ± 0,05dC 1,26 ± 0,06dD 1,06 ± 0,02bC 1,19 ± 0,02cE 30 0,96 ± 0,06bC 1,16 ± 0,07cC 1,28 ± 0,02dC 0,94 ± 0,04bC 0,78 ± 0,02aB 1,21 ± 0,05cdE 40 1,22 ± 0,04dD 0,95 ± 0,02bB 1,20 ± 0,02dC 0,86 ± 0,04aBC 1,07 ± 0,06cC 1,01 ± 0,01cD 1016-3242 (D) AE 0,65 ± 0,01aAB 0,65 ± 0,01aB 0,65 ± 0,01aA 0,65 ± 0,01aC 0,65 ± 0,01aC 0,65 ± 0,01aB 5 0,71 ± 0,02cCD 0,79 ± 0,02dD 0,78 ± 0,02dB 0,7 ± 0,02bcD 0,68 ± 0,02abD 0,66 ± 0,02aBC 10 0,76 ± 0,06cD 0,74 ± 0,01bcC 0,78 ± 0,01cB 0,7 ± 0,04abD 0,69 ± 0,01abD 0,68 ± 0,03aC 20 0,69 ± 0,02bBC 0,75 ± 0,03cC 0,92 ± 0,04dC 0,69 ± 0,01bD 0,66 ± 0,01abC 0,64 ± 0,01aB 30 0,59 ± 0,03cA 0,66 ± 0,02dB 0,66 ± 0,01dA 0,55 ± 0,01bB 0,48 ± 0,01aA 0,64 ± 0,01dB 40 0,66 ± 0,01dB 0,57 ± 0,03cA 0,67 ± 0,01dA 0,47 ± 0,01aA 0,53 ± 0,01bB 0,58 ± 0,01cA 1Eƒe"ikƒ"vtお"vtqpi"dＶpi"dkあw"vjお"ikƒ"vtお"vtwpi"d·pj"ł"8じ"nうej"ejwｂp"*p?5+ Eƒe"ikƒ"vtお"e„"m#"jkうw"kp"jqc"vtqpi"épi"oじv"eじv"jc{"m#"jkうw"kp"vj⇔ぜpi"vtqpi"épi"oじv"j pi"mjƒe"pjcw"ぞ"oざk"rj⇔￢pi"rjƒr"v pj" oとe"8じ"nk‒p"mｘv"picpi"dkあw"vjお"uば"mjƒe"dkうv"*r>2027+0 C: Típj"vjgq"rj⇔￢pi"rjƒr"E; F<"V pj"vjgq"rj⇔￢pi"rjƒr"F
Dk吋w"8欝"6040"A雨pj"QJ"荏"eƒe"pijk羽o"vj泳e"x噂k"o泳e"8瓜"nk‒p"m院v"picpi"mjƒe"pjcw
Ej¿"vj ej<"Vkpj"dじv"dｈr"vj»"*AE2+."zぬ"n#"32"rj¿v-5 kV (M-10P-7M+."zぬ"n#"32"rj¿v-6 kV (M-10P-8M+."zぬ"n#"42"rj¿v-5 kV (M-20P-7M+."zぬ"n#"42"rj¿v-6 kV (M-20P-6K).
603050"Pjk羽v"vt丑pi"n逢嬰pi"*VIC+"e栄c"vkpj"d瓜v" 60305030"Pjk羽v"vt丑pi"n逢嬰pi"*VIC+"e栄c"vkpj"d瓜v"u逸p
A逢運pi" eqpi" VIC" e栄c" vkpj" d瓜v" u逸p" 8逢嬰e" vj吋" jk羽p" vtqpi" j·pj" 6047" vtqpi" 8„" ej¿pi" v»k" vk院p" j pj" mk吋o" vtc" 7" o磯w" i欝o" o磯w" vj»." o磯w"T-20P-6K, T-20P-8K, T-10P-6K, T-10P-:M."n亥p"n逢嬰v"vjgq"vj泳"v詠"v<pi"f亥p"o泳e"8瓜"nk‒p"m院v"picpi0"
V瑛"j·pj"6044 x "d違pi"60;"ej¿pi"vc"pj壱p"vj医{"o泳e"8瓜"o医v"mj嘘k"n逢嬰pi"e栄c"o磯w"
T-10P-:M" vj医r" j挨p" eƒe" o磯w" e”p" n衣k0" Vt‒p" 8逢運pi" eqpi" VIC" mj嘘k" n逢嬰pi" e栄c" eƒe" o磯w"p {"8隠w"v鰻p"vj医v"vjgq"jck"d逢噂e"]72̲0"D逢噂e"8亥w"vk‒p"eƒe"o磯w"vkpj"d瓜v"u逸p"o医v" mj嘘k" n逢嬰pi" vtqpi" mjq違pi" pjk羽v" 8瓜" 48.88" 8院p" V1Ó" ?" 3;9.;9oE0" X噂k"tm1 v瑛" :.8:" *o磯w"V-10P-:M+"8院p"34.98'"*o磯w"AE1+0"Vtqpi"d逢噂e"p {"u詠"jcq"j映v"mj嘘k"n逢嬰pi"n " fq"jk羽p"v逢嬰pi"o医v"p逢噂e"vtqpi"piw{‒p"nk羽w"]72̲0"Ucw"mjk"o医v"p逢噂e"mj嘘k"n逢嬰pi"o磯w" vkpj" d瓜v" piw{‒p" nk羽w" 鰻p" 8鵜pj" 8院p" pjk羽v" 8瓜" 453.;6oE" *AE1+" jc{" pjk羽v" 8瓜" 4;:oC (T-10P-:M+0"Ecq"j挨p"o泳e"pjk羽v"8瓜"p {"u詠"rj¤p"j栄{"o磯w"d逸v"8亥w"z違{"tc"ejq"8院p"mjk" 8衣v" pjk羽v" 8瓜" V2Ó" ?" " 6:9.8;oE" x噂k" o泳e" jcq" j映v" n " :3.77'" *AE1+" x " 8院p" pjk羽v" 8瓜"
a b c d e 3242 cm-1 1647 cm-1 1244 cm-1 1016 cm-1 929 cm-1
600,9oE" x噂k" o泳e" jcq" j映v" 9;.5'" *V-10P-:M+0" Piw{‒p" pj¤p" jcq" j映v" mj嘘k" n逢嬰pi" vtqpi"d逢噂e"p {"n "fq"swƒ"vt·pj"qz{"j„c"eƒe"ej医v"j英w"e挨"]72̲0"M院v"sw違"x隠"jcq"j映v" mj嘘k"n逢嬰pi"vjgq"pjk羽v"8瓜"8逢嬰e"v„o"v逸v"vtqpi"d違pi"60;0"Pj逢"x壱{"mjk"nk‒p"m院v"picpi" h·pj"vj pj"u胤"j衣p"ej院"jcq"j映v"mj嘘k"n逢嬰pi"vtqpi"piw{‒p"nk羽w."n o"v<pi"mj違"p<pi"ej鵜w" 8逢嬰e"pjk羽v"8瓜"j挨p"vkpj"d瓜v"v詠"pjk‒p0" M院v"sw違"pijk‒p"e泳w"e栄c"ej¿pi"v»k"rj́"j嬰r"x噂k"m院v"nw壱p"e栄c"eƒe"pijk‒p"e泳w" vt逢噂e"8¤{"pj逢"e栄c"McxncpkPggnco"x "e瓜pi"u詠"*4234+"x "Ujgtt{"Z0"Zkg"x "e瓜pi"u詠"
(2005) [31,32].
Hình 4.240"A逢運pi"eqpi"VIC"e栄c"vkpj"d瓜v"u逸p
Ej¿"vj ej<"Vkpj"dじv"uｈp"vj»"*AE1+."zぬ"n#"32"rj¿v-6 kV (T-10P-8M+."zぬ"n#"32"rj¿v-8 kV (T-10P-:M+."zぬ"n#"42"rj¿v-6 kV (T-20P-8M+."zぬ"n#"42"rj¿v-8 kV (T-20P-8K).
D違pi"60;0"O泳e"8瓜"jcq"j映v"mj嘘k"n逢嬰pi"e栄c"vkpj"d瓜v"u逸p"mjk"rj¤p"v ej"VIC
Pijk羽o"vj泳e Ikck"8q衣p"3 Ikck"8q衣p"4
tT1 (oC) tm1 (%) tT2 (oC) tm2 (%) AE1 26,66 - 118,08 12,76 231,94 - 487,69 81,92 T-10P-6K 26,66 - 186,73 8,75 270,82 - 548,46 80,98 T-10P-8K 26,66 - 197,97 7,89 298,00 - 600,9 79,19 T-20P-6K 26,66 - 146,14 10,65 247,95 - 488,53 81,01 T-20P-8K 26,66 - 134,12 10,87 247,1 - 538 80,4 tT1 = T1-T1Ó<"MjqＶpi"pjkうv"8じ"zＶ{"tc"swƒ"vt·pj"oＸv"p⇔ずe"vtqpi"vkpj"dじv"uｈp T1<"Pjkうv"8じ"dｈv"8Ｚw"swƒ"vt·pj"8q"pjkうv"vtがpi"n⇔ぢpi"eてc"vkpj"dじv"uｈp T1Ó<"Pjkうv"8じ"mｘv"vj¿e"ikck"8qＴp"3"*ikck"8qＴp"oＸv"p⇔ずe+ tm1 = m1-m1Ó<"jcq"jつv"mjぐk"n⇔ぢpi"fq"swƒ"vt·pj"oＸv"p⇔ずe" m1<"'"mjぐk"n⇔ぢpi"oｄw"ぞ"pjkうv"8じ"V1; m1Ó<"'"mjぐk"n⇔ぢpi"oｄw"ぞ"pjkうv"8じ"V1Ó tT2 = T2-T2Ó<"MjqＶpi"pjkうv"8じ"zＶ{"tc"swƒ"vt·pj"qz{"j„c"eƒe"ejＸv"jのw"e￢"vtqpi"vkpj" dじv"uｈp T2<"Pjkうv"8じ"dｈv"8Ｚw"swƒ"vt·pj"qz{"j„c T2Ó<"Pjkうv"8じ"mｘv"vj¿e"swƒ"vt·pj"qz{"j„c tm2 = m2-m2Ó<"jcq"jつv"mjぐk"n⇔ぢpi"vtqpi"ikck"8qＴp"4"*ikck"8qＴp"qz{"j„c+" m2<"'"mjぐk"n⇔ぢpi"oｄw"ぞ"pjkうv"8じ"V2 ; m2Ó<"'"mjぐk"n⇔ぢpi"oｄw"ぞ"pjkうv"8じ"V2Ó 4.1.3.2. Pjk羽v"vt丑pi"n逢嬰pi"*VIC+"e栄c"vkpj"d瓜v"d逸r M院v"sw違"vjw"8逢嬰e"v瑛"vkpj"d瓜v"d逸r"e pi"ik嘘pi"pj逢"vkpj"d瓜v"u逸p0"O泳e"8瓜"jcq"j映v" mj嘘k"n逢嬰pi"vjgq"pjk羽v"8瓜"e pi"8逢嬰e"ejkc"tc"n o"jck"ikck"8q衣p"ej pj0
V瑛"j·pj"6045 x "d違pi"6032"ej¿pi"vc"pj壱p"vj医{" o泳e"8瓜" o医v"mj嘘k" n逢嬰pi"e栄c" o磯w"O-20P-8M"vj医r"j挨p"eƒe"o磯w"e”p"n衣k0"Vt‒p"8逢運pi"eqpi"VIC"mj嘘k"n逢嬰pi"e栄c" eƒe"o磯w"p {"8隠w"v鰻p"vj医v"vjgq"jck"d逢噂e"]72̲0"D逢噂e"8亥w"vk‒p"eƒe"o磯w"vkpj"d瓜v"u逸p" o医v" mj嘘k" n逢嬰pi" vtqpi" mjq違pi" pjk羽v" 8瓜" 48.88" 8院p" V1Ó" ?" 39:.47oE0" X噂k"tm1 v瑛 8.88"*"o磯w"O-20P-8M+"8院p"35.79'"*"o磯w"AE2+0"Vtqpi"d逢噂e"p {"u詠"jcq"j映v"mj嘘k"
n逢嬰pi"n "fq"jk羽p"v逢嬰pi"o医v"p逢噂e"vtqpi"piw{‒p"nk羽w"]72̲0"Ucw"mjk"o医v"p逢噂e"mj嘘k" n逢嬰pi"o磯w"vkpj"d瓜v"piw{‒p"nk羽w"鰻p"8鵜pj"8院p"pjk羽v"8瓜"472.24oE"*"AE2+"jc{"pjk羽v"8瓜"
276,47oC (M-20P-8M+0"Ecq"j挨p"o泳e"pjk羽v"8瓜"p {"u詠"rj¤p"j栄{"o磯w"d逸v"8亥w"z違{"tc" ejq"8院p"mjk"8衣v"pjk羽v"8瓜"V2Ó"?"503,09oE"x噂k"o泳e"jcq"j映v"n ":7.25'"*AE2+"X "8院p" pjk羽v"8瓜"763.::oE"x噂k"o泳e"jcq"j映v":5.2:'"*O-20P-8M+0"Piw{‒p"pj¤p"jcq"j映v"mj嘘k" n逢嬰pi"vtqpi"d逢噂e"p {"n "fq"swƒ"vt·pj"qz{"j„c"eƒe"ej医v"j英w"e挨"]70̲0"M院v"sw違"x隠"jcq" j映v"mj嘘k"n逢嬰pi"vjgq"pjk羽v"8瓜"8逢嬰e"v„o"v逸v"vtqpi"d違pi"60320"Pj逢"x壱{"mjk"nk‒p"m院v" picpi"j·pj"vj pj"u胤"j衣p"ej院"jcq"j映v"mj嘘k"n逢嬰pi"vtqpi"piw{‒p"nk羽w."n o"v<pi"mj違" p<pi"ej鵜w"8逢嬰e"pjk羽v"8瓜"j挨p"vkpj"d瓜v"v詠"pjk‒p0"
M院v"sw違"pijk‒p"e泳w"e栄c"ej¿pi"v»k"rj́"j嬰r"x噂k"m院v"nw壱p"e栄c"eƒe"pijk‒p"e泳w" vt逢噂e"8¤{"pj逢"e栄c"McxncpkPggnco"x "e瓜pi"u詠"*4234+"x "Ujgtt{"Z0"Zkg"x "e瓜pi"u詠"
(2005) [31,32].
Hình 4.250"A逢運pi"eqpi"VIC"e栄c"vkpj"d瓜v"d逸r
Ej¿"vj ej<"Vkpj"dじv"dｈr"vj»"*AE2+."zぬ"n#"32"rj¿v-5 kV (M-10P-7M+."zぬ"ný 10 phút-6 kV (M-10P-8M+."zぬ"n#"42"rj¿v-5 kV (M-20P-7M+."zぬ"n#"42"rj¿v-6 kV (M-20P-6K).
D違pi"60320"O泳e"8瓜"jcq"j映v"mj嘘k"n逢嬰pi"e栄c"vkpj"d瓜v"d逸r"mjk"rj¤p"v ej"VIC
Pijk羽o"vj泳e Ikck"8q衣p"3 Ikck"8q衣p"4
tT1 (oC) tm1 (%) tT2 (oC) tm2 %) AE2 26,62 - 157,47 13,57 250,02 Î 503,09 85,03 M-10P-5K 26,62 - 160,94 12,35 259,43 Î 521,56 84,82 M-10P-6K 26,62 Î 163,54 10,33 260,28 Î529,18 84,80 M-20P-5K 26,62 - 165,27 8,81 268,87 - 530,05 84,38 M-20P-6K 26,62 - 178,25 6,66 276,47 Î541,88 83,56 tT1 = T1-T1Ó<"MjqＶpi"pjkうv"8じ"zＶ{"tc"swƒ"vt·pj"oＸv"p⇔ずe"vtqpi"vkpj"dじv"dｈr T1<"Pjkうv"8じ"dｈv"8Ｚw"swƒ"vt·pj"8q"pjkうv"vtがpi"n⇔ぢpi"eてc"vkpj"dじv"dｈr T1Ó<"Pjkうv"8じ"mｘv"vj¿e"ikck"8qＴp"3"*ikck"8qＴp"oＸv"p⇔ずe+ tm1 = m1-m1Ó<"jcq"jつv"mjぐk"n⇔ぢpi"fq"swƒ"vt·pj"oＸv"p⇔ずe" m1<"'"mjぐk"n⇔ぢpi"oｄw"ぞ"pjkうv"8じ"V1; m1Ó<"'"mjぐk"n⇔ぢpi"oｄw"ぞ"pjkうv"8じ"V1Ó tT2 = T2-T2Ó<"MjqＶpi"pjkうv"8じ"zＶ{"tc"swƒ"vt·pj"qz{"j„c"eƒe"ejＸv"jのw"e￢"vtqpi"vkpj" dじv"dｈr T2<"Pjkうv"8じ"dｈv"8Ｚw"swƒ"vt·pj"qz{"j„c T2Ó<"Pjkうv"8じ"mｘv"vj¿e"swƒ"vt·pj"qz{"j„c tm2 = m2-m2Ó<"jcq"jつv"mjぐk"n⇔ぢpi"vtqpi"ikck"8qＴp"4"*ikck"8qＴp"qz{"j„c+" m2<"'"mjぐk"n⇔ぢpi"oｄw"ぞ"pjkうv"8じ"V2 ; m2Ó<"'"mjぐk"n⇔ぢpi"oｄw"ぞ"pjkうv"8じ"V2Ó 603060"A員e"8k吋o"j·pj"vjƒk 60306030"A員e"8k吋o"j·pj"vjƒk"e栄c"vkpj"d瓜v"u逸p
Eƒe"違pj"ej映r"j衣v"vkpj"d瓜v"u逸p"vt逢噂e"x "ucw"mjk"z穎"n#"Ctiqp"- rncuoc"d茨pi kính
jk吋p"xk"8k羽p"v穎"swfiv"8逢嬰e"vj吋"jk羽p"荏"j·pj"6046 pj壱p"vj医{"o磯w"vkpj"d瓜v"u逸p"vj»"*"AE1)
e„"d隠"o員v"pj印p."j·pj"p„p"jc{"j·pj"vt泳pi"xƒv"8亥w."e„"o瓜v"ej厩"n o"x "p¿o"荏"ik英c" ]35̲0"O磯w"vkpj"d瓜v"dk院p"v pj"e„"jk羽p"v逢嬰pi"eƒe"j衣v"i亥p"pjcw"nk‒p"m院v"n衣k"x噂k"pjcw0" M院v"sw違"p {"ik嘘pi"x噂k"pijk‒p"e泳w"e栄c"vƒe"ik違"Fgg{ck"x "e瓜pi"u詠"*4232+0"Vw{"pjk‒p" vtqpi"m院v"sw違"8«"8逢嬰e"e»pi"d嘘"pj„o"vƒe"ik違"e”p"ejq"dk院v"t茨pi"eƒe"ofir"xk隠p"d‒p"
piq k"e栄c"j衣v"vkpj"d瓜v"u逸p"d鵜"o医v"8k"8瓜"u逸e"pfiv"uq"x噂k"o磯w"mj»pi"z穎"n#"]5;̲0"Ak隠w" p {"mj»pi"zw医v"jk羽pvtqpi"m院v"sw違"pijk‒p"e泳w"e栄c"ej¿pi"v»k0""
Mjk"pijk‒p"e泳w"vt‒p"vkpj"d瓜v"nk‒p"m院v"picpi"d茨pi"rj逢挨pi"rjƒr"j„c"j丑e"vƒe"ik違" Ocvqu"x "Rfitg¦"*4225+"ejq"dk院v"mj»pi"e„"u詠"vjc{"8鰻k"x隠"j·pj"f衣pị"m ej"vj逢噂e"e栄c" vkpj"d瓜v"dk院p"v pj"uq"x噂k"o磯w"8嘘k"ej泳pi"]76]. Tuy nhiên vtqpi"pijk‒p"e泳w"e栄c"vƒe" ik違"Rj衣o"X<p"J́pi"x "Pcqhwok"Oqtkvc"*4227+"vj·"v́{"x q"j„c"ej医v"ej丑p"8吋"v衣q" vkpj"d瓜v"dk院p"v pj"o "ejq"m院v"sw違"mjƒe"pjcw"x噂k"vkpj"d瓜v"cegv{ncvgf"d鵜"違pj"j逢荏pi" vt‒p"vq p"d瓜"d隠"o員v"j衣v"vkpj"d瓜v"vtqpi"mjk"vkpj"d瓜v"rjqurjcvg"d隠"o員v"e„"違pj"j逢荏pi" pj姻"]77]. Hình 4.260"Jk吋p"xk"8k羽p"v穎"swfiv"o磯w"vkpj"d瓜v"u逸p Chú thích : A (AE1) và B (T-10P-8K) B B A A
D違pi"60330"O w"u逸e"e栄c"vkpj"d瓜v"u逸p
O磯w L a b
AE1 48,58±0,43a 0,33±0,05a 0,97±0,02a
T-10P-8K 49±0,07a 0,32±0,05a 1,07±0,05a
Chú thích: L: lightness - 8じ"uƒpi"eてc"o w="c"n "ikƒ"vtお"ejＴ{"vな"o w"8ぎ"*Tgf+"8ｘp" zcpj"*Itggp+="d<"vな"o w"x pi"*[gnnqy+"8ｘp"zcpj"Dnwg0
60306040"A員e"8k吋o"j·pj"vjƒk"e栄c"vkpj"d瓜v"d逸r
J·pj"f衣pi"e栄c"vkpj"d瓜v"d逸r"vj»"*AE2), tkpj"d瓜v"d逸r"ucw"dk院p"v pj"*O-20P-6K)
8逢嬰e"vj吋"jk羽p"vtqpi"j·pj"60490"pj壱p"vj医{"e違"jck"o磯w"vkpj"d瓜v"p {"8隠w"e„"j·pj"8c" fk羽p"jq員e"j·pj"vt”p."vt‒p"d隠"o員v"e„"pj英pi"n厩"ej¤p"n»pi"x "n厩"mko"pj臼 li ti vt‒p"d隠" o員v0"Mj»pi"e„"u詠"vjc{"8鰻k"x隠"j·pj"f衣pi"e栄c"vkpj"d瓜v"ucw"z穎"n#0"Vw{"pjk‒p"d隠"o員v" vkpj"d瓜v"dk院p"vkpj"j挨k"vj»0"M院v"sw違"pijk‒p"e泳w"e栄c"ej¿pi"v»k"ik嘘pi"x噂k"pijk‒p"e泳w" e栄c" Nknnkco" U xqnk" x " e瓜pi" u詠" *422;+" ]6;̲0" Vtqpi" pijk‒p" e泳w" e栄c" vƒe" ik違" Ugwpi"
Hyun Koo và e瓜pi" u詠" *4232+" mjk" u穎" f映pi" j厩p" j嬰r" uqfkwo" vtkogvcrjqurjcvg"
(UVOR+."uqfkwo"vtkrqn{rjqurjcvg"*UVRR+"8吋"v衣q"tc"vkpj"d瓜v"nk‒p"m院v"picpi"vj·"piq k" d隠"o員v"j衣v"vkpj"d瓜v"dk院p"v pj"vj»"j挨p"uq"x噂k"vkpj"d瓜v"v詠"pjk‒p."e”p"zw医v"jk羽p"vhêm
x́pi" 8gp" vt‒p" d隠" o員v" j衣v" ]6:̲0" M院v" sw違" v逢挨pi" v詠" e pi" 8逢嬰e" e»pi" d嘘" d荏k" vƒe" ik違"
Carmona-Garcic"x "e瓜pi"u詠"*422;+"mjk"v衣q"nk‒p"m院v"picpi"vt‒p"vkpj"d瓜v"ejw嘘k"d茨pi" j厩p" j嬰r" UVOR1UVRR" ]76̲0" M院v" sw違" p {" mj»pi" zw医v" jk羽p" vtqpi" pijk‒p" e泳w" e栄c" ej¿pi"v»k0"A吋"ik違k"vj ej"x́pi"8gp"vt‒p"d隠"o員v"j衣v"vkpj"d瓜v"dk院p"vkpj"Ukpij."Mcwt"x " Oe"Ectvj{"*4229+"ejq"t茨pi"fq"u詠 rj¤p"8q衣p"x "j·pj"vj pj"o瓜v"t«ph sâu trong các
j衣v"vkpj"d瓜v"]79].
E pi"vjgq"m院v"sw違"pijk‒p"e泳w"e栄c"ej¿pi"v»k."rj逢挨pi"rjƒr"v衣q"vkpj"d瓜v"d逸r" nk‒p"m院v"picpi"d茨pi"Ctiqp-rncuoc"mj»pi"n o"vjc{"o w"u逸e"e栄c"vkpj"d瓜v"ucw"z穎"n#" *d違pi"6034+0
Hình 4.270"Jk吋p"xk"8k羽p"v穎"swfiv"o磯w"vkpj"d瓜v"d逸r Chú thích: C (AE2) và D (M-20P-6K) D違pi"60340"O w"u逸e"e栄c"vkpj"d瓜v"d逸r O磯w L b AE2 50,25 ± 0,94a 2,27 ± 0,11a M-20P-6K 50,39 ± 0,69a 2,24 ± 0,04a
Chú thích: L: lightness - 8じ"uƒpi"eてc"o w="d<"vな"o w"x pi"*[gnnqy+"8ｘp"zcpj"Dnwg0
C C
6040"O泳e"8瓜"vk‒w"j„c"in vitro x "8員e"8k吋o"j·pj"vjƒk"e栄c"vkpj"d瓜v 604030"O泳e"8瓜"vk‒w"j„c"in vitro
60403030"O泳e"8瓜"vk‒w"j„c"in vitro e栄c"vkpj"d瓜v"u逸p
J o"n逢嬰pi"vkpj"d瓜v"vk‒w"j„c"pjcpj"*TFỰ"vkpj"d瓜v"vk‒w"j„c"ej壱o"*UFƯ"x " vkpj"d瓜v"vt挨"*TƯ"8逢嬰e"vj吋"jk羽p"vtqpi"d違pi"60350"Ej¿pi"v»k"pj壱p"vj医{"vtqpi"e違"jck" vt逢運pi"j嬰r"j欝"j„c"x "mj»pi"j欝"j„c"o磯w"vt逢噂e"mjk"8q"8瓜"vk‒w"j„c"vj·"n逢嬰pi"TFỤ" UFU"8隠w"ik違o"x "TU"v<pi"8ƒpi"m吋"uq"x噂k"o磯w"vkpj"d瓜v"vj»"*AE1).
X噂k"vt逢運pi"j嬰r"o磯w"vkpj"d瓜v"mj»pi"swc"swƒ"vt·pj"j欝"j„c"vt逢噂e"mjk"8q"8瓜"vk‒w"
hóc" n逢嬰pi" TFU" ik違o" v瑛" 6;.76'" *AE1+" 8院p" 48.78'" *T-10P-:M+=" UFU" ik違o" v瑛" 45.26'"*AE1+"8院p"34.68'"*T-10P-8K). Tw{"pjk‒p"TU"v<pi"v瑛"49.64'"*AE1) 8院p"
60,98% (T-10P-:M+0"M院v"sw違"p {"ejq"vj医{"e„"u詠"ejw{吋p"f鵜ej"vj pj"rj亥p"TFỤ"UFU" vtqpi" vkpj" d瓜v" vj pj" f衣pi" vkpj" d瓜v" vt挨" TU" ucw swƒ" vt·pj" dk院p" v pj" d茨pi"
Argon- plasmạ
Vt逢運pi"j嬰r"o磯w"vkpj"d瓜v"8«"swc"swƒ"vt·pj"j欝"j„c"vt逢噂e"mjk"zƒe"8鵜pj"o泳e"8瓜"
tiêu hóa, RFU"ik違o"44.89'"mjk"uq"uƒpj"ik英c"o磯w"V-10P-:M"x噂k"o磯w"vkpj"d瓜v"vj»" *AE1+." UFU" ik違o" 44.5'" x " TU" v<pi" 66.:'" mjk" uq" uƒpj" ik英c" o磯w" V-10P-:M" x噂k" o磯w"vkpj"d瓜v"vj»"*AE1+0"E pi"ik嘘pi"pj逢"vt逢運pi"j嬰r"o磯w"ej逢c"swc"swƒ"vt·pj"j欝"j„c." mjk"uq"uƒpj"x噂k"o磯w"8嘘k"ej泳pi"ej¿pi"v»k"pj壱p"vj医{"v益"n羽"TFỤ"UFU"ik違o"pj逢pi"TU" v<pi0"D‒p"e衣pj"8„"TU"ik違o"mjk"o磯w"8«"swc"j欝"j„c"vtqpi"mjk"v益"n羽"TFU"x "UFU"e„" zw"j逢噂pi"v<pi"n‒p0"E映"vj吋"TU"ik違o":.95'."UFU"x "TFU"v<pi"n亥p"n逢嬰v"2.78'"x " :.39'"ik英c"o磯w"vkpj"d瓜v"8«"swc"j欝"j„c"x "o磯w"vkpj"d瓜v"mj»pi"swc"j欝"j„c"32"rj¿v0" Pj逢"x壱{"e„"u詠"f鵜ej"ejw{吋p"v瑛"TU"ucpi"TFU"x "UFU0"M院v"sw違"vjw"8逢嬰e"vtqpi"vj " pijk羽o"e栄c"ej¿pi"v»k"ik嘘pi"pj逢"m院v"nw壱p"e栄c"Lwtcnwem"Lwcpucpi"x "e瓜pi"u詠"*4234+" [58̲0"Vjgq"pj„o"vƒe"ik違"p {"j o"n逢嬰pi"TU"vtqpi"vkpj"d瓜v"nk‒p"m院v"picpi"ik違o"f亥p" vtqpi"mjk"j o"n逢嬰pi"UFU"v<pi"f亥p"vjgq"vj運k"ikcp"j欝"j„c0"
D違pi"60350""O嘘k"v逢挨pi"swcp"ik英c"j o"n逢嬰pi RDS, SDS và RS và o泳e"8瓜"nk‒p" m院v"picpi"e栄c"vkpj"d瓜v"u逸p Pijk羽o"vj泳e RDS (%) SDS (%) RS (%) AE1 49,54 ± 0,31a 23,04 ± 0,69a 27,42 ± 0,39a T-20P-6K 40,18 ± 1,02b 16,96 ± 0,28b 42,87 ± 1,16b T-20P-8K 36,34 ± 1,18c 16,52 ± 0,08c 47,13 ± 1,26c A T-10P-6K 32,81 ± 1,16d 15,4 ± 0,92d 51,79 ± 1,08d T-10P-8K 26,56 ± 0,24e 12,46 ± 0,68e 60,98 ± 0,49e AE1 57,4 ± 0,13a 35,15 ± 0,3a 7,45 ± 0,02a T-20P-6K 48,28 ± 0,17b 22,5 ± 0,53b 29,22± 0,37b B T-20P-8K 45,05 ± 0,33c 19,55 ± 0,28c 35,41 ± 0,12c T-10P-6K 38,87 ± 0,35d 13,77 ± 0,03d 41,85 ± 0,46d T-10P-8K 34,73 ± 0,26e 13,02 ± 0,21e 52,25 ± 0,21e Eƒe"ikƒ"vtお"vtqpi"dＶpi"dkあw"vjお"ikƒ"vtお"vtwpi"d·pj"ł"8じ"nうej"ejwｂp"*p?5+ Eƒe"ikƒ"vtお"e„"m#"jkうw"mjƒe"pjcw"dkあw"vjお"uば"mjƒe"dkうv"*r>2027+ C"vkpj"dじv"ej⇔c"swc"jげ"j„c D"vkpj"dじv"8«"swc"jげ"j„c
Dk吋w"8欝"6050"O嘘k"v逢挨pi"swcp"ik英c"o泳e"8瓜"nk‒p"m院v"picpi"x "TU"*'+"vtqpi"vkpj" d瓜v"u逸p
60404040"O泳e"8瓜"vk‒w"j„c"in vitro e栄c"vkpj"d瓜v"d逸r
Vkpj"d瓜v"vk‒w"j„c"pjcpj"*TFỰ"vkpj"d瓜v"vk‒w"j„c"ej壱o"*UFƯ"x "vkpj"d瓜v"vt挨" *TƯ" 8逢嬰e" vj吋" jk羽p" vtqpi" d違pi" 60360" Vtqpi" 8„." ej¿pi" v»k" pj壱p" vj医{" vtqpi" e違" jck" vt逢運pi"j嬰r"j欝"j„c"x "mj»pi"j欝"j„c"o磯w"vt逢噂e"mjk"8q 8瓜"vk‒w"j„c"vj·"n逢嬰pi"TFỤ" UFU"8隠w"ik違o"x "TU"v<pi"8ƒpi"m吋"uq"x噂k"o磯w"vkpj"d瓜v"vj»"*AE2).
X噂k"vt逢運pi"j嬰r"o磯w"vkpj"d瓜v"mj»pi"swc"swƒ"vt·pj"j欝"j„c"vt逢噂e"mjk"8q"8瓜"vk‒w" j„c" n逢嬰pi" TFU" ik違o" v瑛" 76.;5'" *AE2+" 8院p" 55.4:'" *" O-20P-8M+=" UFU" ik違o" v瑛" 44.46'"*AE2+"8院p"9,99% ( M-20P-8M+0"Vw{"pjk‒p"TU"v<pi"v瑛"44.43'"*AE2+"8院p"
58,96% (M-20P-8M+0" M院v" sw違" p {" ejq" vj医{" e„" u詠" ejw{吋p" f鵜ej" vj pj" rj亥p" TFỤ" UFU" vtqpi" vkpj" d瓜v" vj pj" f衣pi" vkpj" d瓜v" vt挨" TU" ucw" swƒ" vt·pj" dk院p" v pj" d茨pi"
Argon- plasmạ
Vt逢運pi"j嬰r"o磯w"vkpj"d瓜v"8«"swc"swƒ"vt·pj"j欝"j„c"vt逢噂e"mjk"zƒe"8鵜pj"o泳e"8瓜" vk‒w"j„c."TFU"ik違o"46.45'"mjk"uq"uƒpj"ik英c"o磯w"O-20P-8M"x噂k"o磯w"vkpj"d瓜v"vj»" *AE2+."UFU"ik違o"36.57'"x "TU"v<pi"5:.8'"mjk"uq"uƒpj"ik英c"o磯w"O-20P-8M"x噂k" o磯w"vkpj"d瓜v"vj»"*AE2+0"E pi"ik嘘pi"pj逢"vt逢運pi"j嬰r"o磯w"ej逢c"swc"swƒvt·pj"j欝"j„c." mjk"uq"uƒpj"x噂k"o磯w"8嘘k"ej泳pi"ej¿pi"v»k"pj壱p"vj医{"v益"n羽"TFỤ"UFU"ik違o"pj逢pi"TU"
v<pi0"D‒p"e衣pj"8„"TU"ik違o"mjk"o磯w"8«"swc"j欝"j„c"vtqpi"mjk"v益"n羽"TFU"e„"zw"j逢噂pi" v<pi"n‒p0"E映"vj吋"TU"ik違o";.:;'."TFU"v<pi"4.7:'"Ik英c"o磯w"vkpj"d瓜v"8«"swc"j欝"j„c"
và o磯w"vkpj"d瓜v"mj»pi"swc"j欝"j„c"32"rj¿v0"Pj逢"x壱{"e„"u詠"f鵜ej"ejw{吋p"v瑛"TU"ucpi"
RDS.
M院v" sw違" vjw" 8逢嬰e" ik嘘pi" x噂k" pijk‒p" e泳w" e栄c" Ugwpi" J{wp" Mqq" x " e瓜pi" u詠" *4232+"]9̲"vt‒p"vkpj"d瓜v"d逸r"vjgq"o泳e"8瓜"v<pi"f亥p"e栄c"nk‒p"m院v"picpi"vj·"eƒe"ikƒ"vt鵜" TFỤ" UFU" ik違o" e”p" TU" v<pi0" E映" vj吋" x噂k" o磯w" 8嘘k" ej泳pi" vƒe" ik違" vjw" 8逢嬰e" j o" n逢嬰pi"TU"n "7.7'"x "o磯w"e„"o泳e"8瓜"nk‒p"m院v"picpi";3.3'"n "7:.7:'0"E”p"j o" n逢嬰pi"UFU"ik違o"v瑛"58.68'"荏"o磯w"8嘘k"ej泳pi"zw嘘pi"e”p"34.4;'"荏"o磯w"e„"nk‒p"m院v" picpi";3.3'0"TFU"ik違o"v瑛"7:.27'"荏"o磯w"8嘘k"ej泳pi"zw嘘pi"e”p"4:.85'0"U詠"mjƒe" pjcw"x隠"j o"n逢嬰pi"eƒe"nq衣k"vkpj"d瓜v"vjw"8逢嬰e"e„"vj吋"fq"j o"n逢嬰pi"co{nqug."fk羽p" v ej"d隠" o員v"j衣v" x "e医w"vt¿e"vkpj"vj吋"e栄c"vkpj"d瓜v"違pj"j逢荏pi"8院p"u詠"v医p"e»pi"e栄c" gp¦{og"vtqpi"swƒ"vt·pj"vj栄{"rj¤p"e栄c"vkpj"d瓜v0"
Vt逢運pi"j嬰r"vkpj"d瓜v"swc"swƒ"vt·pj"j欝"j„c"j o"n逢嬰pi"vkpj"d瓜v"TU"ik違o"j挨p"uq" x噂k"vt逢運pi"j嬰r"mj»pi"e„"j欝"j„c"vw{"pjk‒p"o磯w"e„"nk‒p"m院v"picpi"x磯p"ecq"j挨p"uq"x噂k" o磯w" 8嘘k" ej泳pi0" m院v" sw違" p {" v逢挨pi" v詠" pj逢" pijk‒p" e泳w" e栄c" Lwtcnwem" Lwcpucpi" x " e瓜pi"u詠"*4234+"]78̲0"Pijk‒p"e泳w"e栄c"Ejwpi"x "e瓜pi"u詠"*422:+"n衣k"pj壱p"vj医{"t茨pi" j o"n逢嬰pi"e栄c"TU"vtqpi"vkpj"d瓜v""d逸r"8«"swc"swƒ"vt·pj"j欝"j„c"n "9.2'"vtqpi"vkpj"d瓜v" nk‒p"m院v"picpi"vtqpi"mjk"vkpj"d瓜v"8嘘k"ej泳pi"n "9.5'0"TFU";5.2'"vtqpi"mjk"vkpj"d瓜v"" 8嘘k"ej泳pi"n ";4.9'"]69].
Pj逢"x壱{"pijk‒p"e泳w"x隠"8瓜"vk‒w"j„c"in vitro e栄c"vkpj"d瓜v"nk‒p"m院v"picpi"8«"e„" pj英pi"m院v"sw違"vtƒk"pi逢嬰e"pjcw0"Ak隠w"p {"vjgq"vƒe"ik違"Ejwpi"x "e瓜pi"u詠"*422:+"ik違k" vj ej"n "fq"u詠"mjƒe"dk羽v"vtqpi"nq衣k"vkpj"d瓜v."rj逢挨pi"rjƒr"v衣q"vkpj"d瓜v"nk‒p"m院v"picpi" e pi"pj逢"o泳e"8瓜"nk‒p"m院v"picpi"vtqpi"vkpj"d瓜v"]67].
D違pi"60360"O嘘k"v逢挨pi"swcp"ik英c"j o"n逢嬰pi RDS, SDS và RS và o泳e"8瓜"nk‒p" m院v"picpi"e栄c"vkpj"d瓜v"d逸r Pijk羽o"vj泳e RDS (%) SDS (%) RS (%) AE2 54,93 ± 0,24a 22,24 ± 0,22a 22,21 ± 0,02a M-10P-5K 49,35 ± 0,23b 19,08 ± 0,32b 34,2 ± 0,10b A M-10P-6K 47,83 ± 0,16c 15,4 ± 0,36c 46,14 ± 0,46c M-20P-5K 44,35 ± 0,04d 10,66 ± 0,19d 52,92 ± 0,26d M-20P-6K 33,28 ± 0,34e 7,99 ± 0,42e 58,96 ± 0,24e AE2 60,09 ± 0,37a 29,43 ± 0,74a 10,47 ± 0,57a M-10P-5K 54,66 ± 0,13b 23,74 ± 0,35b 21,61 ± 0,43b B M-10P-6K 45,95 ± 0,02c 19,58 ± 0,31c 34,48 ± 0,34c M-20P-5K 41,26 ± 0,12d 17,62 ± 0,05d 41,12 ± 0,17d M-20P-6K 35,86 ± 0,32e 15,08 ± 0,76e 49,07 ± 0,48e Eƒe"ikƒ"vtお"vtqpi"dＶpi"dkあw"vjお"ikƒ"vtお"vtwpi"d·pj"ł"8じ"nうej"ejwｂp"*p?5+ Eƒe"ikƒ"vtお"e„"m#"jkうw"mjƒe"pjcw"dkあw"vjお"uば"mjƒe"dkうv"*r>2027+ C"vkpj"dじv"ej⇔c"swc"jげ"j„c D"vkpj"dじv"8«"swc"jげ"j„c
Dk吋w"8欝"6060"O嘘k"v逢挨pi"swcp"ik英c"o泳e"8瓜"nk‒p"m院v"picpi"x "TU"*'+"vtqpi"vkpj" d瓜v"d逸r
604040"A員e"8k吋o"j·pj"vjƒk"j衣v"vkpj"d瓜v"ucw"mjk"fq"gp¦{og"vk‒w"j„c"v医p"e»pi
4.2.2030"Vkpj"d瓜v"u逸p
Hình 4.28 n "m院v"sw違"ucw"mjk"ej映r"jk吋p"xk"8k羽p"v穎"swfiv"vt‒p"vkpj"d瓜v"u逸p"vj»"