tools for inventing organizations toward a handbook of organizational processes

... Ethical Journalism A Handbook of Values and Practices for the News and Editorial Departments “ Reporters, editors, photographers and all members of the news staff of The New York Times share a common ... personal gain any nonpublic information acquired at work, or use his or her association with The Times to gain favor or advantage And second, no one may anything that damages The Times’s reputation ... axiomatic standards of behavior governing our dealing with colleagues and going about our work The Rules are available from the office of the associate managing editor for news administration Together...

Ngày tải lên: 06/03/2014, 11:20

... Dulay and Marina K Burt 1975 Natural sequences in child second language acquisition Language Learning, 24(1) Susan Gass 1979 Language transfer and universal grammatical relations Language Learning, ... performance of our parser and mal-ruleaugmented grammar and the unique challenges “She is teach piano on Tuesdays.” Beginner: Inappropriate use of auxiliary and verb morphology problems “She teaches ... hearing peers, and yet the population represents a broad range of ability Among deaf 18year-olds, about half read at or below a fourth grade level, while about 10% read above the eighth-grade...

Ngày tải lên: 17/03/2014, 07:20

Ngày tải lên: 05/10/2012, 09:53

Ngày tải lên: 18/03/2013, 01:45

... containing different concentrations of the analyte are prepared to construct each external calibration curve, consisting of the concentration of an alkyl nitrite on the horizontal axis and peak area ... in rats J Pharm Sci 74:780–782 10) Kielbasa WB, Bauer JA, Fung HL (1999) Analysis of isobutyl nitrite inhalant in rat and human blood: application for pharmacokinetic investigations J Chromatogr ... Terumo, Tokyo, Japan and other manufacturers) and rapidly injected into GC iv Quantitation: a 0.25 mL of the same matrix e (without an analyte), 0.5 mL of the phosphate buffer, 0.05 mL of isobutyl...

Ngày tải lên: 18/10/2013, 00:15

... GC/MS analysis for DAEMS in serum (a) a total ion chromatogram (TIC) and a mass chromatogram; (b) an EI mass spectrum of DAEMS; (c) a CI mass spectrum of DAEMS Poisoning case, and toxic and fatal ... construct a calibration curve for DAEMS consisting of peak area ratio of DAEMS to IS on the vertical axis and DAEMS concentration on the horizontal axis A peak area ratio obtained from a test specimen ... EMPA in serum (a) a TIC and mass chromatograms; (b) an EI mass spectrum of the t-BDMS derivative of EMPA; (c) a CI mass spectrum of the same derivative of EMPA data of animals According to the...

Ngày tải lên: 18/10/2013, 00:15

... 188 Cannabinoids and their metabolites GC analysis of cannabinoids in plant specimensa Reagents and their preparation • • • Extraction and purification of cannabinoids [3]: Cannabis sativa L is ... 25:321–326 6) Matsunaga T, Nagatomo H, Narimatsu S et al (1993) Studies on identification of cannabis seeds I: Qualitative and quantitative analysis of cannabinoids in cannabis seeds Jpn J Forensic ... with cannabinoid concentration on the horizontal axis and with peak area ratio of a cannabinoid to IS on the vertical axis GC analysis of cannabinoids in plant specimens ⊡ Figure 2.2 Gas chromatogram...

Ngày tải lên: 24/10/2013, 19:15

... methods Qualitative analysis is performed by finding a peak appearing at the same retention time as that of the authentic standard after trimethylsilyl (TMS) derivatization; it is also important to ... Reagents and their preparation • • Standard solutions of morphine for a calibration curve (2, and 20 µg/mL): see “Reagents and their preparation”, above of GC and GC/MS analysis section 0.5 M Ammonium ... retention time of a peak of a specimen with that of the authentic standard and also by the confirmation of the absence of such a peak in a blank specimen An HPLC chromatogram for the authentic compounds...

Ngày tải lên: 24/10/2013, 19:15

... cyanosis headache, dyspnea, tachypnea, tachycardia and hypertension mental derangement, listlessness and metabolic acidosis coma, convulsive attack and hypotension death A poisoning case [4] An ... of the oxidation of nitrite into nitrate and the same extractions as those for nitrate A calibration curve for nitrite using blank specimens and IS is also prepared for quantitation in the same ... construct a calibration curve The peak area ratio of nitrate to IS obtained from a test specimen is applied to the calibration curve to calculate its concentration ii Analysis of nitrite i A 0.2-mL...

Ngày tải lên: 24/10/2013, 19:15

... alminoprofen 325, 330, 332 alprazolam 284, 285, 290 alternative specimens Amanita neoovoidea 480 Amanita pantherina 469 Amanita phalloides 469 Amanita verna 469, 474 Amanita virosa 469, 473 amanitin ... aconitum alkaloids 455 acylation 30 adhesives 149 adulterant 491 advanced automated sample processors 31 AED 81 A- esterase 535 air bags 629 alachlor 529 alcohol 135 alcohol dehydrogenase 123 ALD-type ... 137 aldehyde dehydrogenase 123, 137 aldicarb 566 aldrin 529 alkylated adducts 85 alkylated DNAs 85 alkylation 30 alkyl nitrites 153, 655 allobarbital 305, 308 allylesterase 624 allyxycarb 566 alminoprofen...

Ngày tải lên: 24/10/2013, 19:15

... ng/mL for the secondary judgement by GC/MS However, in Japan, such criteria set by official institutions are not available for drugs of abuse Upon judgements of analytical data, the idea of cutoff ... The author et al experienced a fatal cocaine poisoning case and measured concentrations of cocaine and its metabolites in body fluids and various organs A 41-year-old male was found dead in a hotel ... composed of a mixture of non-polar phase and a cation exchanger phase; the mechanisms are reversed-phase extraction plus cation-exchanging action The LRC reservoir is advantageous, because as much as...

Ngày tải lên: 29/10/2013, 01:15

... about A 10-mL volume of ethanol and 10 mL distilled water are passed through a Sep-Pak C18 cartridge using a 10-mL volume glass syringe to activate the cartridge at a flow rate not faster than ... concentrations of pentazocine should be not smaller than for the calibration curve, which is composed of pen- Pentazocine tazocine concentration in the horizontal axis and peak area ratio of pentazocine ... vertical axis The peak area ratio of a test specimen is applied to the calibration curve to obtain its pentazocine concentration Assessment of the method > Table 5.1 shows EI mass spectra of pentazocine...

Ngày tải lên: 29/10/2013, 02:15

... ion appears as the base peak Fragment peaks can be observed at m/z 221, 207, 181 and 167 The fragmentation pathways are shown in > Fig 6.2 The confirmation of LSD should be made with each mass ... amount of chloroform four times The combined chloroform extract is evaporated to dryness; the residue is dissolved in a small amount of methanol to be subjected to further analysis TLC analysis Analytical ... Standard Methods of Chemical Analysis in Poisoning – With Commentary – Nanzando, Tokyo, p 43 and p 151 (in Japanese) 3) Cody JT (2000) Hallucinogens In: Bogusz MJ (ed) Handbook of Analytical...

Ngày tải lên: 08/11/2013, 01:15

... Nakajima K, Nishikawa M et al (1991) Determination of methamphetamine and amphetamine in urine by headspace gas chromatography/mass spectrometry Anal Sci 7:19–22 25) Shima N, Kamata T, Nishikawa ... hyperthermia, rhabdomyolysis, acute renal failure, disseminated intravascular coagulation and death [19, 20] A detailed review by Kalant [16] revealed that 87 MDAs-related fatalities were associated ... generally performed for urine specimens In this chapter, the procedures for GC/MS and LC/MS analyses of MDAs in the forms of tablets and those for GC/MS analysis of MDAs and their main metabolites...

Ngày tải lên: 08/11/2013, 01:15

... mL of chloroform/methanol (9:1) into a glass vial v A small amount of upper aqueous layer is carefully removed by aspiration with a Pasteur pipette The organic layer (chloroform) is evaporated ... headspace solid-phase microextraction (SPME) Chromatographia 43:331–333 14) Nakahara Y, Takahashi K, Sakamoto T et al (1997) Hair analysis for drugs of abuse X VII Simultaneous detection of PCP, ... Lee LF, Halzhauer LB et al (2001) Analysis of urine samples in cases of alleged sexual assault: case history In: Salamore SJ (ed) Benzodiazepines and GHB: Detection and Pharmacology Humana Press,...

Ngày tải lên: 08/11/2013, 01:15

Ngày tải lên: 12/12/2013, 20:53

... Louis, MO, USA) Pure powder of perazine and clospirazine was donated by Mitsubishi Welpharma, Osaka, Japan; that of flupentixol by Takeda Chem Ind Ltd., Osaka, Japan; that of thioproperazine by Shionogi ... obtained For quantitation with mass chromatograms (MCs), a fixed amount of IS and various concentrations of a target compound are added to mL each of blank whole blood or urine, and processed as ... GC/MS At least vials containing various concentrations of a target compound are prepared for a calibration curve Assessment of the method All eleven kinds of phenothiazine drugs gave the base peaks...

Ngày tải lên: 15/12/2013, 12:15

... to draw a calibration curve A peak area ratio of a test specimen is applied to the calibration curve to calculate its concentration Assessment of the method The butyrophenone drugs analyzable ... cases, and toxic and fatal concentrations Notes a) When GC/MS, HPLC and LC/MS are compared for analysis of haloperidol and bromperidol, the LC/MS seems of the best choice for their trace analysis ... Van Medical, Tokyo, p 56 (in Japanese) 19) Uges DRA (1997) Blood level data In: Brandenberger H, Maes RAA (eds) Analytical Toxicology for Clinical, Forensic and Pharmaceutical Chemists Walter de...

Ngày tải lên: 15/12/2013, 12:15

... (in Japanese) 3) Tanaka E, Terada M, Nakamura T et al (1997) Forensic analysis of eleven cyclic antidepressants in human biological samples using a new reversed-phase chromatographic column of ... pupil diameter, mm; light reaction, prompt; heart rate, 100/min with the sinus rhythm Although gastric lavage and administration of a purgative and activated charcoal were performed after admission, ... time of a test peak with that of an authentic compound Although an analytical case using TSK gel Super-Octyl Poisoning cases, and toxic and fatal concentrations (particle diameter µm) was reported...

Ngày tải lên: 15/12/2013, 12:15

... Mass chromatograms of triazolam, 4-hydroxytriazolam, α-hydroxytriazolam and alprazolam (IS) A 100-ng aliquot each of triazolam, 4-hydroxytriazolam and α-hydroxytriazolam and 50 ng of alprazolam ... 299 328 325 313 342 bromazepam prazepam 10.01 10.10 315 324 nimetazepam mexazolam flurazepam nitrazepam clonazepam estazolam alprazolam tofisopam etizolam triazolam brotizolam 10.30 10.75 10.83 ... bromazepam, 11: prazepam, 12: nimetazepam, 13: mexazolam, 14: flurazepam, 15: nitrazepam, 16: clonazepam, 17: estazolam, 18: alprazolam, 19: tofisopam, 20: etizolam, 21: triazolam, 22: brotizolam...

Ngày tải lên: 15/12/2013, 12:15