... particularly effective in the analysis of organic pollutants. 24.7. ANALYSIS OF WATER SAMPLES The preceding sections of this chapter have covered the major kinds of analysis techniques that are ... LLC 24 CHEMICAL ANALYSIS OF WATER AND WASTEWATER __________________________ __________________________ 24.1. GENERAL ASPECTS OF ENVIRONMENTAL CHEMICAL ANALYSIS Scientists’ understanding of the ... know- ledge of the identities and quantities of pollutants and other chemical species in water, air, soil, and biological systems. Therefore, proven, state -of- the-art techniques of chemical analysis, ...
Ngày tải lên: 23/07/2013, 20:57
... quality control program. The minimum requirements of this program consist of an initial demonstration of laboratory capability and an ongoing analysis of spiked samples to evaluate and document data ... for the required analysis of a QC check standard will depend upon the number of parameters being simultaneously tested, the complexity of the sample matrix, and the performance of the laboratory. ... Pesticide Residue Analysis; Some Practical Aspects,” Journal of the Association of Official Analytical Chemists, 48, 1037 (1965). 11. Cole, T., Riggin, R., and Glaser, J. “Evaluation of Method Detection...
Ngày tải lên: 14/02/2014, 03:20
Tài liệu METHODS FOR ORGANIC CHEMICAL ANALYSIS OF MUNICIPAL AND INDUSTRIAL WASTEWATER doc
... quality control program. The minimum requirements of this program consist of an initial demonstration of laboratory capability and an ongoing analysis of spiked samples to evaluate and document data ... for the required analysis of a QC check standard will depend upon the number of parameters being simultaneously tested, the complexity of the sample matrix, and the performance of the laboratory. 8.4.1 ... dilution standard be prepared at a concentration of 15 µg/mL of each internal standard compound. The addition of 10 µL of this standard to 5.0 mL of sample or calibration standard would be equivalent...
Ngày tải lên: 14/02/2014, 03:20
APPENDIX A TO PART 136 METHODS FOR ORGANIC CHEMICAL ANALYSIS OF MUNICIPAL AND INDUSTRIAL WASTEWATER pot
... 15-40% of Mass 95. 75 30-60% of Mass 95. 95 Base Peak, 100% Relative Abundance. 96 5-9% of Mass 95. 173 <2% of Mass 174. 174 >50% of Mass 95. 175 5-9% of Mass 174. 176 >95% but 101% of Mass ... for the required analysis of a QC check standard will depend upon the number of parameters being simultaneously tested, the complexity of the sample matrix, and the performance of the laboratory. ... the base of the water column. The purging device illustrated in Figure 1 meets these design criteria. solution of 5 mL of sample or standard is equivalent to a concentration of 30 µg/L of each...
Ngày tải lên: 05/03/2014, 21:20
APPENDIX A TO PART 136 METHODS FOR ORGANIC CHEMICAL ANALYSIS OF MUNICIPAL AND INDUSTRIAL WASTEWATER: METHOD 604—PHENOLS docx
... for the required analysis of a QC check standard will depend upon the number of parameters being simultaneously tested, the complexity of the sample matrix, and the performance of the laboratory. 6. ... quality control program. The minimum requirements of this program consist of an initial demonstration of laboratory capability and an ongoing analysis of spiked samples to evaluate and document data ... example of the separations achieved by this column is shown in Figure 2. 12.9 Calibrate the system daily with a minimum of three aliquots of calibration standards, containing each of the phenols of...
Ngày tải lên: 05/03/2014, 21:20
CHEMICAL ANALYSIS OF ANTIBIOTIC RESIDUES IN FOOD pptx
... Natural Occurrence of CAP, 235 7.4.4 Analysis of CAP in Herbs and Grass (Feed) Using LC-MS, 236 7.4.5 Conclusions, 236 7.5 Nitrofurans, 236 7.5.1 Background, 236 7.5.2 Analysis of Nitrofurans, 236 7.5.3 ... Background, 227 7.2.2 Analysis, 229 7.2.3 Conclusions, 230 7.3 Ceftiofur and Desfuroylceftiofur, 230 7.3.1 Background, 230 7.3.2 Analysis Using Deconjugation, 231 7.3.3 Analysis of Individual Metabolites, ... area of environmental issues related to veterinary use of antimicrobials. For the bench analyst, it provides not only information on sources of methods of analysis but also an understanding of...
Ngày tải lên: 11/03/2014, 03:20
APPENDIX A TO PART 136 METHODS FOR ORGANIC CHEMICAL ANALYSIS OF MUNICIPAL AND INDUSTRIAL WASTEWATER: METHOD 605—BENZIDINES pdf
... for the required analysis of a QC check standard will depend upon the number of parameters being simultaneously tested, the complexity of the sample matrix, and the performance of the laboratory. 8.4.1 ... identifications should be based upon measurements of actual retention time variations of standards over the course of a day. Three times the standard deviation of a retention time for a compound can be ... collection of a minimum of 250 mL of sample. Sample containers must be kept refrigerated at 4°C and protected from light during compositing. If the sampler uses a peristaltic pump, a minimum length of compressible...
Ngày tải lên: 14/03/2014, 20:20
APPENDIX A TO PART 136 METHODS FOR ORGANIC CHEMICAL ANALYSIS OF MUNICIPAL AND INDUSTRIAL WASTEWATER: METHOD 611—HALOETHERS potx
... containing a concentration of C, in µg/L. Equation 2 where: A = Amount of material injected (ng). V = Volume of extract injected (µL). i V = Volume of total extract (µL). t V = Volume of water extracted ... for the required analysis of a QC check standard will depend upon the number of parameters being simultaneously tested, the complexity of the sample matrix, and the performance of the laboratory. 8.4.1 ... 136 METHODS FOR ORGANIC CHEMICAL ANALYSIS OF MUNICIPAL AND INDUSTRIAL WASTEWATER METHOD 611—HALOETHERS 1. Scope and Application 1.1 This method covers the determination of certain haloethers....
Ngày tải lên: 14/03/2014, 20:20
Mechanics and Analysis of Composite Materials ppt
... (they are not monolithic and consist of thin fibrils). MECHANICS AND ANALYSIS OF COMPOSITE MATERIALS 30 Tzx- Merhanics and analysis of composite materials 7 ZY Fig. 2.1. A solid ... for analysis of composite materials. Chapter 3 is devoted to the basic structural element of a composite material - unidirectional composite ply. In addition to traditional description of ... special class of man-made materials utilizing natural potentials of material strength and structure. Chapter 4 contains a description of typical composite layers made of unidirec- tional,...
Ngày tải lên: 22/03/2014, 12:20
APPENDIX A TO PART 136 METHODS FOR ORGANIC CHEMICAL ANALYSIS OF MUNICIPAL AND INDUSTRIAL WASTEWATER: METHOD 607—NITROSAMINES docx
... quality control program. The minimum requirements of this program consist of an initial demonstration of laboratory capability and an ongoing analysis of spiked samples to evaluate and document data ... the method. When results of sample spikes References 1. Fine, D.H., Lieb, D., and Rufeh, R. “Principle of Operation of the Thermal Energy Analyzer for the Trace Analysis of Volatile and Non-Volatile ... for the required analysis of a QC check standard will depend upon the number of parameters being simultaneously tested, the complexity of the sample matrix, and the performance of the laboratory. 8.4.1...
Ngày tải lên: 22/03/2014, 14:20
METHODS FOR ORGANIC CHEMICAL ANALYSIS OF MUNICIPAL AND INDUSTRIAL WASTEWATER doc
... characteristic masses of each parameter of interest must maximize in the same or within one scan of each other. 14.1.2 The retention time must fall within ±30 seconds of the retention time of the authentic ... FOR ORGANIC CHEMICAL ANALYSIS OF MUNICIPAL AND INDUSTRIAL WASTEWATER METHOD 625—BASE/NEUTRALS AND ACIDS 1. Scope and Application 1.1 This method covers the determination of a number of organic ... elevated baselines in the total ion current profiles. All of these materials must be routinely demonstrated to be free from interferences under the conditions of the analysis by running laboratory reagent...
Ngày tải lên: 28/03/2014, 19:20
APPENDIX A TO PART 136 METHODS FOR ORGANIC CHEMICAL ANALYSIS OF MUNICIPAL AND INDUSTRIAL WASTEWATER ppt
... method of determining cleanliness of work surfaces and tools is to wipe the surface with a piece of filter paper. Extraction and analysis by gas chromatography can achieve a limit of sensitivity of ... only that volume of spiking solution should be added to the sample so that the final extract will contain 25 ng/mL of internal standard at the time of analysis. 10.3 Add 60 mL of methylene chloride ... listed, depending upon the nature of interferences in the sample matrix. 1.4 Because of the extreme toxicity of this compound, the analyst must prevent exposure to himself, of to others, by materials knows or...
Ngày tải lên: 28/03/2014, 20:20
Multivariate Analysis of Ecological Data ppt
... issues • Users of the ordination methods too often ignore third and higher ordination axes. While these ordination axes are often not interpretable and, in the case of a direct gradient analysis, ... test of the H 0 : there is no effect of environmental variables on species composition, i.e. the effect of both variables is zero. The rejection of the null hypothesis means that at least one of ... variance of species data : 5.2 27.4 41.9 53.2 of species-environment relation: 100.0 .0 .0 .0 Sum of all unconstrained eigenvalues .904 Sum of all canonical eigenvalues .047 The dose explains 4.7% of...
Ngày tải lên: 29/03/2014, 17:20
Thermal Analysis of Polymeric Materials pptx
... 349 Finger printing of materials 350 Quantitative analysis of the glass transition 354 Quantitative analysis of the heat of fusion 355 4.4 Temperature-modulated Calorimetry 4.4.1 Principles of Temperature-modulated ... theoretical basis of the experimental results of “Thermal Analysis of Polymeric Materials. ” The book contains, as shown above, a critically selected, limited series of topics. The field of flexible ... to some degree because developments of convenient methods of measurement have been slow and teaching of the understanding of the basics of thermal analysis is often wanting. Flexible, linear macromolecules,...
Ngày tải lên: 27/06/2014, 15:20
Mechanics and Analysis of Composite Materials Valery V, Vasiliev & Evgeny pptx
... MECHANICS AND ANALYSIS OF COMPOSITE MATERIALS Valery V. Vasiliev Professor of Aerospace Composite Structures Director of School of Mechanics and Design Russian State University of Technology, ... first of all, to mechanics of composite materials which is discussed in this book in conjunction with analysis of composite materials. As we hope, thus constructed combination of materials ... mechanics of composite materials, design, analysis, fabrication, and application of composite structures. According to the list of books on composites presented in Mechanics of Fibrous...
Ngày tải lên: 27/06/2014, 18:20
Designation: C 25 – 99 - Chemical Analysis of Limestone, Quicklime, and Hydrated Lime1 pptx
Ngày tải lên: 10/07/2014, 23:20
Designation: C 114 – 00 - Chemical Analysis of Hydraulic Cement1 pot
Ngày tải lên: 10/07/2014, 23:20
Designation: C 471M – 96 METRIC - Chemical Analysis of Gypsum and Gypsum Products [Metric]1 ppsx
Ngày tải lên: 10/07/2014, 23:20
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