BSI Standards Publication BS EN 2833 005 2013 Aerospace series — Glass fibre thermosetting preimpregnates — Technical specification Part 005 Glass fabric/phenolic resin preimpregnate BS EN 2833 005 20[.]
BS EN 2833-005:2013 BSI Standards Publication Aerospace series — Glass fibre thermosetting preimpregnates — Technical specification Part 005: Glass fabric/phenolic resin preimpregnate BS EN 2833-005:2013 BRITISH STANDARD National foreword This British Standard is the UK implementation of EN 2833-005:2013 The UK participation in its preparation was entrusted to Technical Committee ACE/65, Non-metallic materials for aerospace purposes A list of organizations represented on this committee can be obtained on request to its secretary This publication does not purport to include all the necessary provisions of a contract Users are responsible for its correct application © The British Standards Institution 2013 Published by BSI Standards Limited 2013 ISBN 978 580 81716 ICS 49.025.40 Compliance with a British Standard cannot confer immunity from legal obligations This British Standard was published under the authority of the Standards Policy and Strategy Committee on 31 August 2013 Amendments issued since publication affected Date TextText affected BS EN 2833-005:2013 EN 2833-005 EUROPEAN STANDARD NORME EUROPÉENNE EUROPÄISCHE NORM August 2013 ICS 49.025.40 English Version Aerospace series - Glass fibre thermosetting preimpregnates Technical specification - Part 005: Glass fabric/phenolic resin preimpregnate Série aérospatiale - Préimprégnés de verre textile/résine thermodurcissable - Spécification technique - Partie 005 : Verre textile/résine phénolique préimprégnés Luft- und Raumfahrt - Warmhärtbare Glasfaser - Prepregs Technische Lieferbedingungen - Teil 005: Gewebe Prepregs aus Glasfaser und Phenolharz This European Standard was approved by CEN on May 2013 CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN member This European Standard exists in three official versions (English, French, German) A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management Centre has the same status as the official versions CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and United Kingdom EUROPEAN COMMITTEE FOR STANDARDIZATION COMITÉ EUROPÉEN DE NORMALISATION EUROPÄISCHES KOMITEE FÜR NORMUNG Management Centre: Avenue Marnix 17, B-1000 Brussels © 2013 CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Members Ref No EN 2833-005:2013: E BS EN 2833-005:2013 EN 2833-005:2013 (E) Contents Page Foreword Scope Normative references Definitions, abbreviations Material description .5 5.1 5.2 5.3 Testing Screening Qualification Batch release BS EN 2833-005:2013 EN 2833-005:2013 (E) Foreword This document (EN 2833-005:2013) has been prepared by the Aerospace and Defence Industries Association of Europe - Standardization (ASD-STAN) After enquiries and votes carried out in accordance with the rules of this Association, this Standard has received the approval of the National Associations and the Official Services of the member countries of ASD, prior to its presentation to CEN This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by February 2014, and conflicting national standards shall be withdrawn at the latest by February 2014 Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights CEN [and/or CENELEC] shall not be held responsible for identifying any or all such patent rights According to the CEN-CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and the United Kingdom BS EN 2833-005:2013 EN 2833-005:2013 (E) Scope This standard specifies the requirements for glass fabric/phenolic resin preimpregnates It shall be used together with EN 2833-1 Normative references The following documents, in whole or in part, are normatively referenced in this document and are indispensable for its application For dated references, only the edition cited applies For undated references, the latest edition of the referenced document (including any amendments) applies EN 2155-12 Aerospace series — Test methods for transparent materials for aircraft glazing — Part 12: Determination of linear thermal expansion EN 2377 Aerospace series — Glass fibre reinforced plastics — Test method — Determination of apparent interlaminar shear strength EN 2379 Aerospace series — Fluids for assessment of non-metallic materials EN 2489 Aerospace series — Fibre reinforced plastics — Determination of the action of test fluids EN 2743 Aerospace series — Fibre reinforced plastics — Standard procedures for conditioning prior to testing unaged materials EN 2824 Aerospace series — Burning behaviour of non-metallic materials under the influence of radiating heat and flames — Determination of smoke density and gas components in the smoke of materials — Test equipment, apparatus and media EN 2825 Aerospace series — Burning behaviour of non-metallic materials under the influence of radiating heat and flames — Determination of smoke density EN 2826 Aerospace series — Burning behaviour of non-metallic materials under the influence of radiating heat and flames — Determination of gas components in the smoke EN 3783 properties Aerospace series — Fibre composite materials — Normalization of fibre dominated mechanical EN 3844-1 Aerospace series — Flammability of non-metallic materials — Part 1: Small burner test, vertical – Determination of the vertical flame propagation EN 38344-2 Aerospace series — Flammability of non-metallic materials — Part 2: Small burner test, horizontal — Determination of the horizontal flame propagation 1) EN 3844-3 Aerospace series — Flammability of non-metallic materials — Part 3: Small burner test, 45 — Determination of the resistance of material to flame and glow propagation and to flame penetration ISO 1183-2 Plastics — Methods for determining the density of non-cellular plastics — Part 2: Density gradient column method ISO 1889 Reinforcement yarns — Determination of linear density ISO 3572 Textiles — Weaves — Definitions of general terms and basic weaves prEN 2823 Aerospace series — Fibre reinforced plastics — Determination of the effect of exposure to humid atmosphere on physical and mechanical characteristics 1) BS EN 2833-005:2013 EN 2833-005:2013 (E) prEN 2833-1 Aerospace series — Glass fibre thermosetting preimpregnates — Technical specification — Part 1: General requirements 1) prEN 3615 Aerospace series — Fibre reinforced plastics — Determination of the conditions of exposure to humid atmosphere and of moisture absorption 1) prEN 3703 Aerospace series — Heat release rate for materials and products under the influence of radiating heat and flames — Test method 1) prEN 6032 Aerospace series — Fibre reinforced plastics — Test method — Determination of the glass transition temperatures 1) prEN 6037 strength 1) Aerospace series — Fibre reinforced plastics — Test method — Determination of bearing prEN 7000-1 Aerospace series — Non-metallic materials — Rules for the drafting and presentation of material standards — Part 1: General rules 1) ASTM D-2520 Standard Test Methods for Complex Permittivity (Dielectric Constant) of Solid Electrical Insulating Materials at Microwave Frequencies and Temperatures to 650 °C 2) Definitions, abbreviations Not applicable Material description See table Table – Description of preimpregnate material Parameter Resin Reinforcement Type Type Phenolic Grade Flame resistant Fibre “E” glass Form Fabric in accordance with ISO 3572 1) Published as ASD-STAN Prestandard at the date of publication of this standard 2) Published by: American Society for Testing and Materials (ASTM), 1916 Race Street, Philadelphia, PA 19103, USA BS EN 2833-005:2013 EN 2833-005:2013 (E) Testing 5.1 Screening Screening shall be carried out in accordance with prEN 2833-1 and tables 2, and of this standard 5.2 Qualification Qualification shall be carried out in accordance with prEN 2833-1 and tables 2, 3, and of this specification 5.3 Batch release BS EN 2833-005:2013 Batch release shall be carried out in accordance with prEN 2833-1 and tables and of this specification prEN 7000-1 Characteristic No 301 301 104 104 102 106 a b c d e 104 110 108 105 112 10 11 12 13 14 Gel time/viscosity DSC HPLC Infra-red RF Measurement Glass transition temperature Coefficient of thermal expansion Thickness/ply Fibre content Density (resin) Tack Resin flow Physico-chemical tests as defined in prEN 2833-1 Resin content Volatiles Density (fibre) Fibre mass/unit area Preimpregnate mass/unit area Characteristic ASTM D-2520 prEN 6032 Method B EN 2155-12 – – ISO 1183-2 Method A – – – – – – – – ISO 1889 – – Test method prEN 2833-1 &/or S: Screening; Q: Qualification; B: Batch release; : required for batch release; Equilibrium conditions to be in accordance with prEN 2823; Immersion temperature shall be determined experimentally in accordance with prEN 3615 301 Processed condition 107 107 104 103 301 Delivery condition Test No − − 1 1 1 1 1 − 1 S a 1 1 3 3 3 3 3 Q b − − − − − + + + + + − + + − + + B No of batches required for c Remarks To be measured in the dry condition Also wet after reaching equlibrium at θ °C/85 % RH d e Warp & weft direction The manufacturer shall ensure that the resin block is cured to a standard cure without exotherm, and is void free The requirement for physico-chemical testing as part of batch acceptance testing is to be determined at qualification Fibre density may be obtained from the fibre manufacturers certificate Table – Physical properties – Screening, qualification and batch release EN 2833-005:2013 (E) BS EN 2833-005:2013 EN 2833-005:2013 (E) 305 308 308 307 322 313 311 312 306 316 15 16 17 18 19 20 21 22 23 24 25 d Climbing drum peel Flatwise tensile d Bending stress on sandwich Flexural strength – warp ILSS – 0° Bearing strength In-plane shear (± 45°) Compression – weft Compression – warp Tensile – weft Tensile – warp Characteristic d − − − − − prEN 6037 − − − − − 3 3 3 3 Q b 23 °C − − + + − − – − − − B c Dry − − − − – − − S a 80 °C 1 3 − 1 1 Q b f g − − − − − − − − − S a 80 °C − − – − 1 1 1 Q b Wet 70 °C/85 % RH NOTE All mechanical test results are to be reported from the calculations based on actual specimen dimensions In addition, results of test numbers 15,16,17,18, 19, 20 & 22 are to be reported adjusted to the nominal fibre volume reported in the standard Adjustment shall be in accordance with EN 3783 method B using the nominal cured ply thickness of the relevant material standard e No Of batches to be tested/ test conditions BS EN 2833-005:2013 + Test method prEN 2833-1 &/or Table – Mechanical properties – Screening, qualification and batch release programme S: Screening; Q: Qualification; B: Batch release +: required for batch release; High resin content preimpregnates only; According to EN 2743; Equilibrium conditions to be in accordance with prEN 2823; Conditioning temperature 70 °C shall be used in the specific material standard, or obtained by experiment according to prEN 3615 305 Test No a b c d e f g prEN 7000-1 Characteristic No EN 2833-005:2013 (E) BS EN 2833-005:2013 EN 2833-005:2013 (E) 501 27 Test fuel Liquid 103 (phosphate ester) Environment 7.1 2.2 EN 2379 line No 23 °C/1 000 h 70 °C/1 000 h Ageing conditions EN 2377 EN 2377 Test method 109 109 109 109 28 29 30 31 B: Batch release Q: Qualification S: Screening prEN 7000-1 characteristic No Test No 1 Batches to be tested at 23 °C Heat release Toxic gases Smoke density Flammability 12 s Vertical Overall mean after Mean peak value Flaming mode Non-flaming mode Flaming mode Non-flaming mode Horizontal 60 s Vertical Characteristic prEN 3703 EN 2826 1 1 EN 2824 & 3 3 3 1 3 Q 1 S – – – – – – – – – B No Of batches required for EN 2825 EN 3844-2 EN 2824 & EN 3844-1 Test method Remarks – action of liquid chemicals – residual percentage The following shall be determined in accordance with EN 2489 Remarks If the batch tested for screening or the first batch tested for qualification give results which are less than 30 % of the requirements in the material standard, then the further two qualification batches need not be tested for these characteristics Testing to be carried out on monolithic laminate and honeycomb sandwich structures Table – Fire, smoke and toxicity screening and qualification programme All mechanical test results are to be reported from the calculations based on actual specimen dimensions 501 26 NOTE prEN 7000-1 characteristic No Test No Table – Environmental resistance – Qualification programme EN 2833-005:2013 (E) BS EN 2833-005:2013 EN 2833-005:2013 (E) This page deliberately left blank This page deliberately left blank NO COPYING WITHOUT BSI PERMISSION EXCEPT AS PERMITTED BY COPYRIGHT LAW British Standards Institution (BSI) BSI is the national body responsible for preparing British Standards and other standards-related publications, information and services 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