THE ANALYSIS OF SLAGS AND RELATED OXIDE TYPE MATERIALS () Á symposium presented at the PiHsburgh Conference Cleveland, Ohio, Z7 March 1973 sponsored by ASTM E 2 on Emission Špectroscopy ASTM SPECIAL T[.]
Contents Tape Introductory Remarks G L Mason Side The Application of Multi-Channel Spectrometers to the Elemental Analysis of Oxide Materials W Ramsden, Applied Research Laboratories, Ltd., Luton (Beds.), England Current Status of X-Ray Emission Analysis for the Analysis of Slags and Related Oxide-Type Materials -R Jenkins, Philips Electronic Instruments, Mount Vernon, N, Y 10550 1. .continued Side Atomic Absorption Spectrophotometry in the Analysis of Slags and Oxides M D Amos, Varian Techtron Pty Ltd., Melbourne, Australia 3171 Utility of the Optical Emission Spectrometer in the Analysis of Refractories, Slags, and Other Oxide Materials-J R Ryan and R K Scott, Garber Research Center, Harbison-Walker Refractories, Division of Dresser Industries, Inc., Pittsburgh, Pa 15227 X-Ray Emission Spectrometer Analysis of Slags and Related Materials J C Cline and R A Pontello, Globe Metallurgical Corp., Division of Interlake, Inc., Beverly, Ohio 45715 continued Side Analysis of Slags by Atomic Absorption Spectrophotometry-H G Zelinske and D H Arendt, Amsted Research Labs., Bensenviile, Ill 60106 2 Questions and Answers 2 (~) BY AMERICAN SOCIETY FOR TESTING AND MATERIALS 1973 Copyright by ASTM Int'l (all rights reserved); Sun Jan 21:31:53 EST 2016 Downloaded/printed by University of Washington (University of Washington) pursuant to License Agreement No further reproductions auth STP542-EB/Mar 1973 W Ramsden The Application of Multi-Channel Spectrometers to the Elemental Analysis of Oxide Materials z 7o ~- 65 55 u- 50 o~ 45 ~? 4O _~3s ~ 50 ~- 25 )'i ~ 2o I I 10 MILLING TIME,m, FIG I E f f e c t of p a r t i c l e size on e m i s s i o n Copyright by ASTM Int'l (all rights reserved); Sun Jan 21:31:53 EST 2016 Copyright~1973 bybyASTM International www.astm.org Downloaded/printed University of Washington (University of Washington) pursuant to License Agreement No further reproductions authorized ANALYSIS OF SLAGS AND RELATED OXIDE-TYPE MATERIALS 7I ~t'~ - ~ i j - ~ ~o0 ~9 I Influence | O f Grinding ? GRIKtDIN;TIHE.m~n Time, High Grade Sinter, Mean O f Laboratory Results ~Ca0 I z w Ib " ~ ~ ' 13 S~Oz ] t~,o & ill I , I I I I r162 Influence Fig I I I I ] S T T|H,~mm Of Grinding Time, Low Grade Sinter, /Vtean O f Effect O f Grind;ng Time on XRF Analysis Of Laboratory Results Sinters Copyright by ASTM Int'l (all rights reserved); Sun Jan 21:31:53 EST 2016 Downloaded/printed by University of Washington (University of Washington) pursuant to License Agreement No further reproductions authorized RAMSDEN ON MULTI-CHANNEL SPECTROMETERS Copyright by ASTM Int'l (all rights reserved); Sun Jan 21:31:53 EST 2016 Downloaded/printed by University of Washington (University of Washington) pursuant to License Agreement No further reproductions authorized ANALYSIS OF SLAGS AND RELATED OXIDE-TYPE MATERIALS Copyright by ASTM Int'l (all rights reserved); Sun Jan 21:31:53 EST 2016 Downloaded/printed by University of Washington (University of Washington) pursuant to License Agreement No further reproductions authorized RAMSDEN ON MULTI-CHANNEL SPECTROMETERS Fig SiOz / 60 FIRE BRICKS 40 2O SINTER BASIC 5LAG CHROME OF~E 1000 2000 m volts Copyright by ASTM Int'l (all rights reserved); Sun Jan 21:31:53 EST 2016 Downloaded/printed by University of Washington (University of Washington) pursuant to License Agreement No further reproductions authorized ANALYSIS OF SLAGS AND RELATED OXIDE-TYPE MATERIALS Copyright by ASTM Int'l (all rights reserved); Sun Jan 21:31:53 EST 2016 Downloaded/printed by University of Washington (University of Washington) pursuant to License Agreement No further reproductions authorized 0"2 0.4 1"2 20 30 40 0"2 ~ I '2 i'4 - I 10 I 20 iron per cent Effect of a b s o r p t i o n c o r r e c t i o n s on c a l i b r a t i o n for Fe in iron ores and sinter iron, per mlt FIG i I0 Copyright by ASTM Int'l (all rights reserved); Sun Jan 21:31:53 EST 2016 Downloaded/printed by University of Washington (University of Washington) pursuant to License Agreement No further reproductions authorized ~ o 1'4 , I 30 I 40 m I m -r :D Z Z rT1 rU) "o C Z Z m ANALYSIS OF SLAGS A N D RELATED OXIDE-TYPE MATERIALS Fig 1,5 C~ILqEC lEO X'RAY INT|N$1~ J / 1.0 0.5 o.s lo 0.5 1.0 % MgO ~.~ 1.5 1.0 0.5 1.5 2.0 % MgO Copyright by ASTM Int'l (all rights reserved); Sun Jan 21:31:53 EST 2016 Downloaded/printed by University of Washington (University of Washington) pursuant to License Agreement No further reproductions authorized 18 ANALYSIS OF SLAGS AND RELATED OXIDE-TYPE MATERIALS 11 9~ 10 $0 crystal s p e c t r o m t e r J 1~ 0.2 Wawlan~)th~ j 04 Comparative resolutions of the flow counter, the scintillation counter, the semiconductor counter, end the crystal spectrometer Figure # Copyright by ASTM Int'l (all rights reserved); Sun Jan 21:31:53 EST 2016 Downloaded/printed by University of Washington (University of Washington) pursuant to License Agreement No further reproductions