0
  1. Trang chủ >
  2. Khoa Học Tự Nhiên >
  3. Hóa học - Dầu khí >

Ebook A Handbook of spectroscopic data chemistry Part 2

Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 17)

Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 17)

... sampling until injection to GC, and from the standard solution to a test specimen) In principle, the sampling, extraction and GC analysis should be made at low temperature, in a gastight state and ... transformation in rats J Pharm Sci 74:780–782 10) Kielbasa WB, Bauer JA, Fung HL (1999) Analysis of isobutyl nitrite inhalant in rat and human blood: application for pharmacokinetic investigations J Chromatogr ... concentration of an alkyl nitrite on the horizontal axis and peak area on the vertical axis The concentration of the analyte in a specimen is calculated using the calibration curve i Assessment and some...
  • 6
  • 580
  • 0
Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 67)

Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 67)

... GC/MS analysis for DAEMS in serum (a) a total ion chromatogram (TIC) and a mass chromatogram; (b) an EI mass spectrum of DAEMS; (c) a CI mass spectrum of DAEMS Poisoning case, and toxic and fatal ... GC/MS analysis for EMPA in serum (a) a TIC and mass chromatograms; (b) an EI mass spectrum of the t-BDMS derivative of EMPA; (c) a CI mass spectrum of the same derivative of EMPA data of animals According ... concentrations of DAEMS are spiked into blank serum specimens containing a fixed amount of DAEMO (IS) each and extracted as described before Since the base peaks of DAEMS and DAEMO (IS) equally appear...
  • 9
  • 548
  • 0
Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 20)

Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 20)

... 188 Cannabinoids and their metabolites GC analysis of cannabinoids in plant specimensa Reagents and their preparation • • • Extraction and purification of cannabinoids [3]: Cannabis sativa L is ... construct a calibration curve with cannabinoid concentration on the horizontal axis and with peak area ratio of a cannabinoid to IS on the vertical axis GC analysis of cannabinoids in plant specimens ... side-chain hydroxylated ∆6-tetrahydrocannabinol metabolites Acta Pharm Suec 16:21–33 9) Yamamoto I, Watanabe K, Narimatsu S et al (1990) A GC-MS method for determination of ∆9-tetrahydrocannabinol-11-oic...
  • 8
  • 509
  • 0
Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 21)

Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 21)

... Main metabolic pathways of morphine, heroin and codeine The thick and thin arrows show the main and minor metabolic pathways, respectively ⊡ Figure 3.1 196 Morphine and its analogues GC and ... Qualitative analysis is made by the comparison of the retention time of a peak of a specimen with that of the authentic standard and also by the confirmation of the absence of such a peak in a ... morphine, codeine and tetrahydropapaveroline in Parkinsonian patient undergoing L-3,4-dihydroxyphenylalanine therapy: a possible biosynthetic pathway of morphine from L-3,4-dihydroxyphenylalanine...
  • 12
  • 479
  • 0
Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 70)

Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 70)

... normal cyanosis headache, dyspnea, tachypnea, tachycardia and hypertension mental derangement, listlessness and metabolic acidosis coma, convulsive attack and hypotension death A poisoning case ... centrifugation at 3,000 rpm for min, 1- or 4- L of the upper layer is injected into GC Various known amounts of nitrate and a fixed amount of IS are added to blank specimens and processed in the same way ... of the oxidation of nitrite into nitrate and the same extractions as those for nitrate A calibration curve for nitrite using blank specimens and IS is also prepared for quantitation in the same...
  • 6
  • 489
  • 0
Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 71 and End)

Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 71 and End)

... amanitin 473, 477, 479 amido-type local anesthetic 385 1-amino-4-phenylbutane 173 2-amino-6-hydroxymethyl8-hydroxyquinazoline 482 aminomethyl phosphonic acid 546 7-aminonitrazepam 19 5-aminoquinoline ... alminoprofen 325, 330, 332 alprazolam 284, 285, 290 alternative specimens Amanita neoovoidea 480 Amanita pantherina 469 Amanita phalloides 469 Amanita verna 469, 474 Amanita virosa 469, 473 amanitin ... N-chloromethylphthalimide 327 N-de-ethyl-LSD 228 n-decane 165 n-heptane 165 n-hexane 165 N-methyl- 1-( 3,4-methylenedioxyphenyl )-2 -butanamine 229 N-methyl- 1-( 3,4-methylenedioxyphenyl )-3 -butanamine 233 N-methyl-bis(trifluoroacetamide)...
  • 17
  • 559
  • 0
Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 22)

Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 22)

... shows mass spectra of the authentic cocaine, EME and BE after derivatization Setting up of cutoff values are very common in USA and Europe as a part of QC (quality control) and QA (quality assurance) ... Significance and problems of doping tests and toxin analysis Nipponrinsho 57:361–363 (in Japanese) 10) Sander R, Ryser MA, Lamoreaux TC et al (1985) An epidemic of cocaine associated deaths in Utah ... and death In addition, the ratios of cocaine to BE in blood and in the brain, and the brain-to-blood ratios of cocaine and BE were compared with those described in literature [11]; such comparison...
  • 12
  • 479
  • 0
Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 23)

Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 23)

... concentration in the horizontal axis and peak area ratio of pentazocine to IS in the vertical axis The peak area ratio of a test specimen is applied to the calibration curve to obtain its pentazocine ... bring its pH to about A 10-mL volume of ethanol and 10 mL distilled water are passed through a Sep-Pak C18 cartridge using a 10-mL volume glass syringe to activate the cartridge at a flow rate ... (17) 285 (9) Poisoning case, and toxic and fatal concentrations A 17-year-old female [11] ingested about 100 tablets of pentazocine (total amount estimated, 2.5 g) and fell into unconsciousness...
  • 5
  • 428
  • 0
Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 24)

Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 24)

... blood and urine, because its amount to be ingested is as small as about 10 µg and LSD is rapidly metabolized in human bodies As metabolites of LSD, 2-oxo-LSD, 3-, 1 3- and 14-hydroxy-LSDs and an N-de-ethyl-LSD ... Jiho Inc., Tokyo, pp 108–109 (in Japanese) 2) The Pharmaceutical Society of Japan (ed) (1992) Standard Methods of Chemical Analysis in Poisoning – With Commentary – Nanzando, Tokyo, p 43 and p ... N-de-ethyl-LSD are known [3] After oral ingestion of 160 µg LSD, the maximum blood concentration of LSD was ng/mL and its half-life is said to be about h The concentrations of LSD of LSD-abusing...
  • 4
  • 465
  • 0
Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 25)

Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 25)

... main metabolites 4-hydroxy-3-methoxymethamphetamine (HMMA) and 4-hydroxy-3-methoxyamphetamine (HMA) in urine specimens are presented 3,4-Methylenedioxyamphetamines Reagents and their preparation ... concentrations 9) Pizarro N, Ortuño J, Farré M et al (2002) Determination of MDMA and its metabolites in blood and urine by gas chromatography-mass spectrometry and analysis of enantiomers by capillary ... Rapid simultaneou determination of amphetamine, methamphetamine, 3,4-methylenedioxyamphetamine, 3,4-methylenedioxymethamphetamine, and 3,4-methylenedioxyethylamphetamine in urine by solid-phase...
  • 11
  • 509
  • 0
Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 26)

Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 26)

... Levine B et al (2002) Intra- and interindividual variations in urinary concentrations of endogenous gamma-hydroxybutyrate J Anal Toxicol 26:340–346 26) Yeatman DT, Reid K (2003) A study of urinary ... responding verbally; the levels of serum creatinin kinase and aspartate aminotransferase were more than 100-times the normal limits On hospital day 2, he became rigid, diaphoretic and had a temperature ... human body fluids by headspace solid-phase microextraction (SPME) Chromatographia 43:331–333 14) Nakahara Y, Takahashi K, Sakamoto T et al (1997) Hair analysis for drugs of abuse X VII Simultaneous...
  • 12
  • 492
  • 0
Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 27) ppt

Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 27) ppt

... Louis, MO, USA) Pure powder of perazine and clospirazine was donated by Mitsubishi Welpharma, Osaka, Japan; that of flupentixol by Takeda Chem Ind Ltd., Osaka, Japan; that of thioproperazine by Shionogi ... concentration on the horizontal axis and of peak area ratio of a drug to IS on the vertical axis The above peak area ratio obtained from a specimen is applied to the calibration curve to obtain its ... GC/MS At least vials containing various concentrations of a target compound are prepared for a calibration curve Assessment of the method All eleven kinds of phenothiazine drugs gave the base peaks...
  • 7
  • 458
  • 0
Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 28) pptx

Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 28) pptx

... Butyrophenones HPLC analysis Instrument: an SPD-M1 0A photodiode array detector (DAD), a CTO-1 0A column oven, an SIL-1 0A autosampler and an LC-10AD pump system (all from Shimadzu Corp., Kyoto, Japan) HPLC ... with relatively high molecular weights, LC/MS may be most suitable Poisoning cases, and toxic and fatal concentrations A 2-year plus month-old female and an 11-month-old male [18] had ingested ... IS and 0.5 mL of M NaOH are placed in a 15-mL volume glass centrifuge tube with a ground -in stopper and mixed well, followed by addition of mL of the mixture of n-hexane/isopropanol and its shaking...
  • 8
  • 592
  • 0
Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 29) ppt

Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 29) ppt

... and tetracyclic antidepressants and carbamazepine obtained by HPLC-UV A: carbamazepine, B: desipramine, C: maprotiline, D: nortriptyline, E: amoxapine, F: setiptiline, G: mianserin, H: imipramine, ... concentrations of tricyclic and tetracyclic antidepressants Compound amitriptyline amoxapine carbamazepine clomipramine desipramine dosulepin imipramine lofepramine maprotiline mianserin nortriptyline ... (in Japanese) 3) Tanaka E, Terada M, Nakamura T et al (1997) Forensic analysis of eleven cyclic antidepressants in human biological samples using a new reversed-phase chromatographic column of...
  • 11
  • 464
  • 0
Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 30) doc

Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 30) doc

... chromatograms of triazolam, 4-hydroxytriazolam, α-hydroxytriazolam and alprazolam (IS) A 100-ng aliquot each of triazolam, 4-hydroxytriazolam and α-hydroxytriazolam and 50 ng of alprazolam were added ... 4-hydroxytriazolam and α-hydroxytriazolam in plasma and urine The quantitativeness could be observed in the range of 50–400 ng/mL for all compounds in both plasma and urine Toxic and fatal concentrations ... oxazolam, cloxazolam, mexazolam, flutazolam and haloxazolam having oxazolo rings in their structures [1] In such cases, the relatively low injection temperature and the use of a wide-bore capillary...
  • 10
  • 597
  • 0

Xem thêm

Từ khóa: Báo cáo thực tập tại nhà thuốc tại Thành phố Hồ Chí Minh năm 2018Nghiên cứu sự hình thành lớp bảo vệ và khả năng chống ăn mòn của thép bền thời tiết trong điều kiện khí hậu nhiệt đới việt namNghiên cứu tổ chức pha chế, đánh giá chất lượng thuốc tiêm truyền trong điều kiện dã ngoạiNghiên cứu tổ hợp chất chỉ điểm sinh học vWF, VCAM 1, MCP 1, d dimer trong chẩn đoán và tiên lượng nhồi máu não cấpGiáo án Sinh học 11 bài 13: Thực hành phát hiện diệp lục và carôtenôitGiáo án Sinh học 11 bài 13: Thực hành phát hiện diệp lục và carôtenôitQuản lý hoạt động học tập của học sinh theo hướng phát triển kỹ năng học tập hợp tác tại các trường phổ thông dân tộc bán trú huyện ba chẽ, tỉnh quảng ninhPhối hợp giữa phòng văn hóa và thông tin với phòng giáo dục và đào tạo trong việc tuyên truyền, giáo dục, vận động xây dựng nông thôn mới huyện thanh thủy, tỉnh phú thọPhát hiện xâm nhập dựa trên thuật toán k meansThiết kế và chế tạo mô hình biến tần (inverter) cho máy điều hòa không khíSở hữu ruộng đất và kinh tế nông nghiệp châu ôn (lạng sơn) nửa đầu thế kỷ XIXChuong 2 nhận dạng rui roQuản lý nợ xấu tại Agribank chi nhánh huyện Phù Yên, tỉnh Sơn La (Luận văn thạc sĩ)Tranh tụng tại phiên tòa hình sự sơ thẩm theo pháp luật tố tụng hình sự Việt Nam từ thực tiễn xét xử của các Tòa án quân sự Quân khu (Luận văn thạc sĩ)Nguyên tắc phân hóa trách nhiệm hình sự đối với người dưới 18 tuổi phạm tội trong pháp luật hình sự Việt Nam (Luận văn thạc sĩ)Giáo án Sinh học 11 bài 14: Thực hành phát hiện hô hấp ở thực vậtBÀI HOÀN CHỈNH TỔNG QUAN VỀ MẠNG XÃ HỘIChiến lược marketing tại ngân hàng Agribank chi nhánh Sài Gòn từ 2013-2015Đổi mới quản lý tài chính trong hoạt động khoa học xã hội trường hợp viện hàn lâm khoa học xã hội việt namQUẢN LÝ VÀ TÁI CHẾ NHỰA Ở HOA KỲ