Thermal Analysis - Fundamentals and Applications to Polymer Science Part 10 pot

... in the case of DSC-RLI. 6.5 Simultaneous DSC-X-Ray Analysis Simultaneous DSC-X-ray analysis is a very powerful and versatile method for following changes in the morphology and structure of a ... DSC-TLI (Section 6.4.2), are available for simultaneous DSC-small-angle X-ray scattering, wide-angle X-ray diffraction and synchrotron orbital radiation analysis (SAXS, 0.25 < 2 θ ≤...

Ngày tải lên: 10/08/2014, 12:21

... 430 K and at 439 K are attributed to melting of α-type crystals and melting of recrystallized α-type crystals, respectively. At high heating rates only the melting peaks of ß-type and α-type ... (IV) 10; (V) 20; (VI) 40 K/min. (B) Decon- volution of the DSC curve recorded at 10 K/min. (Reproduced by permission of the Japan Society of Calorimetry and Thermal Analysis fr...

Ngày tải lên: 10/08/2014, 12:21

... of Polymer Chemistry, Cornell University Press, Ithaca, New York (1953). [22] Mandelkern, L. Crystallization of Polymers, McGraw-Hill, New York (1964). [23] Yamamoto, Y. , Nakazato, M. and Saito, ... cooling, is called the gel-sol transition and can be monitored by HS-DSC. The HS-DSC curve of the gel-sol transition is often very broad and structured on both heating and cooling. Hys...

Ngày tải lên: 10/08/2014, 12:21

... 6.27. Thermal diffusivity of n-alkane as a function of temperature and the corresponding DSC curve. The low- temperature feature is due to a crystal -to- crystal transition and the high-temperature ... of short-duration pulses and the thermal emission transient observed by means of a wide-band infrared detector (Figure 6.32). An optothermal decay curve plots the intensity of...

Ngày tải lên: 10/08/2014, 12:21

... xl0 -3 2.777 778 x10 -7 9.868 96 x10 -3 0 .101 972 4.184 1 3.965 73 x10 -3 1.162 222 x10 -6 4.129 29 x10 -2 0.426649 1.055 040 x10 3 2.521 61 x10 2 1 2.930 667 x10 -4 10. 412 44 1.075 84 x10 2 3.6 ... x10 2 3.6 x10 6 8.604 21 x10 5 3.412 19 x10 3 1 3.552 92 x10 4 3.670 98 x10 5 1.013 25 x10 2 24.217 3 9.603 90 x10 -2 2.814 583 x10 -5 1 10. 332 23 9.806 65...

Ngày tải lên: 10/08/2014, 12:21

... 96 , 109 , 111 , 113 , 115 WAXD, see Thermally stimulated current Wide - angle X - ray scattering 140 William - Landel - Ferry (WLF) equation 132 Work station 4 X X - ray diffractometry ... 106 , 109 , 110 , 111 , 115 , 139 , 159 DSC melting curve, PE 32 , 33 DSC, automated 21 heat - flux type 8 , 9 , 10 , 160 power compensation 11 , 12...

Ngày tải lên: 10/08/2014, 12:21

... (mA) BRP-1a 0.122 0.011 BRP-1b 0.096 0.012 BRP-1c 0.114 0.013 BRP-2a 0.089 0.009 BRP-2b 0.092 0.009 BRP-2c 0 .102 0.009 SAA-1a 0. 110 0.011 SAA-1b 0.079 0. 010 SAA-1c 0.088 0.011 SAA-2a 0.083 ... implanted detector with the same active volume thickness is shown in Figure 12. 1 10 100 100 0 100 00 100 000 0 500 100 0 1500 2000 2500 Channel Number Counts per Channel 1 10...

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Ngày tải lên: 11/08/2014, 09:21