... number of aspects of constructing a model of grammatical representation need further devel- opment. Some of these aspects have been alluded to in the course of this presentation. Any model of grammatical ... acquisition of syntax by Tomasello, Lieven, Pine, and others offers evidence for a usage-based, inductive model of the acquisition of syntax. Evidence from very detailed...
Ngày tải lên: 03/07/2014, 01:20
... solution b . Many of the phenothiazine drugs are in the forms of hydrochloride salt. For example, to prepare 1 mg/mL solution of the free form of chlorpromazine, the amount of chlorpromazine ... 10–100 fold. k) As probable reasons of such a phenomenon, the slight thermal decomposition of the authentic standard during the step of GC, and/or protection of the target phenot...
Ngày tải lên: 15/12/2013, 12:15
Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 28) pptx
... volume of urine or blood, 0.05 mL IS and 0.5 mL of 1 M NaOH are placed in a 15-mL volume glass centrifuge tube with a ground-in stopper and mixed well, followed by addi- tion of 6 mL of the ... dissolved in 0.1 mL of the mobile phase of HPLC or LC/MS. ii. For HPLC-DAD and LC/MS, 50 and 20 µL of the above solution are injected, respec - tively. iii. For the SIM of LC/MS, the i...
Ngày tải lên: 15/12/2013, 12:15
Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 29) ppt
... mobile phase (B). With the use of the Eclipse XDB-C 8 column, the peak top of nortriptyline (D) could be separated from that of amoxapine (E), but major parts of their peaks could not be separated. ... tentative identi cation of drugs, a UV absorbance spectrum can be measured together with the con rmation of coincidence of retention time of a test peak with that of an...
Ngày tải lên: 15/12/2013, 12:15
Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 31) ppt
... possibilities of concomitant ingestion of other drugs should be taken into consideration. HPLC chromatograms for blood extracts in the presence and absence of bromisovalum and IS. The concentration of ... 10 mL distilled water and eluted with 3 mL of dichloromethane/methanol (9:1). vi. A er removal of a small amount of the upper layer (aqueous phase) of eluate with a Past...
Ngày tải lên: 15/12/2013, 12:15
Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 32) ppt
... column with a particle diameter of 2 µm in place of 5 µm; the smaller diameter gives various advantages, such as higher sensitivity, rapid analysis and a smaller amount of the ow of mobile phase. ... good linearity in the range of 0.2–10 ng on-column (0.2– 10 µg/mL). e detection limits of this method were 60–90 µg/mL in serum. e recovery rates of 0.1–5.0 µg of barbitu...
Ngày tải lên: 15/12/2013, 12:15
Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 37) pptx
... steam of nitrogen with warming at 40 °C. vi. e residue is dissolved in 100 µL of the mobile phase. vii. A xed amount of the solution is injected into HPLC. viii. For construction of calibration ... 75:734–736 24) Chaikin P, Adir J (1987) Unusual absorption profile of phenytoin in a massive overdose case. J Clin Pharmacol 27:70–73 354 Antiepileptics Mobile phase: 0.01 M pot...
Ngày tải lên: 15/12/2013, 12:15
Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 38) pptx
... condensation of the eluate, there is a possibility of loss of the analyte due to its adsorption to the glassware. It is preferable to use a plastic container for condensation under a stream of nitrogen ... Preparation of the monocholine ester of succinic acid and some related derivatives. J Am Chem Soc 75:4725–4727 3) The Pharmaceutical Society of Japan (ed) (1992) Standard...
Ngày tải lên: 24/12/2013, 18:15
Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 39) ppt
... urine of subjects, who had ingested each of them. The results were obtained after single oral intake of each drug. In the analysis of atenolol, double peaks appeared for this drug, because of ... performance. As untoward e ects of these drugs, chill of extremities due to the contraction of vessels and aggravation of bronchial asthma due to contraction of the bronchi c...
Ngày tải lên: 24/12/2013, 18:15
Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 43) pptx
... contained. During preparation of the solutions and also during analysis, there is a possibility of decomposition of the hypochlorite ion. As shown in > Figure 1.1, the peaks of such decomposition ... rapidly. Because of such reasons, there are no data available on the fatal blood levels of hypochlorite. ere is a report describing the di culty for detecting hypochlorite f...
Ngày tải lên: 24/12/2013, 18:15