Chita : A Memory of Last Island This Etext ppt

... wild cane, and marsh grasses. For, at a hasty glance, the general appearance of this marsh verdure is vague enough, as it ranges away towards the sand, to convey the idea of amphibious vegetation, ... tells of hereditary refinement of habit and of mind: a natural grace, a thorough-bred ease and elegance of movement, a quickness and delicacy of perception. She became st...

Ngày tải lên: 06/03/2014, 23:21

... concentration on the horizontal axis and of peak area ratio of a drug to IS on the vertical axis.  e above peak area ratio obtained from a specimen is applied to the calibration curve to obtain ... MO, USA). Pure powder of perazine and clospi- razine was donated by Mitsubishi Welpharma, Osaka, Japan; that of  upentixol by Takeda Chem. Ind. Ltd., Osaka, Japan; that of thiopr...

Ngày tải lên: 15/12/2013, 12:15

... Butyrophenones HPLC analysis Instrument: an SPD-M1 0A photodiode array detector ( DAD), a CTO-1 0A column oven, an SIL-1 0A autosampler and an LC-10AD pump system (all from Shimadzu Corp., Kyoto, Japan). HPLC ... spiked to blank blood or urine to draw a calibration curve. A peak area ratio of a test specimen is applied to the calibration curve to calculate its concentration. A...

Ngày tải lên: 15/12/2013, 12:15

... antidepressants and carbamazepine obtained by HPLC-UV. A: carbamazepine, B: desipramine, C: maprotiline, D: nortriptyline, E: amoxapine, F: setiptiline, G: mianserin, H: imipramine, I: amitriptyline, ... Japanese) 3) Tanaka E, Terada M, Nakamura T et al. (1997) Forensic analysis of eleven cyclic antidepressants in human biolo- gical samples using a new reversed-phase chromatographic...

Ngày tải lên: 15/12/2013, 12:15

... Tanaka E, Nakamura T, Nagashima A et al. (2001) Determination of plasma bromvalerylurea and its main meta- bolite by a simple high-performance liquid chromatographic method and quantitation of ... bromide and urea: 5 g of 2-bromohexanoyl bromide (Aldrich, Milwaukee, WI, USA) and an equimolar amount of urea are placed in a 100 mL volume eggplant-shaped glass  ask and warmed in...

Ngày tải lên: 15/12/2013, 12:15

... µg/mL. 1: barbital; 2: allobarbital; 3: metharbital; 4: phenobarbital; 5: cyclobarbital; 6: pentobarbital; 7: hexobarbital; 8: amobarbital; 9: secobarbital; 1 0: thiopental; 1 1: IS [ 5-(4-methylphenyl)-5-phenylhydantoin]. ⊡ ... activated charcoal. JAMA 24 7:2 400–2401 24) Furuno J, Sugawara N (1972) On a fatal case of thiopental shock and the meta...

Ngày tải lên: 15/12/2013, 12:15

... diazepam. 353 HPLC analysis of antiepileptics and some metabolites in plasma [15] Reagents and their preparation • Ethosuximide, primidone, phenobarbital, carbamazepine, phenytoin and carbamazepine- epoxide ... kinds of antiepileptics ( ethosuximide, primidone, lamotrigine, phenobarbi- tal, phenytoin and carbamazepine) and two carbamazepine metabolites ( carbamazepine-diol and carbamaze...

Ngày tải lên: 15/12/2013, 12:15

... ➁ : methanol/tetrahydrofuran/5 % formic acid ( 7:7 :6 , v/v); ➂ : methanol/chloroform/acetic acid ( 5:4 :1 , v/v); ➃ : Dragendorff reagent; ➄ : iodoplatinate reagent TLC analysis 362 Muscle relaxants ... ammonium acetate/acetoni- trile can be used. With ODS-type columns, tri uoroacetic acid can be added to a mobile phase as an ion-pairing reagent for analysis...

Ngày tải lên: 24/12/2013, 18:15

... uoroacetic anhydride, a base peak at a higher mass number due to a TFA derivative of a β-blocker can be obtained a er heating and evaporation of the excess reagent; for example, the mass spectrum ... concentrations of the authentic standard of a drug and the IS, and are processed according to the above procedure to construct each calibra- tion curve. By applying the peak...

Ngày tải lên: 24/12/2013, 18:15

... solutions are analyzed by the above CE to construct a calibration curve (concentration of a hypochlorite ion in a specimen vs. peak area). A peak area obtained from a specimen is applied to the calibration ... conditions: an HP 3D CE system (Yokogawa Analytical Systems, Tokyo, Japan); bu er solution: HP Basic Anion Bu er; column temperature: 30 °C; impressed voltage: –30 kV;...

Ngày tải lên: 24/12/2013, 18:15